Patents Assigned to M. Technique Co., Ltd.
  • Publication number: 20150246395
    Abstract: The present invention addresses the problem of providing a method for producing metal microparticles in which the particle diameter and the coefficient of variation are controlled. Using at least two kinds of fluid to be processed including a fluid which contains at least one kind of reducing agent, the fluid to be processed is mixed in a thin film fluid formed between at least two processing surfaces, at least one of which rotates relative to the other, and which are disposed facing each other and capable of approaching and separating from each other, and metalmicroparticles are separated.
    Type: Application
    Filed: October 2, 2012
    Publication date: September 3, 2015
    Applicant: M. TECHNIQUE CO., LTD.
    Inventors: Masaki Maekawa, Masakazu Enomura
  • Publication number: 20150174660
    Abstract: The present invention addresses the problem of providing a method for producing nickel microparticles in which the ratio of crystallite's diameter to the particle diameter of the nickel microparticles is controlled. At least two types of fluids to be processed are used, including a nickel compound fluid in which a nickel compound is dissolved in a solvent, and a reducing agent fluid in which a reducing agent is dissolved in a solvent. Sulfate ions are included in the nickel compound fluid, and polyol is included in the nickel compound fluid and/or the reducing agent fluid. The fluid to be processed is mixed in a thin film fluid formed between at least two processing surfaces (1, 2), at least one of which rotates relative to the other, and which are disposed facing each other and capable of approaching and separating from each other, and nickel microparticles are precipitated.
    Type: Application
    Filed: October 2, 2012
    Publication date: June 25, 2015
    Applicant: M. TECHNIQUE CO., LTD.
    Inventors: Masaki Maekawa, Masakazu Enomura
  • Publication number: 20150140474
    Abstract: The present invention provides a method for producing metal-supported carbon, which includes supporting metal microparticles on the surface of carbon black, by a liquid-phase reduction method, in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, as well as a method for producing crystals comprising fullerene molecules and fullerene nanowhisker/nanofiber nanotubes, which includes uniformly stirring and mixing a solution containing a first solvent having fullerene dissolved therein, and a second solvent in which fullerene is less soluble than in the first solvent, in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other.
    Type: Application
    Filed: January 29, 2015
    Publication date: May 21, 2015
    Applicant: M. TECHNIQUE CO., LTD.
    Inventor: Masakazu ENOMURA
  • Publication number: 20150114179
    Abstract: The problem addressed by the present invention is providing a method for producing microparticles. At least two fluids to be processed, a raw material fluid that contains a raw material and a processing fluid that contains a substance for processing the raw material are mixed in a thin film fluid formed between at least two surfaces for processing that are disposed so as to face each other, that can approach and separate from each other and at least one of which rotates relative to the other, and microparticles of the raw material that is processed are obtained. At this time, the proportion of the microparticles of the raw material which has been processed that coalesces with each other is controlled by controlling the circumferential speed of the rotation in a confluence section in which the raw material fluid and processing fluid flow together.
    Type: Application
    Filed: May 1, 2012
    Publication date: April 30, 2015
    Applicant: M. TECHNIQUE CO., LTD.
    Inventor: Masakazu Enomura
  • Publication number: 20150110709
    Abstract: A method for producing a nanoparticle to separate a diketopyrrolopyrrole pigment includes separating an ?-type diketopyrrolopyrrole pigment nanoparticle having high crystallinity by carrying out separation of the diketopyrrolopyrrole pigment and crystal type transformation to the ?-type with substantially a single step. The ?-type diketopyrrolopyrrole pigment nanoparticle is separated by mixing a diketopyrrolopyrrole pigment solution having the diketopyrrolopyrrole pigment dissolved in a solvent and an alcohol solvent containing an alcohol compound solvent in a thin film fluid formed between at least two processing surfaces 1 and 2 arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. An acidic substance is contained in at least any one of the diketopyrrolopyrrole pigment solution and the alcohol solvent at this moment.
    Type: Application
    Filed: October 21, 2014
    Publication date: April 23, 2015
    Applicant: M. Technique Co., Ltd.
    Inventor: Masakazu ENOMURA
  • Patent number: 9005567
    Abstract: A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution.
    Type: Grant
    Filed: August 26, 2011
    Date of Patent: April 14, 2015
    Assignee: M. Technique Co., Ltd.
