Abstract: The pressure-reduced saline water treatment system combines both forward osmosis and reverse osmosis techniques for the desalination of salt water, such as seawater. A feed side of the reverse osmosis desalination unit is in fluid communication with the feed side of the forward osmosis desalination unit, such that seawater drawn through the feed side of the forward osmosis desalination unit is fed into the feed side of the reverse osmosis desalination unit. The reverse osmosis desalination unit outputs product water extracted from the seawater from a permeate side thereof. The feed side of the reverse osmosis desalination unit outputs a reject stream, which is fed to a draw side of the forward osmosis desalination unit, such that the draw side of the forward osmosis desalination unit receives the reject stream and outputs concentrated brine.

Abstract: The desalination system with mineral recovery is a system for desalinating water using spray drying, which allows for both the production of purified water and the recovery of mineral salts. The desalination system with mineral recovery is a two-stage system for zero-liquid discharge (ZLD) desalination of feed water. The feed water may be, for example, seawater, reverse osmosis (RO) brine (i.e., the waste brine from a RO process), nano-filtration (NF) reject, multistage flash (MSF) brine, or the like. The first stage receives the feed water and uses a spray drying process to produce concentrated brine and a first volume of purified water. The concentrated brine is fed to the second stage, which also uses a spray drying process to produce a second volume of purified water and a volume of recovered mineral salts.

Abstract: The fatigue cracking machine for circumferential notched tensile (CNT) specimens is a device for pre-cracking a CNT specimen prior to SCC testing. The machine uses a specimen holding cylinder attached to the shaft of a motor by a coupling, the holding cylinder being rotatably mounted in a bearing mounted in a bearing support fixed to a platform. The machine also uses a load cylinder rotatably mounted in a load bearing supported in a load fork, the load fork having a shaft adjustably mounted in a bearing support block. A dial indicator is fixed to a post rigidly mounted on the platform with the indicator's plunger bearing against the load bearing. An adjustment bolt bears against the end of the load fork shaft to displace the load bearing, applying a bending force to the specimen while it rotates, the displacement being measured by the dial indicator.

Abstract: The system and method for pretreating turbid seawater utilizes polyelectrolyte dosing, clarification through a clarifier system and centrifugation in a decanter centrifuge followed by microfiltration to treat seawater prior to its injection through a desalination plant. The system for pretreating turbid seawater includes a static mixer for mixing a polyelectrolyte with a stream of turbid seawater to produce a polyelectrolyte-treated seawater mixture. At least one clarifier tank is in fluid communication with the static mixer for receiving the polyelectrolyte-treated seawater mixture and removing a first portion of solids therefrom to produce a clarified seawater mixture. A decanter centrifuge is in fluid communication with the at least one clarifier tank for receiving the clarified seawater mixture and removing a second portion of solids therefrom to produce centrifuged seawater.

Abstract: The method of making a nanocomposite polyelectrolyte membrane is a process for forming membranes for use in hydrogen and methanol fuel cell applications, for example. A hydrophobic polymer, such as polypropylene, is blended with a nanofiller, such halloysite nanotubes (HNTs) or propylene-grafted maleic anhydride nano-layered silica (Ma-Si), to form a dry mix, which is then pelletized for extrusion in a twin-screw extruder to form a thin film nanocomposite. The thin film nanocomposite is then annealed and cold stretched at room temperature. The cold stretching is followed by stretching at a temperature ranging from approximately 110° C. to approximately 140° C. The nanocomposite is then heat set to form the nanocomposite polyelectrolyte membrane. The nanocomposite polyelectrolyte membrane may then be further plasma etched and impregnated with a sulfonated polymer, such as sulfonated melamine formaldehyde, a polycarboxylate superplasticizer or perfluorosulfonic acid.

Abstract: A thin film nanocomposite nanofiltration membrane or TFC-NF membrane includes an ultrafiltration support membrane coated with a trimesic acid coating layer. The trimesic acid coating layer is formed or self-assembled on the ultrafiltration support membrane by pouring an aqueous solution of a water soluble tertiary amine on the support membrane to form a first coating layer and then applying a solution of trimesolychloride on the first coating layer. In other words, the trimesic acid coating layer can be formed as a result of the liquid-liquid interface of the water soluble tertiary amine and the trimesolychloride. A total thickness of the TFC-NF membrane can be about 150 ?m. The thin film nanocomposite nanofiltration membrane can be free from MPD monomers.

