Patents Assigned to MATERIALS RESEARCH INSTITUTE CO., LTD.
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Patent number: 11980833Abstract: An efficient simulated moving bed device and an efficient simulated moving bed process are provided. The efficient simulated moving bed device comprises an adsorption bed, a raw material feeding system, a desorbent feeding system, a circulating system, an extract system, a raffinate system, a program-controlled valve group, and an automatic control system.Type: GrantFiled: July 5, 2019Date of Patent: May 14, 2024Assignee: Inner Mongolia Yitai Coal-based New Materials Research Institute Co., Ltd.Inventors: Zhen Qian, Jingwei Wu, Juncheng Li, Jingquan Zhang, Qinge Jian, Xiaolong Zhang, Yuan Gao, Xueting Wu, Haoting Chen
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Patent number: 11926711Abstract: A thermoplastic starch (TPS)/polylactic acid (PLA)/poly(butylene adipate-co-terephthalate) (PBAT) blend modified biodegradable resin is prepared by using a chain extender, and is prepared from the following raw materials: 20-30 parts by weight of TPS; 20-30 parts by weight of PLA; 40-60 parts by weight of PBAT; and 0.5-0.9 parts by weight of a chain extender KL-E. The preparation method is a two-step method: blending the TPS with the PBAT in a twin screw for granulating; mixing TPS/PBAT mixed granules with PLA granules, and dissolving the chain extender KL-E into an ethyl acetate solution. The chain extender KL-E can be uniformly distributed in PLA and TPS/PBAT mixed granules by using a spraying method, and the remaining short-chain molecules and terminal carboxyl molecules in the mixed granules can be changed into long-chain molecules.Type: GrantFiled: October 12, 2019Date of Patent: March 12, 2024Assignee: NANJING WURUI BIODEGRADABLE NEW MATERIAL RESEARCH INSTITUTE CO., LTD.Inventor: Tingwei Wang
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Patent number: 11817552Abstract: The present disclosure discloses a method for plasma modification of sodium super ionic conductor type solid electrolyte, which comprises: dielectric barrier discharge plasma modification of sodium super ionic conductor solid electrolyte particles to obtain activated sodium super ionic conductor solid electrolyte particles; weigh the polymer and the activated sodium super ionic conductor solid electrolyte particles in a predetermined proportion, dissolve the polymer and the activated sodium super ionic conductor solid electrolyte particles in an organic solvent to obtain a mixed solution, then pour the mixed solution into a preset mold, and then dry it to remove the organic solvent and form a composite solid electrolyte film. The composite solid electrolyte film is taken out of the mold and rolled to obtain the composite solid electrolyte film after rolling treatment.Type: GrantFiled: November 24, 2022Date of Patent: November 14, 2023Assignees: KUNMING UNIVERSITY OF SCIENCE AND TECHNOLOGY, JIANGSU FENGCHI CARBON-BASED NEW MATERIALS RESEARCH INSTITUTE CO., LTD.Inventors: Feng Liang, Minjie Hou, Da Zhang, Tao Zhang, Sunzu Xiang, Wenlong Jiang, Baoqiang Xu, Bin Yang
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Patent number: 11732058Abstract: A multi-stage modified thermoplastic starch (TPS) masterbatch is obtained by four-stage modification treatment as follows: (i) 100 parts of starch with a moisture content of 15% to 30% are added to a high-speed mixer and stirred under room temperature; (ii) Heated to 50° C. to 70° C., polybutadiene (PB), plasticizer and a chemical modifier are added. The mixture is then stirred a second time; (iii) Heated to 75° C. to 95° C., tackifier, lubricant, filler and chain extender are added. The mixture is again stirred a third time. (iv) A biodegradable resin is added at this temperature, and the resulting mixture is stirred a fourth time. After the stirring is completed, the resulting mixture is incubated at this temperature for a predetermined time, and then added to a twin-screw extruder for melt extrusion. The present invention also discloses a preparation method and use.Type: GrantFiled: July 24, 2020Date of Patent: August 22, 2023Assignee: Nanjing Wurui Biodegradable New Material Research Institute Co., LTD.Inventors: Changping Chen, Yucai Shen
