Abstract: A process comprising spent metal etching solutions, the process comprising the steps of: 1) extracting the metal ions from the spent etching solution by means of a liquid ion exchanger; 2) washing the liquid ion exchanger by means of water; 3) vaporizing the washing water; 4) crystallizing the concentrate after vaporization; 5) filtering the regenerated etching solution; 6) restoring the quality of the etching solution; 7) reextracting the metal from the metal-loaded ion exchanger; 8) washing the liquid ion exchanger; 9) neutralizing the washing water; 10) filtering after carrying out the neutralization; and 11) recovering metal electrolytically.