Abstract: The method of producing lithium titanate anode material for lithium ion battery applications is comprising of: a) mixing of mixed phase having 60-80% anatase and 20-40% rutile of TiO2 as titanium precursor with Li2CO3 as lithium precursor in a stoichiometric ratio of 5:4 and adding with 2 to 5% stearic acid as process control agent as well as carbon precursor; b) milling in horizontal attrition milling unit maintained with the ball to powder ratio of 10:1-12:1 at 250-500 rpm for 0.5 to 2 hrs c) repeating the milling for 40 to 48 times; d) palletisation of the milled powder to a diameter of 30-35 mm under a pressure of 0.5-1 ton; e) annealing under inert atmosphere at a temperature of 700-900° C. for a period of 2-12 hrs; and f) grinding the resultant annealed composite powder to a fine powder. Resultant powder has shown excellent electrochemical properties in terms of charge-discharge, cyclic-stability and rate capability.

Abstract: The method of producing lithium titanate anode material for lithium ion battery applications is comprising of: a) mixing of mixed phase having 60-80% anatase and 20-40% rutile of TiO2 as titanium precursor with Li2CO3 as lithium precursor in a stoichiometric ratio of 5:4 and adding with 2 to 5% stearic acid as process control agent as well as carbon precursor; b) milling in horizontal attrition milling unit maintained with the ball to powder ratio of 10:1-12:1 at 250-500 rpm for 0.5 to 2 hrs c) repeating the milling for 40 to 48 times; d) palletisation of the milled powder to a diameter of 30-35 mm under a pressure of 0.5-1 ton; e) annealing under inert atmosphere at a temperature of 700-900° C. for a period of 2-12 hrs; and f) grinding the resultant annealed composite powder to a fine powder. Resultant powder has shown excellent electrochemical properties in terms of charge-discharge, cyclic-stability and rate capability.

Abstract: A process for forming coatings on metallic web, the process including: immersing at least three metallic webs in an electrolytic solution contained in a reaction chamber; passing wave multiphase alternating current across said metallic webs by using back-to-back thyristors connected in parallel; moving the metallic webs through the electrolytic solution; and removing the coated webs from the reaction chamber.

Abstract: The present invention is a device for coating surfaces of metallic work pieces with an electrically conductive material by employing short duration high current packets of pulses in which the work piece forms the cathode and the consumable coating material forms the anode, which are connected to a generator for generating pulses by charging and discharging a bank of capacitors using a MOSFET. The invention is also a device for controlling the on and off time of a metal oxide semiconductor field effect transistor (MOSFET).

Abstract: An apparatus for continuously forming thin ceramic coatings on metal sheets, foils or wires. The apparatus has a reaction chamber, perforated nylon sheets, nylon bar guides, copper rods attached to a power supply, nylon collecting rods, and an inlet and an outlet. The reaction chamber is capable of containing an electrolytic solution. The copper rods are separately connected to the R, Y, or B phase of the power supply. Each phase is provided with two thyristors and the output of the thyristors is connected to the copper rods using current transformers. A process for continuously forming thin ceramic coatings on metal sheets, foils or wires is also provided.

Abstract: A process for forming coatings on metallic web, the process including: immersing at least three metallic webs in an electrolytic solution contained in a reaction chamber; passing wave multiphase alternating current across said metallic webs by using back-to-back thyristors connected in parallel; moving the metallic webs through the electrolytic solution; and removing the coated webs from the reaction chamber.

Abstract: The present invention is a device for coating surfaces of metallic work pieces with an electrically conductive material by employing short duration high current packets of pulses in which the work piece forms the cathode and the consumable coating material forms the anode, which are connected to a generator for generating pulses by charging and discharging a bank of capacitors using a MOSFET. The invention is also a device for controlling the on and off time of a metal oxide semiconductor field effect transistor (MOSFET).

Abstract: An apparatus for continuously forming thin ceramic coatings on metal sheets, foils or wires. The apparatus having a reaction chamber, perforated nylon sheets, nylon bar guides, copper rods attached to a power supply, nylon collecting rods, and an inlet and an outlet. The reaction chamber is capable of containing an electrolytic solution. The copper rods are separately connected to the R, Y, or B phase of the power supply. Each phase is provided with two thyristors and the output of the thyristors is connected to the copper rods using current transformers. A process for continuously forming thin ceramic coatings on metal sheets, foils or wires is also provided.

Abstract: A process for forming oxide based dense ceramic composite coatings on reactive metal and allow bodies involves suspension of at least two reactive metal or alloy bodies in a non-metallic, non-conducting, non-reactive chamber in such a way that it causes either partial or full immersion of the bodies in a continuously circulating electrolyte. Thyristor controlled, modified shaped wave multiphase alternating current power supply is applied across the bodies where in each body is connected to an electrode. Electric current supplied to the bodies is slowly increased to a particular value till the required current density is achieved and the maintained at the same level throughout the process. Visible arcing at the surface of the immersed regions of the bodies is identified when the applied electric potential crosses 60V. Electric potential is further increased gradually to compensate the increasing resistance of the coating.