Abstract: The method involves measuring hydrogen permeation in the tubes by mass spectrometry, wherein the tube is inserted into a high or ultrahigh vacuum device in which a mass spectrometer and a total pressure gauge are located. H2 or H2 and inert gas mixtures are circulated inside the tube at the required partial pressure. The tube is then heated and the appearance of H2 outside the tube is observed. The flow thereof inside the tube and emergence time, called permeation time, are determined based on permeation curves. The emergence time of the first microcrack is also determined.
Type:
Grant
Filed:
March 13, 2003
Date of Patent:
March 29, 2005
Assignees:
Consejo Superior de Investigaciones Cientificas, Iberdrola
Inventors:
José Luis Sacedón Adelantado, Eduardo Santamera Gago, Marcos Díaz Muñoz, José Serafin Moya Corral, Elisa Román García, Angel Samuel Pérez Ramírez, Begoña Remartínez Zato