Patents Assigned to Melamine Chemicals, Inc.
  • Patent number: 5795507
    Abstract: Spherical porous polymer pigment beads of melamine formaldehyde resin with uniform diameter were prepared by a water-in-oil emulsion polymerization of colored methylolmelamine aqueous solution. The dyes combined with methylolmelamine to give an excellent hue stability. The pigmented melamine formaldehyde beads (PMFB) with mean size of 3-6 micron as an organic pigment showed excellent weather and heat stability, chemical resistant properties and disperability in an application medium.
    Type: Grant
    Filed: June 24, 1996
    Date of Patent: August 18, 1998
    Assignee: Melamine Chemicals, Inc.
    Inventors: George M. Crews, Ji Shen
  • Patent number: 5514797
    Abstract: A method of purifying melamine produced from urea in a high-pressure, non-catalytic, non-aqueous process is described. In the method impure melamine is heated to a temperature of from about 250.degree. to about 1000.degree. F. under a pressure from about 600 to 3000 psi in the presence of ammonia to provide melamine having a purity of 99.0% or above. The method is economical since chemical treatment and recrystallization steps are not required.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: May 7, 1996
    Assignee: Melamine Chemicals, Inc.
    Inventors: David Best, Amit Gupta
  • Patent number: 5514796
    Abstract: A high-pressure, non-catalytic process for producing melamine from urea wherein the melamine is recovered directly as a dry powder without washing or recrystallization is described. In the process, liquid melamine is fed to a cooling unit where it is quenched with a liquid medium, preferably liquid ammonia. By increasing the pressure within the cooling unit to a pressure in excess of 600 psi and preferably to 1200 to 1400 psi provides melamine having a purity in excess of 99%.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: May 7, 1996
    Assignee: Melamine Chemicals, Inc.
    Inventors: David Best, Amit Gupta
  • Patent number: 5254665
    Abstract: Ammeline-melamine-formaldehyde resins (AMFR) containing from 5-100% ammeline were synthesized by the polymerization of the sodium salt of ammeline, which must be made in advance, melamine, and formaldehyde in basic medium (pH=9.2-10.0). In this copolymerization, it is possible to make uniform random AMFR resins with any mole ratio of ammeline salt to melamine. Preferably the AMFR resin will contain from 5-10% ammeline. As an "ionomer" or a "polyelectrolyte," both the solid and solution properties of these resins (such as melting temperature, solubility, solution stability, etc.) depended directly on the mole ratio of ammeline to melamine and formaldehyde, and/or on the pH value of the medium in which the AMFR resin was present. The pH value controlled the ammeline rings/ammeline's salt groups and also the ratio of unprotonated to protonated amino groups on both the melamine and ammeline rings.
    Type: Grant
    Filed: August 24, 1992
    Date of Patent: October 19, 1993
    Assignee: Melamine Chemicals, Inc.
    Inventors: George M. Crews, Shen Ji, Charles U. Pittman, Jr., Ruicheng Ran
  • Patent number: 5139555
    Abstract: Process of furnishing slow release nitrogen to field soil comprising inserting and distributing in the soil in particulate or granular form melamine, ammeline, ammelide, cyanuric acid, mixtures thereof, their salts, and mixtures thereof.
    Type: Grant
    Filed: September 18, 1985
    Date of Patent: August 18, 1992
    Assignee: Melamine Chemicals, Inc.
    Inventor: Donald E. Freepons
  • Patent number: 5125952
    Abstract: A storage-stable dispersion providing melamine in the form of a concentrated liquid for effective use as an end product or as an ingredient for conversion into other products. The dispersion contains melamine particles finer than about 50 microns in diameter, admixed with a chemically inert suspending liquid, having a specific gravity between 0.9 and 1.3 grams per milliliter, containing between 0.03 and 0.20 percent of a chemically inert thickening agent, which interacts physically with the suspending liquid to increase viscosity to between 250 and 3000 centipoise, thereby substantially maintaining the melamine particles in a stable dispersion and preventing their settling. The dispersion composition is an effective form of melamine for accurate dispensing as an agricultural, pulp and paper, or fire-retardant ingredient. Effective thickening agents include xanthan gums, carrageenans, polyacrylamide, chemically treated cellulose, and clays.
    Type: Grant
    Filed: August 6, 1987
    Date of Patent: June 30, 1992
    Assignee: Melamine Chemicals, Inc.
    Inventors: William P. Moore, John H. Detrick
  • Patent number: 5120821
    Abstract: A process of producing melamine formaldehyde resins using crude or impure melamine is described. The process using the impure or crude melamine includes the control of the pH within the range of from about 8 to 10, and preferably 9 to 9.2 during at least the initial stages of the formaldehyde/melamine reaction. The pH control provides resins having commercially acceptable characteristics, with the cook times of the resin formation also being commercially acceptable.
    Type: Grant
    Filed: February 22, 1991
    Date of Patent: June 9, 1992
    Assignee: Melamine Chemicals, Inc.
    Inventors: George M. Crews, Shen Ji
  • Patent number: 5071682
    Abstract: The present invention is directed to a method of using non-resinous melamine to safen urea formaldehyde-wood composites and the product produced thereby. The method involves incorporation of non-resinous melamine into a urea formaldehyde-wood composite in a manner which leaves most of the melamine free to serve as a flame retardant and formaldehyde scavenger. The non-resinous melamine is incorporated into the urea formaldehyde-wood composite prior to curing the urea formaldehyde resin.
