Patents Assigned to JIANGSU CHENGYANG CROP SCIENCE CO., LTD.
  • Patent number: 9227900
    Abstract: A method is for preparing 1-(4-chlorophenyl)-2-cyclopropyl-1-propanone and an intermediate thereof, where in the method for preparing a compound of formula (I), ?-alkoxy p-chlorobenzyl phosphonate (II) and cyclopropyl methyl ketone are used as raw materials, and subjected to a Homer-Wadsworth-Emmons reaction in an organic solvent in the presence of a base, so as to prepare a derivative of alkoxy propylene with the structure of formula (III); and the resulting derivative of alkoxy propylene (III) is hydrolyzed under acidic conditions to obtain 1-(4-chlorophenyl)-2-cyclopropyl-1-propanone (I).
    Type: Grant
    Filed: November 18, 2013
    Date of Patent: January 5, 2016
    Assignee: Jiangsu Chengyang Crop Science Co., Ltd.
    Inventors: Minghua Xu, Shangcheng Xu, Xiaojun Wang, Chuanhui Yu, Qin Wan, Jiabin Hu
  • Publication number: 20150299078
    Abstract: A method is for preparing 1-(4-chlorophenyl)-2-cyclopropyl-1-propanone and an intermediate thereof, where in the method for preparing a compound of formula (I), ?-alkoxy p-chlorobenzyl phosphonate (II) and cyclopropyl methyl ketone are used as raw materials, and subjected to a Homer-Wadsworth-Emmons reaction in an organic solvent in the presence of a base, so as to prepare a derivative of alkoxy propylene with the structure of formula (III); and the resulting derivative of alkoxy propylene (III) is hydrolyzed under acidic conditions to obtain 1-(4-chlorophenyl)-2-cyclopropyl-1-propanone (I).
    Type: Application
    Filed: November 18, 2013
    Publication date: October 22, 2015
    Applicant: JIANGSU CHENGYANG CROP SCIENCE CO., LTD.
    Inventors: Minghua XU, Shangcheng XU, Xiaojun WANG, Chuanhui YU, Qin WAN, Jiabin HU