Abstract: A method for preparing nanosized sulfide catalysts includes providing an aqueous solution having an organometallic complex, mixing the organometallic complex with a sulfiding agent, an emulsifier, and a hydrocarbon oil to prepare a water-in-oil nanoemulsion; subjecting the water-in-oil nanoemulsion to thermal decomposition and isolating a solid product from the liquid.

Abstract: The catalyst for mild-hydrocracking of residual oil includes a porous alumina support a plurality of transition metals impregnated on the alumina support. The support has a specific surface area greater than 150 m2/g, a total pore volume ranging from about 0.25 ml/g to about 1.5 ml/g, about 20% of the pores having a diameter greater than 150 nm, about 70% of the pores having a diameter ranging from about 2 nm to about 150 nm, and about 10% of the pores having a diameter less than 2 nm. The plurality of transition metals include one Group VIII element and one or more Group VI elements.

Abstract: The integrated reverse osmosis/pressure retarded osmosis system includes a first housing configured for pretreating feed brine, a second housing, a third housing configured for pretreatment of seawater, a first splitter positioned in communicating relation with the third housing, a first pump positioned in communicating relation with the first splitter, a fourth housing positioned in communicating relation with the first pump, a mixer positioned in communicating relation with the second housing and the first splitter, a first energy recovery system positioned in communicating relation with the second housing, a second energy recovery system positioned in communicating relation with the fourth housing, and a generator. The fourth housing configured for receiving pressurized seawater and producing desalinated product water by reverse osmosis. The second housing configured to receive feed brine from an oil production waste stream and decrease the salinity of the feed brine by pressure retarded osmosis.

Abstract: A hydrodemetallization (HDM) catalyst includes an alumina and carbon extrudate support having a weight ratio of about 1:1 alumina to carbon and bimodal type pore size distribution, i.e., both meso-porosity and macro-porosity. The support can be impregnated with at least one hydrogenation active metal and, optionally, at least one promoter metal from the transition metals of Groups 6, 8, 9, and 10 of the Periodic Table. The hydrogenation active metal can be, for example, Mo, W, and Fe. The promoter metal can be, for example, Co, Ni, and Fe. The catalyst may further include ethylene diamine tetra acetic acid (EDTA).

Abstract: The planchet holder for electrodeposition of materials includes a container cover configured to securely fit over the mouth of a beaker. An elongate suspension post passes through a through-hole in the cover a predetermined distance, and a holder assembly is coupled to the suspension post to be suspended within the beaker at a select height from the bottom of the beaker. A planchet receptacle extends axially from a body of the holder assembly, and a substrate recess is formed at a distal end of the planchet receptacle for selective placement of a planchet. An endcap is secured onto the planchet receptacle to securely capture the planchet, and a port in the endcap exposes one face of the planchet for electrodeposition of a material. The planchet holder holds the planchet stationary within the beaker and exposes only one face for electrodeposition and subsequent analysis, thereby reducing time and costs.

Abstract: A method for synthesis of MgH2/Ni nanocomposites includes balancing magnesium (Mg) powder in a ball milling container with helium (He) gas atmosphere; adding a plurality of nickel (Ni) milling balls to the container; introducing hydrogen (H2) gas to the container to form a MgH2 powder; milling the MgH2 powder using the Ni-balls as milling media to provide MgH2/Ni nanocomposites. The milling can be high-energy ball milling, e.g., under 50 bar of hydrogen gas atmosphere. The high-energy ball milling can be reactive ball milling (RBM). The method can be used to attach Ni to MgH2 powders to enhance the kinetics of hydrogenation/dehydrogenation of MgH2.

Abstract: The bore hole tracer injection apparatus is a mechanical device for inserting a tracer agent into a bore hole at a predetermined depth. Outer and inner cylinders have side ports, with the side ports of the cylinders misaligned to prevent fluid escape from the inner cylinder until desired. The bottom of the inner cylinder includes a filler passage. A line passes through the top of the outer cylinder and attaches to a rod across the top of the inner cylinder, above the closed top thereof. The inner cylinder is filled with a tracer agent, and the apparatus is lowered into the bore hole to the desired depth. A weight is then dropped down the line, and jars the outer cylinder down around the inner cylinder when it contacts the top of the outer cylinder. This aligns the side ports of the cylinders to allow escape of the tracer agent therefrom.

