Patents Assigned to JFE Chemical Corporation
  • Patent number: 11942641
    Abstract: Resin-adhered graphite particles are obtained by causing a modified novolac-type phenolic resin to adhere to graphite particles. At least part of surfaces of the graphite particles is coated with a carbonaceous coating by heating the resin-adhered graphite particles in a non-oxidizing atmosphere at 900 to 1,500° C. to carbonize the modified novolac-type phenolic resin. Arylene groups having hydroxy groups account for 5 to 95 mol % of arylene groups constituting the modified novolac-type phenolic resin. The obtained carbonaceous substance-coated graphite particles exhibit excellent battery properties when used as a negative electrode material for a lithium ion secondary battery.
    Type: Grant
    Filed: November 9, 2020
    Date of Patent: March 26, 2024
    Assignees: JFE Chemical Corporation, Sumitomo Bakelite Co., Ltd.
    Inventors: Ryuta Haga, Motoharu Obika, Kunihiko Eguchi, Yoshikazu Kobayashi, Masakatsu Asami
  • Patent number: 11840452
    Abstract: Provided is spherically-shaped coated graphite exhibiting excellent cycle capacity-maintaining property when used as a negative electrode material for a lithium ion secondary battery. The spherically-shaped coated graphite includes: spherically-shaped graphite in which primary particles with an equivalent spherical diameter of not more than 0.8 ?m have a volume ratio of more than 40.0% and not more than 70.0%, and primary particles with an equivalent spherical diameter of not less than 1.5 ?m and not more than 3.0 ?m have a volume ratio of not less than 3.0% and not more than 17.0%, in a particle size distribution of primary particles obtained using X-ray computed tomography; and a carbonaceous substance covering the spherically-shaped graphite, and a pore volume of pores with a pore size of 7.8 nm to 36.0 nm is not more than 0.017 cm3/g, and a mass of infiltrated dibutyl phthalate is less than 0.70 g/cm3.
    Type: Grant
    Filed: July 28, 2022
    Date of Patent: December 12, 2023
    Assignees: JFE Chemical Corporation, JFE Steel Corporation
    Inventors: Ryota Yamaji, Yasushi Madokoro, Akira Matsuzaki, Yusuke Fushiwaki, Mikito Suto
  • Patent number: 11804594
    Abstract: Provided is carbonaceous substance-coated graphite particles that exhibit excellent battery properties when used as a negative electrode material for a lithium ion secondary battery. The carbonaceous substance-coated graphite particles includes: graphite particles; and carbonaceous coatings covering at least part of surfaces of the graphite particles, and the carbonaceous substance-coated graphite particles have a specific surface area SBET determined by BET method of 4.0 to 15.0 m2/g, and a pore volume Vs of pores with a pore size of 7.8 to 36.0 nm is 0.001 to 0.026 cm3/g, and in a pore size distribution graph with the pore size being plotted on a horizontal axis and a dV/dP value obtained by differentiating the pore volume with the pore size being plotted on a vertical axis, a pore size Pmax with which the dV/dP value is maximized is 2.5 to 5.5 nm.
    Type: Grant
    Filed: July 28, 2022
    Date of Patent: October 31, 2023
    Assignees: JFE Chemical Corporation, JFE Steel Corporation
    Inventors: Mikito Suto, Yusuke Fushiwaki, Akira Matsuzaki, Ryota Yamaji, Ryuta Haga
  • Patent number: 11804593
    Abstract: Provided are carbonaceous substance-coated graphite particles that include: graphite particles; and carbonaceous coatings covering at least part of surfaces of the graphite particles, the carbonaceous substance-coated graphite particles have a maximum particle diameter of 30.0 to 90.0 ?m, a pore volume Vs of pores with a pore size of 7.8 to 36.0 nm is 0.009 to 0.164 cm3/g, and in a pore size distribution graph with the pore size being plotted on a horizontal axis and a dV/dP value obtained by differentiating the pore volume with the pore size being plotted on a vertical axis, a pore size Pmax with which the dV/dP value is maximized is 2.5 to 5.5 nm.