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Patent number: 11545661Abstract: A high-capacity and long-life negative electrode hydrogen storage material of La—Mg—Ni type for secondary rechargeable nickel-metal hydride battery and a method for preparing the same are provided in the present invention. A chemical formula of the negative electrode hydrogen storage material of La—Mg—Ni type is La1-x-yRexMgy(Ni1-a-bAlaMb)z, wherein Re is at least one of Ce, Pr, Nd, Sm, Y, and M is at least one of Ti, Cr, Mo, Nb, Ga, V, Si, Zn, Sn; 0?x?0.10, 0.3?y?0.5, 0<a?0.05, 0?b?0.02, 2.3?z<3.0. The negative electrode hydrogen storage material of La—Mg—Ni type in the present invention has excellent charge-discharge capacity and cycle life. The negative electrode hydrogen storage material of La—Mg—Ni type can be applied in both common secondary rechargeable nickel-metal hydride battery and secondary rechargeable nickel-metal hydride battery with ultra-low self-discharge and long-term storage performance.Type: GrantFiled: May 31, 2019Date of Patent: January 3, 2023Assignees: JIANGSU JITRI ADVANCED ENERGY, MATERIALS RESEARCH INSTITUTE CO., LTD.Inventors: Jianmin Wu, Shaoxiong Zhou
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Patent number: 11524282Abstract: A regeneration method for a benzene alkylation solid acid catalyst, comprising: purging the solid acid catalyst in a reactor with a gas; continuously injecting n-hexane at a feed port of the reactor and heating the n-hexane to wash the solid acid catalyst, and discharging the n-hexane entraining benzene alkylation reaction residues from a discharge port of the reactor; and stopping injecting n-hexane, cleaning off a liquid in the reactor by purging with the gas, and cooling the reactor. In the regeneration method of the present disclosure, the regeneration liquid used is n-hexane, which can increase the solubility of the residues in channels and enhance the regeneration effect. Meanwhile, permanent damage to the channel structure of the catalyst caused by carbon burning regeneration can be avoided, thereby prolonging the lifetime of the catalyst.Type: GrantFiled: June 11, 2019Date of Patent: December 13, 2022Assignee: Inner Mongolia Yitai Coal-based New Materials Research Institute Co., Ltd.Inventors: Zhen Qian, Jingwei Wu, Juncheng Li, Xiaolong Zhang, Hongcheng Cao, Yuan Gao, Xueting Wu
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Patent number: 11370732Abstract: The present disclosure provides a method of separating ?-olefin by a simulated moving bed. The method comprises using a coal-based Fischer-Tropsch synthetic oil as a raw material to obtain a target olefin having a carbon number N within a range from 9 to 18, wherein the raw material is subjected to treatment steps including pretreatment, fraction cutting, alkane-alkene separation, and isomer separation, thereby obtaining a high purity ?-olefin product. As compared to conventional rectification and extraction processes, the product obtained by the method of the present disclosure has advantages of higher purity, higher yield, lower energy consumption, and significantly reduced production cost.Type: GrantFiled: June 14, 2019Date of Patent: June 28, 2022Assignee: INNER MONGOLIA YITAI COAL-BASED NEW MATERIALS RESEARCH INSTITUTE CO., LTD.Inventors: Juncheng Li, Zhen Qian, Jingwei Wu, Xiaolong Zhang, Qinge Jian, Yuan Gao, Xueting Wu, Haoting Chen
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Patent number: 11306262Abstract: Disclosed are a pretreatment method and system for a fraction oil for the production of alkylbenzene, the method comprising: adding a fraction oil, a weak base solution and an inorganic salt solution into a reactor, and leaving same to stand and layering same after the reaction is complete; adding water and an inorganic salt solution into an oil phase for washing with water; extracting same with a polar solvent having a high boiling point, and then adsorbing same with an adsorbent to separate oxygen-containing compounds in the neutral fraction oil; sending the extraction agent containing the oxygen-containing compounds to an extraction agent recovery unit; and then sending the neutral fraction oil to an alkylation reactor for a reaction.Type: GrantFiled: June 11, 2019Date of Patent: April 19, 2022Assignee: INNER MONGOLIA YITAI COAL-BASED NEW MATERIALS RESEARCH INSTITUTE CO., LTD.Inventors: Zhen Qian, Jingwei Wu, Xiaolong Zhang, Jingquan Zhang, Juncheng Li, Qinge Jian
