Abstract: An improved method is described for presulfiding and preconditioning a residuum hydrotreating or hydrocracking catalyst as an integrated part of the hydroconversion process in which catalyst is added on-stream intermittently or continuously without interruption of the hydroconversion process. The method is used to condition, activate, or presulfide fresh or regenerated catalyst prior to its addition to the hydroconversion reactor utilizing product streams from the hydroconversion process.
Abstract: A process for catalytic multi-stage hydrogenation of heavy carbonaceous feedstocks using catalytic ebullated bed reactors is operated at selected flow and operating conditions so as to provide improved reactor operations and produce increased yield of lower boiling hydrocarbon liquid and gas products. The disclosed process advantageously takes advantage of an external gas/liquid separation unit associated with the first stage reactor to allow for a more efficient and effective catalytic hydrocracking process. The more efficient process is primarily a result of the increased catalyst loading and lower gas hold-up in the ebullated reactors.
Type:
Grant
Filed:
May 29, 1998
Date of Patent:
August 7, 2001
Assignee:
IFP North America, Inc.
Inventors:
James J. Colyar, James B. MacArthur, Eric D. Peer
Abstract: A pressurized vertically-oriented catalytic reactor vessel has a fluid flow distribution grid plate fixedly mounted transversely in the reactor lower portion for supporting a bed of particulate catalyst above the grid plate, and has at least one elongated conduit for catalyst addition/withdrawal extending upwardly through the reactor lower head and the grid plate. The catalyst addition/withdrawal conduit has a concentric bellows type expansion unit sealably attached at its lower end to the upper side of the grid plate, the bellows unit being sealably attached at its upper end to the catalyst conduit, so that the conduit can thermally expand vertically, and gas leakage cannot occur around the conduit and the grid plate into the catalyst bed.