    Type: Grant
    Filed: July 28, 2022
    Date of Patent: October 31, 2023
    Assignees: JFE Chemical Corporation, JFE Steel Corporation
    Inventors: Mikito Suto, Yusuke Fushiwaki, Akira Matsuzaki, Ryota Yamaji, Ryuta Haga
  • Publication number: 20230290933
    Abstract: Provided are carbonaceous substance-coated graphite particles that include: graphite particles; and carbonaceous coatings covering at least part of surfaces of the graphite particles, the carbonaceous substance-coated graphite particles have a maximum particle diameter of 30.0 to 90.0 ?m, a pore volume Vs of pores with a pore size of 7.8 to 36.0 nm is 0.009 to 0.164 cm3/g, and in a pore size distribution graph with the pore size being plotted on a horizontal axis and a dV/dP value obtained by differentiating the pore volume with the pore size being plotted on a vertical axis, a pore size Pmax with which the dV/dP value is maximized is 2.5 to 5.5 nm.
    Type: Application
    Filed: July 28, 2022
    Publication date: September 14, 2023
    Applicants: JFE CHEMICAL CORPORATION, JFE STEEL CORPORATION
    Inventors: Mikito Suto, Yusuke Fushiwaki, Akira Matsuzaki, Ryota Yamaji, Ryuta Haga
  • Publication number: 20230290934
    Abstract: Provided is carbonaceous substance-coated graphite particles that exhibit excellent battery properties when used as a negative electrode material for a lithium ion secondary battery. The carbonaceous substance-coated graphite particles includes: graphite particles; and carbonaceous coatings covering at least part of surfaces of the graphite particles, and the carbonaceous substance-coated graphite particles have a specific surface area SBET determined by BET method of 4.0 to 15.0 m2/g, and a pore volume Vs of pores with a pore size of 7.8 to 36.0 nm is 0.001 to 0.026 cm3/g, and in a pore size distribution graph with the pore size being plotted on a horizontal axis and a dV/dP value obtained by differentiating the pore volume with the pore size being plotted on a vertical axis, a pore size Pmax with which the dV/dP value is maximized is 2.5 to 5.5 nm.
    Type: Application
    Filed: July 28, 2022
    Publication date: September 14, 2023
    Applicants: JFE CHEMICAL CORPORATION, JFE STEEL CORPORATION
    Inventors: Mikito Suto, Yusuke Fushiwaki, Akira Matsuzaki, Ryota Yamaji, Ryuta Haga
  • Publication number: 20230286806
    Abstract: Provided is spherically-shaped coated graphite exhibiting excellent cycle capacity-maintaining property when used as a negative electrode material for a lithium ion secondary battery. The spherically-shaped coated graphite includes: spherically-shaped graphite in which primary particles with an equivalent spherical diameter of not more than 0.8 ?m have a volume ratio of more than 40.0% and not more than 70.0%, and primary particles with an equivalent spherical diameter of not less than 1.5 ?m and not more than 3.0 ?m have a volume ratio of not less than 3.0% and not more than 17.0%, in a particle size distribution of primary particles obtained using X-ray computed tomography; and a carbonaceous substance covering the spherically-shaped graphite, and a pore volume of pores with a pore size of 7.8 nm to 36.0 nm is not more than 0.017 cm3/g, and a mass of infiltrated dibutyl phthalate is less than 0.70 g/cm3.
    Type: Application
    Filed: July 28, 2022
    Publication date: September 14, 2023
    Applicants: JFE CHEMICAL CORPORATION, JFE STEEL CORPORATION
    Inventors: Ryota Yamaji, Yasushi Madokoro, Akira Matsuzaki, Yusuke Fushiwaki, Mikito Suto
  • Publication number: 20230107067
    Abstract: Resin-adhered graphite particles are obtained by causing a modified novolac-type phenolic resin to adhere to graphite particles. At least part of surfaces of the graphite particles is coated with a carbonaceous coating by heating the resin-adhered graphite particles in a non-oxidizing atmosphere at 900 to 1,500° C. to carbonize the modified novolac-type phenolic resin. Arylene groups having hydroxy groups account for 5 to 95 mol % of arylene groups constituting the modified novolac-type phenolic resin. The obtained carbonaceous substance-coated graphite particles exhibit excellent battery properties when used as a negative electrode material for a lithium ion secondary battery.
    Type: Application
    Filed: November 9, 2020
    Publication date: April 6, 2023
    Applicants: JFE CHEMICAL CORPORATION, SUMITOMO BAKELITE CO., LTD.