    Inventors: Jun Kuraki, Kaeko Araki, Masaki Maekawa, Daisuke Honda, Masakazu Enomura
  • Publication number: 20150098858
    Abstract: The purpose of the present invention is to provide novel solid gold-nickel alloy nanoparticles and a production method thereof. Provided are solid gold-nickel alloy nanoparticles having a particle diameter of 500 nm or less. In particular, gold-nickel alloy nanoparticle are provided in which the concentration of nickel in the gold-nickel alloy is 2.0-92.7 wt %, and the main component is a gold-nickel alloy in which gold and nickel are in a nano-level fine mixed state. The gold-nickel alloy particles have as the main component a substitutional solid solution of gold and nickel. These gold-nickel alloy particles are optimally formed by mixing and discharging gold ions, and a substance having reducing characteristics in the thin film fluid occurring between processing surfaces which are arranged facing each other, which can move towards and away from each other, and at least one of which rotates relative to the other.
    Type: Application
    Filed: March 15, 2013
    Publication date: April 9, 2015
    Applicant: M. TECHNIQUE CO., LTD.
    Inventors: Masaki Maekawa, Kazuya Araki, Daisuke Honda, Masakazu Enomura
  • Patent number: 8992981
    Abstract: It is an object of the present invention to provide a method for producing microparticles, which can produce monodispersed microparticles, causes no clogging with a product due to self-dischargeability, requires no great pressure, and is excellent in productivity, wherein a fluid in which at least one kind of microparticle materials is dissolved is introduced between two processing surfaces arranged to be opposite to each other to be able to approach to and separate from each other, at least one of which rotates relative to the other, to be formed into a thin film fluid, and the thin film fluid is cooled or heated (warmed) to allow saturation solubility to change, thereby separating microparticles.
    Type: Grant
    Filed: September 11, 2008
    Date of Patent: March 31, 2015
    Assignee: M Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Patent number: 8980958
    Abstract: A method for producing an emulsion is provided. At least a fluid to be processed that forms continuous phase and a fluid to be processed that forms dispersed phase are mixed in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, whereby the emulsion having variation coefficient of 0.3 to 30% in a particle size distribution is obtained.
    Type: Grant
    Filed: September 11, 2008
    Date of Patent: March 17, 2015
    Assignee: M. Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Patent number: 8978702
    Abstract: A fluid processing apparatus for processing a material to be processed between processing surfaces of processing members capable of approaching to and separating from each other, so as to rotate relative to each other, introduces a first fluid between the processing surfaces, introduces a second fluid between the processing surfaces from another flow path independent of the first fluid, and mixes and stirs the first and second fluids between the processing surfaces to undergo treatment. A processing member is composed by assembling a plurality of divided components of the processing member. An opening and a flow path are formed in the space between the plurality of components. This eliminates the need to create all ring-shaped disks which are the processing member as one block, and also eliminates the need to substantially process the flow path leading to the opening, thereby making it possible to easily undergo decomposition and cleaning.
    Type: Grant
    Filed: February 21, 2011
    Date of Patent: March 17, 2015
    Assignee: M. Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Patent number: 8974986
    Abstract: A method for producing metal-supported carbon includes supporting metal microparticles on the surface of carbon black, by a liquid-phase reduction method, in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other.
    Type: Grant
    Filed: July 4, 2008
    Date of Patent: March 10, 2015
    Assignee: M. Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Publication number: 20150030760
    Abstract: The invention addresses the problem of providing a method for producing microparticles. Provided is a method for producing microparticles. For the first process, seed microparticles are separated in a thin film fluid that forms between at least two processing surfaces, which are disposed facing each other, which can approach or separate from each other and at least one of which rotates relative to the other, and the fluid comprising the separated seed microparticles is discharged as a discharge fluid. Subsequently, for the second process, the separated seed microparticles are grown in the discharged discharge fluid to obtain the intended microparticles. Uniform and homogeneous micropartcles are obtained as a result of the microparticle producing method comprising the two process.
    Type: Application
    Filed: February 29, 2012
    Publication date: January 29, 2015
    Applicant: M. TECHNIQUE CO., LTD.
    Inventor: Masakazu Enomura
  • Patent number: 8927020
    Abstract: A production method is provided for obtaining a biologically ingestible material having an intended diameter with low energy as compared with conventional methods. The method includes mixing a fluid to be processed in a dispersed phase containing a pharmacologically active substance and a fluid to be processed in a continuous phase including at least a disperse solvent, while each of the fluids is retained in an independent state, in a thin film fluid formed between two processing surfaces arranged to be opposite to each other to be able to approach to and separate from each other, at least one of which rotates relative to the other, through independent pathways corresponding to the respective phases, whereby the components contained in the fluid to be processed in a dispersed phase are formed into microparticles having a desired diameter.
