Abstract: The present invention relates to an improved and efficient process for the synthesis of 2-[2-(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-2,4-dihydro-3H-1,2,4-triazole-3-thione, compound of formula (I) (Prothioconazole). The present invention more particularly relates to an improved process for manufacturing of 2-(1-chloro-cycloprop-1-yl)-3-(2-chloro phenyl)-2-hydroxy propyl-1-hydrazine (compound of formula III) and 2-[2-(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2,4-triazolidine-3-thione (compound of formula II) which are mainly used for synthesis of Prothioconazole which is knows as an active compound with microbicidal fungicidal properties.
Type:
Grant
Filed:
December 20, 2018
Date of Patent:
April 5, 2022
Assignee:
GSP CROP SCIENCE PVT. LTD.
Inventors:
Subhash Rajaram Kadam, Nilesh Jani, Ravindra Shinde, Kenal V. Shah, Bhavesh V. Shah, Ajit Singh Gujral, Ganganarasaiah Byregowda, Ganadi Sivaiah, Jivan Dhanraj Pawar, Hari Narayan Pati
Abstract: The present invention relates to a novel and improved process for preparation of methyl [2-({[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy}methyl)phenyl]methoxycarbamate (Pyraclostrobin) of formula (I) in free form or in agrochemically acceptable salt form useful as a pest control agent starting from methyl [2-({[1-(4-chlorophenyl)-1-H-pyrazol-3-yl]oxy}methyl)phenyl]hydroxycarbamatein simple manner and in high purity and good yield.
Type:
Grant
Filed:
January 16, 2019
Date of Patent:
February 8, 2022
Assignee:
GSP CROP SCIENCE PVT. LTD.
Inventors:
Ajit Singh Gujral, Kenal V. Shah, Bhavesh V. Shah, Subhash Rajaram Kadam, Nilesh N. Jani, Ravindra Y. Shinde
Abstract: The present invention relates to an improved and efficient process for the synthesis of 2-[2-(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-2,4-dihydro-3H-1,2,4-triazole-3-thione, compound of formula (I) (Prothioconazole). The present invention more particularly relates to an improved process for manufacturing of 2-(1-chloro-cycloprop-1-yl)-3-(2-chloro phenyl)-2-hydroxy propyl-1-hydrazine (compound of formula III) and 2-[2-(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2,4-triazolidine-3-thione (compound of formula II) which are mainly used for synthesis of Prothioconazole which is knows as an active compound with microbicidal fungicidal properties.
Type:
Application
Filed:
December 20, 2018
Publication date:
November 26, 2020
Applicant:
GSP CROP SCIENCE PVT. LTD.
Inventors:
Subhash Rajaram Kadam, Nilesh Jani, Ravindra Shinde, Kenal V. Shah, Bhavesh V. Shah, Ajit Singh Gujral, Ganganarasaiah Byregowda, Ganadi Sivaiah, Jivan Dhanraj Pawar, Hari Narayan Pati