    Inventors: Ryuta Haga, Motoharu Obika, Kunihiko Eguchi, Yoshikazu Kobayashi, Masakatsu Asami
  • Publication number: 20210408521
    Abstract: Resin-adhered graphite particles are obtained by causing a modified novolac-type phenolic resin to adhere to graphite particles. At least part of surfaces of the graphite particles is coated with a carbonaceous coating by heating the resin-adhered graphite particles in a non-oxidizing atmosphere at 900 to 1,500° C. to carbonize the modified novolac-type phenolic resin. Arylene groups having hydroxy groups account for 5 to 95 mol % of arylene groups constituting the modified novolac-type phenolic resin. The obtained carbonaceous substance-coated graphite particles exhibit excellent battery properties when used as a negative electrode material for a lithium ion secondary battery.
    Type: Application
    Filed: September 8, 2021
    Publication date: December 30, 2021
    Applicants: JFE CHEMICAL CORPORATION, SUMITOMO BAKELITE CO., LTD.
    Inventors: Ryuta Haga, Motoharu Obika, Kunihiko Eguchi, Yoshikazu Kobayashi, Masakatsu Asami
  • Patent number: 10930929
    Abstract: The present invention provides a Li-ion secondary cell negative-electrode material with which it is possible to adequately suppress reductive decomposition of a liquid electrolyte by an active material during charging, the Li-ion secondary cell negative-electrode material exhibiting a high discharge capacity that exceeds the theoretical capacity of graphite and exceptional initial charging efficiency and cycle characteristics. In this negative-electrode material for a Li-ion secondary cell, the surfaces of particles of SiOx (O?x<2) contain Li and at least one metallic element M selected from among Si, Al, Ti, and Zr, and have a coating of a Li-containing oxide comprising a composition in which M/Li>5 with respect to the molar ratio.
    Type: Grant
    Filed: January 6, 2017
    Date of Patent: February 23, 2021
    Assignee: JFE CHEMICAL CORPORATION
    Inventor: Tomoyuki Tahara
  • Patent number: 10906855
    Abstract: Provided are: a method for producing fluorenylidene diallylphenols represented by formula (1), the method including a reaction step for reacting fluorenones represented by formula (2) and allylphenols represented by formula (3) in the presence of an acid catalyst, excluding compounds having mercapto groups, the amount of acid catalyst being 0.001-20 mol per mol of compound represented by formula (2); and fluorenylidene diallylphenols represented by formula (4).
    Type: Grant
    Filed: October 6, 2017
    Date of Patent: February 2, 2021
    Assignee: JFE CHEMICAL CORPORATION
    Inventor: Yoshinori Kitahara
  • Patent number: 10865325
    Abstract: Provided are: a thermally curable composition which contains benzoxazine-based compounds obtained by condensing aromatic diamines, a phenol compound, and an aldehyde compound, the aromatic diamines being a mixture comprising 4,4?-oxydianiline and 3,4?-oxydianiline, the mass ratio of the 4,4?-oxydianiline to the 3,4?-oxydianiline being 50:50 to 80:20; a varnish of the thermally curable composition; and a thermally cured object.
    Type: Grant
    Filed: June 20, 2017
    Date of Patent: December 15, 2020
    Assignee: JFE CHEMICAL CORPORATION
    Inventor: Hiroaki Nakao
  • Publication number: 20200190001
    Abstract: Provided are: a method for producing fluorenylidene diallylphenols represented by formula (1), the method including a reaction step for reacting fluorenones represented by formula (2) and allylphenols represented by formula (3) in the presence of an acid catalyst, excluding compounds having mercapto groups, the amount of acid catalyst being 0.001-20 mol per mol of compound represented by formula (2); and fluorenylidene diallylphenols represented by formula (4).
    Type: Application
    Filed: October 6, 2017
    Publication date: June 18, 2020
    Applicant: JFE CHEMICAL CORPORATION
    Inventor: Yoshinori Kitahara
  • Patent number: 10604629
    Abstract: A polyamide acid composition and a polyimide composition are obtained from a tetracarboxylic acid compound containing an aromatic tetracarboxylic acid compound having a naphthalene skeleton and a diamine compound containing an aromatic diamine compound having a biphenyl skeleton.
    Type: Grant
    Filed: April 11, 2016
    Date of Patent: March 31, 2020
    Assignee: JFE CHEMICAL CORPORATION
    Inventors: Youhei Inoue, Hiroaki Mori
  • Patent number: 10538660
    Abstract: A method for producing a dicyclopentadiene-modified phenolic resin. The method including reusing a fluorine-based ion-exchange resin as a catalyst in a reaction between a phenol and a dicyclopentadiene, the fluorine-based ion-exchange resin having been used as a catalyst when a phenol and a dicyclopentadiene are allowed to react with each other to produce a first dicyclopentadiene-modified phenolic resin. In the method, the fluorine-based ion-exchange resin is washed with an organic solvent. The dicyclopentadiene-modified phenolic resin obtained by the method has a stable quality, has a high purity, and is inexpensive.