    Type: Grant
    Filed: September 10, 2008
    Date of Patent: January 6, 2015
    Assignee: M Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Patent number: 8911545
    Abstract: A forced ultrathin film rotary reaction method is used to maintain a minute space of 1 mm or less between two processing surfaces capable of approaching to and separating from each other and being rotating relative to each other, and the minute space is maintained between the two processing surfaces to serve as a flow path of a fluid to be processed thereby forming a forced thin film of the processed fluid and separating the pigment material in the forced thin film.
    Type: Grant
    Filed: July 4, 2008
    Date of Patent: December 16, 2014
    Assignee: M. Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Patent number: 8889885
    Abstract: A method for producing a nanoparticle to separate a diketopyrrolopyrrole pigment includes separating an ?-type diketopyrrolopyrrole pigment nanoparticle having high crystallinity by carrying out separation of the diketopyrrolopyrrole pigment and crystal type transformation to the ?-type with substantially a single step. The ?-type diketopyrrolopyrrole pigment nanoparticle is separated by mixing a diketopyrrolopyrrole pigment solution having the diketopyrrolopyrrole pigment dissolved in a solvent and an alcohol solvent containing an alcohol compound solvent in a thin film fluid formed between at least two processing surfaces 1 and 2 arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. An acidic substance is contained in at least any one of the diketopyrrolopyrrole pigment solution and the alcohol solvent at this moment.
    Type: Grant
    Filed: February 1, 2011
    Date of Patent: November 18, 2014
    Assignee: M. Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Publication number: 20140301892
    Abstract: The present invention addresses the problem of providing a novel, solid silver-copper alloy. Provided is a solid silver-copper alloy in which the concentration of copper contained in the silver-copper alloy is 0.1-99.94 wt %, and which has, as the principal constituent thereof, a non-eutectic structure which does not contain a eutectic when the solid silver-copper alloy is at room temperature. This silver-copper alloy can be produced by mixing a fluid containing silver ions and copper ions with a fluid containing a reducing agent, and separating silver-copper alloy particles therefrom. It is preferable to mix the fluid containing the silver ions and copper ions with the fluid containing the reducing agent in a thin-film fluid formed between processing surfaces arranged so as to face one another, capable of approaching toward and separating from one another, and capable of having at least one surface rotate relative to the other.
    Type: Application
    Filed: August 16, 2012
    Publication date: October 9, 2014
    Applicant: M. TECHNIQUE CO., LTD.
    Inventors: Masaki Maekawa, Daisuke Honda, Masakazu Enomura
  • Patent number: 8841352
    Abstract: It is an object to provide a method for producing compound semiconductor particles in which monodisperse compound semiconductor particles can be prepared according to the intended object, clogging with products does not occur due to self-dischargeability, a large pressure is not necessary, and productivity is high. In producing compound semiconductor particles by separating and precipitating, in a fluid, semiconductor raw materials, the fluid is formed into a thin film fluid between two processing surfaces arranged so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, and the semiconductor raw materials are separated and precipitated in the thin film fluid.
    Type: Grant
    Filed: August 7, 2008
    Date of Patent: September 23, 2014
    Assignee: M Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Publication number: 20140221685
    Abstract: A method for producing a high-quality barium titanyl salt includes using, as the fluids to be treated, at least two kinds of fluids, namely, a barium titanium mixed solution that is obtained by dissolving both a barium compound and a titanium compound in a solvent, a compound solution that is obtained by dissolving, in a solvent, a compound capable of deposing the barium and titanium contained in the barium-titanium mixed solution into a barium titanyl salt, and if necessary, one or more other fluids; and mixing these fluids together in a thin film fluid formed at least between two treating surfaces and to form a barium titanyl salt. The treating surfaces are so arranged as to face each other in an approachable/separable state with one of the treating surfaces and being capable of turning relatively to the other.
    Type: Application
    Filed: March 27, 2012
    Publication date: August 7, 2014
    Applicant: M. TECHNIQUE CO., LTD.
    Inventor: Masakazu Enomura
  • Patent number: 8747699
    Abstract: An aqueous solution containing a polymer dispersant and a metal compound, and an aqueous solution of a reducing agent, are joined together and uniformly mixed while being subjected to reduction reaction to give metal microparticles, in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, by using a reaction apparatus of uniform stirring and mixing the above aqueous solutions.
    Type: Grant
    Filed: July 4, 2008
    Date of Patent: June 10, 2014
    Assignee: M. Technique Co., Ltd.
    Inventor: Masakazu Enomura
  • Publication number: 20140155247
    Abstract: At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
    Type: Application
    Filed: July 5, 2012
    Publication date: June 5, 2014
    Applicant: M. TECHNIQUE CO., LTD.
    Inventors: Shiho Aoyagi, Kaeko Araki, Masaki Maekawa, Jun Kuraki, Masakazu Enomura