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Publication number: 20220041816Abstract: A thermoplastic starch (TPS)/polylactic acid (PLA)/poly(butylene adipate-co -terephthalate) (PBAT) blend modified biodegradable resin is prepared by using a chain extender, and is prepared from the following raw materials: 20-30 parts by weight of TPS; 20-30 parts by weight of PLA; 40-60 parts by weight of PBAT; and 0.5-0.9 parts by weight of a chain extender KL-E. The preparation method is a two-step method: blending the TPS with the PBAT in a twin screw for granulating; mixing TPS/PBAT mixed granules with PLA granules, and dissolving the chain extender KL-E into an ethyl acetate solution. The chain extender KL-E can be uniformly distributed in PLA and TPS/PBAT mixed granules by using a spraying method, and the remaining short-chain molecules and terminal carboxyl molecules in the mixed granules can be changed into long-chain molecules.Type: ApplicationFiled: October 12, 2019Publication date: February 10, 2022Applicant: NANJING WURUI BIODEGRADABLE NEW MATERIAL RESEARCH INSTITUTE CO., LTD.Inventor: Tingwei WANG
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Publication number: 20220008840Abstract: An efficient simulated moving bed device and an efficient simulated moving bed process are provided. The efficient simulated moving bed device comprises an adsorption bed, a raw material feeding system, a desorbent feeding system, a circulating system, an extract system, a raffinate system, a program-controlled valve group, and an automatic control system.Type: ApplicationFiled: July 5, 2019Publication date: January 13, 2022Applicant: Inner Mongolia Yitai Coal-based New Materials Research Institute Co., Ltd.Inventors: Zhen Qian, Jingwei Wu, Juncheng Li, Jingquan Zhang, Qinge Jian, Xiaolong Zhang, Yuan Gao, Xueting Wu, Haoting Chen
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Publication number: 20220002445Abstract: A multi-stage modified thermoplastic starch (TPS) masterbatch is obtained by four-stage modification treatment as follows: (i) 100 parts of starch with a moisture content of 15% to 30% are added to a high-speed mixer and stirred under room temperature; (ii) Heated to 50° C. to 70° C., polybutadiene (PB), plasticizer and a chemical modifier are added. The mixture is then stirred a second time; (iii) Heated to 75° C. to 95° C., tackifier, lubricant, filler and chain extender are added. The mixture is again stirred a third time. (iv) A biodegradable resin is added at this temperature, and the resulting mixture is stirred a fourth time. After the stirring is completed, the resulting mixture is incubated at this temperature for a predetermined time, and then added to a twin-screw extruder for melt extrusion. The present invention also discloses a preparation method and use.Type: ApplicationFiled: July 24, 2020Publication date: January 6, 2022Applicant: Nanjing Wurui Biodegradable New Material Research Institute Co., LTD.Inventors: Changping Chen, Yucai Shen
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Publication number: 20210380505Abstract: The present disclosure provides a method of separating ?-olefin by a simulated moving bed. The method comprises using a coal-based Fischer-Tropsch synthetic oil as a raw material to obtain a target olefin having a carbon number N within a range from 9 to 18, wherein the raw material is subjected to treatment steps including pretreatment, fraction cutting, alkane-alkene separation, and isomer separation, thereby obtaining a high purity ?-olefin product. As compared to conventional rectification and extraction processes, the product obtained by the method of the present disclosure has advantages of higher purity, higher yield, lower energy consumption, and significantly reduced production cost.Type: ApplicationFiled: June 14, 2019Publication date: December 9, 2021Applicant: Inner Mongolia Yitai Coal-based New Materials Research Institute Co., Ltd.Inventors: Juncheng Li, Zhen Qian, Jingwei Wu, Xiaolong Zhang, Qinge Jian, Yuan Gao, Xueting Wu, Haoting Chen