Abstract: A system for measuring glass transition temperature of a polymer can include a cell having a closed bottom and a peripheral wall extending from the bottom, a sample holder having a first supporting pin and a second supporting pin spaced apart from the first supporting pin, a loading probe in the cell for selectively contacting a polymer sample disposed on the sample holder, a temperature probe in the cell, a heater in the cell, a temperature sensor, a source of pressure, a source of gas in communication with the cell, and a data acquisition system operably connected to the loading probe, the temperature probe and the source of pressure. The first and second supporting pins and the loading probe in the cell provide a three-point flexural bending assembly for measuring bending of the polymer sample under varied conditions of temperature and pressure in the presence of a gas.

Abstract: The system for testing stress corrosion cracking (SCC) includes an autoclave having at least one heating element selectively actuated to heat the interior portion of the autoclave, the autoclave being configured for receiving a liquid and/or gas and for forming a corrosive fluid. The system also includes a circulation assembly having a flow line and a test section line. A plurality of test sections is positioned in series along the test section line and configured for receiving the corrosive fluid via the test section line once the required temperature is reached to expose the specimens directly to the corrosive fluid, the fluid flowing through a section of the flow line parallel to the test section line until the required temperature is reached. The circulation assembly includes a circulating pump, a flowmeter positioned along the flow line, and a pressure assembly mounted on the autoclave.

Abstract: The combination multi-effect distillation and multi-stage flash evaporation system integrates a multi-stage flash (MSF) evaporation system with a multi-effect distillation (MED) system such that the flashing temperature range of the MSF process is shifted upward on the temperature scale, while the MED distillation process operates in the lower temperature range. The multi-stage flash evaporation system includes a plurality of flash evaporation/condensation stages, such that the multi-stage flash evaporation system receives a volume of seawater or brine from an external source and produces distilled water. The multi-effect distillation system includes a plurality of condensation/evaporation effects, such that the multi-effect distillation system receives concentrated brine from the multi-stage flash desalination system and produces distilled water.

Abstract: The seawater surface sampling device is a buoyant device for sampling the topmost layer of water in a body of water in order to study water properties specific to depths of only about 0.5 cm. The seawater sampling device includes a buoyant housing having an open upper end, a lower wall and at least one sidewall. The lower wall has a concave contour, and an aperture is formed through the lower wall at an apex of the concave contour. A pump is mounted on an upper surface of the lower wall, within the buoyant housing, and is in fluid communication with the aperture for extracting the water sample therethrough. A sample holder is also mounted on the upper surface of the lower wall, within the buoyant housing, for removably receiving a sample collection bottle.

Abstract: A method for synthesizing nanodiamonds includes high energy ball milling of graphite powder for a period of at least 52 hours at a rotation speed of about 400 rotations per minute to produce nanodiamonds. The ball milling can occur in an inert atmosphere at ambient pressure and room temperature. The nanodiamonds can have a spherical morphology and a particle size distribution ranging from about 1 nanometer to about 10 nanometers.

Abstract: The composition for hydrogen storage is a composite of MgH2 powder and a metallic glassy Zr70Ni20Pd10 powder. Preferably, the metallic glassy Zr70Ni20Pd10 powder forms about 5 wt % of the composition for hydrogen storage. The composition for hydrogen storage is prepared by mixing MgH2 powder and Zr70Ni20Pd10 powder to form a mixture, and then performing reactive ball milling on the mixture. Preferably, the reactive ball milling is performed under 50 bar of hydrogen gas atmosphere for a period of 50 hours.

Abstract: The method of dissipating water wave energy includes using an array of vertically-extending breakwater walls for dissipating the energy of water waves in an area of interest. Each vertically-extending wall has a plurality of horizontally-extending slots formed therethrough. The areas and/or configurations of the horizontally-extending slots can be varied such that each vertically-extending wall can have a unique degree of porosity. Each vertically extending wall can be positioned in succession in front of a water-impregnable rear barrier. The slots of one vertically-extending wall can be staggered or nonaligned relative to the next vertically-extending wall in succession.