Abstract: Ethylbenzene and para-xylene and/or meta-xylene are difficult to separate by distillation because they boil only 2.3 C..degree. and 3.1 C..degree. apart. Ethylbenzene can be readily separated from the xylenes by using extractive distillation in which the extractive distillation agent is a mixture of pentachlorophenol admixed with certain chlorinated and/or oxygenated organic compounds boiling higher than the xylenes. A typical mixture comprises pentachlorophenol, benzene hexachloride and 1,2,4-trichlorobenzene.
Type:
Grant
Filed:
February 23, 1981
Date of Patent:
November 10, 1981
Assignee:
International Synthetic Rubber Co., Ltd.
Abstract: Ethylbenzene and para-xylene and/or meta-xylene are difficult to separate by distillation because they boil only 2.3 C..degree. and 3.1 C..degree. apart. Ethylbenzene can be readily separated from the xylenes by using extractive distillation in which the extractive distillation agent is a mixture of oxygen-containing organic compounds boiling higher than the xylenes. The mixture typically includes phthalic anhydride and maleic anhydride with or without a solvent.
Type:
Grant
Filed:
January 12, 1981
Date of Patent:
September 29, 1981
Assignee:
International Synthetic Rubber Co., Ltd.
Abstract: A process for preparing a modified titanium chloride component for a titanium-containing Ziegler olefin polymerization catalyst comprising (1) treating an ether-free organo-magnesium compound with an oxygen-containing organic compound other than an ether, or with carbon dioxide or oxygen under anhydrous conditions and (2) reacting the product with titanium tetrachloride.
Type:
Grant
Filed:
December 13, 1977
Date of Patent:
April 22, 1980
Assignee:
The International Synthetic Rubber Co. Ltd.
Abstract: A thermoplastic elastomeric material comprising a hydrogenated copolymer of a conjugated diene characterised in that the copolymer before hydrogenation is a random copolymer of 70 to 99 mole % of at least one conjugated diene and 30 to 1 mole % of at least one vinyl aromatic compound, is of number average molecular weight of at least 100,000, and has a vinyl content of at most 40 mole % based on total monomers, and in that the copolymer is hydrogenated to an extent such that the mole percentage saturation is in the range 40 to 90%.
Type:
Grant
Filed:
September 8, 1971
Date of Patent:
January 27, 1976
Assignee:
The International Synthetic Rubber Co., Ltd.
Inventors:
John Richard Hawkins, John Michael Locke