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Publication number: 20210218020Abstract: A high-capacity and long-life negative electrode hydrogen storage material of La—Mg—Ni type for secondary rechargeable nickel-metal hydride battery and a method for preparing the same are provided in the present invention. A chemical formula of the negative electrode hydrogen storage material of La—Mg—Ni type is La1-x-yRexMgy(Ni1-a-bAlaMb)z, wherein Re is at least one of Ce, Pr, Nd, Sm, Y, and M is at least one of Ti, Cr, Mo, Nb, Ga, V, Si, Zn, Sn; 0?x?0.10, 0.3?y?0.5, 0<a?0.05, 0?b?0.02, 2.3?z<3.0. The negative electrode hydrogen storage material of La—Mg—Ni type in the present invention has excellent charge-discharge capacity and cycle life. The negative electrode hydrogen storage material of La—Mg—Ni type can be applied in both common secondary rechargeable nickel-metal hydride battery and secondary rechargeable nickel-metal hydride battery with ultra-low self-discharge and long-term storage performance.Type: ApplicationFiled: May 31, 2019Publication date: July 15, 2021Applicant: Jiangsu JITRI Advanced Energy Materials Research Institute Co., Ltd.Inventors: Jianmin Wu, Shaoxiong Zhou
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Publication number: 20210170378Abstract: A regeneration method for a benzene alkylation solid acid catalyst, comprising: purging the solid acid catalyst in a reactor with a gas; continuously injecting n-hexane at a feed port of the reactor and heating the n-hexane to wash the solid acid catalyst, and discharging the n-hexane entraining benzene alkylation reaction residues from a discharge port of the reactor; and stopping injecting n-hexane, cleaning off a liquid in the reactor by purging with the gas, and cooling the reactor. In the regeneration method of the present disclosure, the regeneration liquid used is n-hexane, which can increase the solubility of the residues in channels and enhance the regeneration effect. Meanwhile, permanent damage to the channel structure of the catalyst caused by carbon burning regeneration can be avoided, thereby prolonging the lifetime of the catalyst.Type: ApplicationFiled: June 11, 2019Publication date: June 10, 2021Applicant: Inner Mongolia Yitai Coal-based New Materials Research Institute Co., Ltd.Inventors: Zhen Qian, Jingwei Wu, Juncheng Li, Xiaolong Zhang, Hongcheng Cao, Yuan Gao, Xueting Wu
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Publication number: 20210054296Abstract: Disclosed are a pretreatment method and system for a fraction oil for the production of alkylbenzene, the method comprising: adding a fraction oil, a weak base solution and an inorganic salt solution into a reactor, and leaving same to stand and layering same after the reaction is complete; adding water and an inorganic salt solution into an oil phase for washing with water; extracting same with a polar solvent having a high boiling point, and then adsorbing same with an adsorbent to separate oxygen-containing compounds in the neutral fraction oil; sending the extraction agent containing the oxygen-containing compounds to an extraction agent recovery unit; and then sending the neutral fraction oil to an alkylation reactor for a reaction.Type: ApplicationFiled: June 11, 2019Publication date: February 25, 2021Applicant: Inner Mongolia Yitai Coal-based New Materials Research Institute Co., Ltd.Inventors: Zhen Qian, Jingwei Wu, Xiaolong Zhang, Jingquan Zhang, Juncheng Li, Qinge Jian
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Publication number: 20190292343Abstract: A method of preparation of a cardo polyetherketone structural foam material, including the following steps: 1) performing a mould pressing on a cardo polyetherketone resin by a high-temperature vulcanizing machine to prepare a foaming billet; 2) placing the foaming billet in a foaming cavity of a mould-pressing machine, performing a penetration and a swelling by introducing a supercritical fluid to achieve diffusion equilibrium, forming a polymer-supercritical fluid homogeneous solution, and 3) making the polymer-supercritical fluid homogeneous solution supersaturated through a sudden release of the inner pressure of the system, thereby inducing nucleation and foaming, and finally forming a structural foam having a closed pore structure with a uniform pore size and an adjustable pore density. The production process of the present invention is clean, environmentally friendly, and has relatively high efficiency. The obtained structural foam has good mechanical properties.Type: ApplicationFiled: December 2, 2016Publication date: September 26, 2019Applicants: Changzhou Tiansheng New Materials Research Institute Co., Ltd., Chang Chun Institute of Applied Chemistry Chinese Academy of SciencesInventors: Guangyuan ZHOU, Honghua WANG, Wei LI