Abstract: A method for the qualitative determination of the visible levels of glycol and/or formaldehyde at significant concentrations greater than 10 ppm (10 ppm-10,000 ppm range) in a water sample, in which the sample is treated first with periodic acid, then with iodide-thiosulfate and finally with acetyl acetone to yield a yellow color without the benefit of heat. This yellow color is visible to the naked eye and proportional to the amount of contaminants ethylene glycol, propylene glycol and/or formaldehyde present in the original water sample.