    Type: Grant
    Filed: July 28, 2016
    Date of Patent: January 21, 2020
    Assignee: JFE CHEMICAL CORPORATION
    Inventor: Kazuya Takemura
  • Publication number: 20190270907
    Abstract: Provided are: a thermally curable composition which contains benzoxazine-based compounds obtained by condensing aromatic diamines, a phenol compound, and an aldehyde compound, the aromatic diamines being a mixture comprising 4,4?-oxydianiline and 3,4?-oxydianiline, the mass ratio of the 4,4?-oxydianiline to the 3,4?-oxydianiline being 50:50 to 80:20; a varnish of the thermally curable composition; and a thermally cured object.
    Type: Application
    Filed: June 20, 2017
    Publication date: September 5, 2019
    Applicant: JFE Chemical Corporation
    Inventor: Hiroaki Nakao
  • Patent number: 10351660
    Abstract: A phenolic resin composition and an epoxy resin composition from which a cured epoxy resin having excellent heat resisting properties and a low dielectric constant can be produced. The phenolic resin composition contains a modified phenolic resin and a tetrakisphenolethane compound, the modified phenolic resin being prepared by condensation of a cyclic hydrocarbon compound having two or more unsaturated bonds and a compound having a phenolic hydroxyl group, in which the content of the tetrakisphenolethane compound is 3% to 60% by mass with respect to the total content of the modified phenolic resin and the tetrakisphenolethane compound. The epoxy resin composition is prepared by epoxidizing the phenolic resin composition. The cured epoxy resin is prepared by allowing the epoxy resin composition to react with a hardener.
    Type: Grant
    Filed: November 10, 2014
    Date of Patent: July 16, 2019
    Assignee: JFE CHEMICAL CORPORATION
    Inventor: Kazuya Takemura
  • Publication number: 20190081323
    Abstract: The present invention provides a Li-ion secondary cell negative-electrode material with which it is possible to adequately suppress reductive decomposition of a liquid electrolyte by an active material during charging, the Li-ion secondary cell negative-electrode material exhibiting a high discharge capacity that exceeds the theoretical capacity of graphite and exceptional initial charging efficiency and cycle characteristics. In this negative-electrode material for a Li-ion secondary cell, the surfaces of particles of SiOx (0?x<2) contain Li and at least one metallic element M selected from among Si, Al, Ti, and Zr, and have a coating of a Li-containing oxide comprising a composition in which M/Li>5 with respect to the molar ratio.
    Type: Application
    Filed: January 6, 2017
    Publication date: March 14, 2019
    Applicant: JFE Chemical Corporation
    Inventor: Tomoyuki Tahara
  • Patent number: 10174165
    Abstract: There is provided a polyimide composition that is useful for electronic substrate materials, retains high heat resistance and mechanical strength intrinsic to polyimides, and has a lower dielectric constant and dielectric loss tangent. A polyimide composition for use in electronic substrate materials, containing a polyimide produced by polymerization between a diamine component containing 5-(4-aminophenoxy)-3-[4-(4-aminophenoxy)phenyl]-1,1,3-trimethylindan and an acid component containing 3,3?,4,4?-biphenyltetracarboxylic acid dianhydride.
    Type: Grant
    Filed: April 20, 2015
    Date of Patent: January 8, 2019
    Assignee: JFE CHEMICAL CORPORATION
    Inventors: Youhei Inoue, Hiroaki Mori
  • Patent number: 10170752
    Abstract: A method for producing an amorphous carbon particle includes the steps of: obtaining a first crosslinked product by admixing mesophase particles with an amorphous carbon precursor and thereafter subjecting the mixture to a crosslinking treatment, or obtaining a second crosslinked product by crosslinking the amorphous carbon precursor and thereafter admixing the mesophase particles with the crosslinked precursor; and subjecting the first or second crosslinked product to an infusibilization treatment and thereafter firing the product to produce amorphous carbon particles including the mesophase particles within the particles.
    Type: Grant
    Filed: June 12, 2013
    Date of Patent: January 1, 2019
    Assignee: JFE CHEMICAL CORPORATION
    Inventors: Makiko Ijiri, Ryuta Haga, Tetsuo Shiode, Katsuhiro Nagayama