    Type: Grant
    Filed: July 28, 1989
    Date of Patent: December 10, 1991
    Assignee: Melamine Chemicals, Inc.
    Inventor: William P. Moore
  • Patent number: 5022917
    Abstract: Liquid compositions provide a source of a herbicide or other biologically active substance in combination with a particular nitrogenous chemical, preferably melamine. After application, the herbicide is characterized by enhanced efficacy as compared to the efficacy observed when applied alone.
    Type: Grant
    Filed: February 12, 1990
    Date of Patent: June 11, 1991
    Assignee: Melamine Chemicals, Inc.
    Inventor: G. Graham Allan
  • Patent number: 4969947
    Abstract: A one-step method of preparing coated particulate plant nutrients wherein a polyfunctional coupling agent is applied to a mobile mass of plant nutrient particles containing functional groups which are chemically reactive with the functional groups of the coupling agent, while simultaneously applying a second reactive material containing functional groups also reactive with the functional groups of the coupling agent, maintaining the mobile mass at a temperature between 30.degree. C. and 300.degree. C. until a strong, water-insoluble particle. The product of the one-step method is a controlled-release plant nutrient having excellent attrition resistance.
    Type: Grant
    Filed: April 12, 1988
    Date of Patent: November 13, 1990
    Assignee: Melamine Chemicals, Inc.
    Inventor: William P. Moore
  • Patent number: 4832728
    Abstract: Relates to a fertilizer product in granular form, to processes for making and using it. The granules have strength, sizes and weights suitable for mechanical dispensing and application to and into the soil. These granules combine particles of a nitrogen source of poor solubility in pH 7 water at 20.degree. C., that converts slowly to a useful form, together with a binder that holds these fine particles together.
    Type: Grant
    Filed: September 18, 1985
    Date of Patent: May 23, 1989
    Assignee: Melamine Chemicals, Inc.
    Inventors: G. Graham Allan, Donald E. Freepons, George M. Crews
  • Patent number: 4804403
    Abstract: An attrition-resistant, controlled release fertilizer comprising a water-soluble central mass containing nucleophilic reactive functional groups surrounded and chemically bonded to a base coating formed by reacting a molecular excess of a coupling agent with the nucleophilic groups of the central particles, and a water-insoluble layer, surrounding and chemically bonded with the base coating, formed by the reaction and polymerization of the excess functional groups of the coupling agent used in forming the base coating is described. A preparation method is provided.
    Type: Grant
    Filed: August 6, 1987
    Date of Patent: February 14, 1989
    Assignee: Melamine Chemicals, Inc.
    Inventor: William P. Moore
  • Patent number: 4619735
    Abstract: Degradation of paper is retarded by treating paper with melamine. Method of treating existing paper with melamine to stop or retard degradation and methods for inclusion of melamine in paper as made to provide an age resistance paper are described. Rare books, paintings and prints can be preserved or books, paintings and prints as originally formed can use melamine-treated paper to retard degradation.
    Type: Grant
    Filed: February 13, 1985
    Date of Patent: October 28, 1986
    Assignee: Melamine Chemicals, Inc.
    Inventor: Richard V. Norton
  • Patent number: 4565867
    Abstract: This high-pressure, high-temperature anhydrous process prepares melamine from urea. It is a primary object of the present invention to provide a highly energy-efficient and improved continuous process for the production of melamine from urea which utilizes a simplified process to produce and recover a high-grade (96 to 99.5% purity) melamine as a dry powder directly from liquid melamine melt. Molten urea is supplied to a reactor maintained at high temperature (700.degree. to 800.degree. F.) and high pressure (1700 to 2200 psig) whereby melamine, CO.sub.2, and NH.sub.3 are formed. The reactor effluent stream containing liquid melamine, CO.sub.2, and NH.sub.3 is transferred to a gas separator where CO.sub.2 and NH.sub.3 containing melamine are separated and cycled to a scrubber unit for scrubbing with molten urea reactant to remove the melamine before transfer of the CO.sub.2 and NH.sub.3 gases at high pressure to an adjacent urea plant for utilization in producing urea.
    Type: Grant
    Filed: January 9, 1985
    Date of Patent: January 21, 1986
    Assignee: Melamine Chemicals, Inc.
    Inventors: Roger E. Thomas, David E. Best
  • Patent number: 4560400
    Abstract: Relates to a fertilizer product in granular form, to processes for making and using it. The granules have strength, sizes and weights suitable for mechanical dispensing and application to and into the soil. These granules combine particles of a nitrogen source of poor solubility in pH 7 water at 20.degree. C., that converts slowly to a useful form, together with a binder that holds these fine particles together.
    Type: Grant
    Filed: November 17, 1983
    Date of Patent: December 24, 1985
    Assignee: Melamine Chemicals, Inc.
    Inventors: G. Graham Allan, Donald E. Freepons, George M. Crews
  • Patent number: 4559075
    Abstract: Process of furnishing slow release nitrogen to field soil comprising inserting and distributing the soil in particulate or granular form melamine, ammeline, ammelide, cyanuric acid, mixtures thereof, their salts, and mixtures thereof.
    Type: Grant
    Filed: November 17, 1983
    Date of Patent: December 17, 1985
    Assignee: Melamine Chemicals, Inc.
    Inventor: Donald E. Freepons
  • Patent number: 4554003
    Abstract: Process of furnishing slow release nitrogen to field soil comprising inserting and distributing in the soil in particulate or granular form melamine, ammeline, ammelide, cyanuric acid, mixtures thereof, their salts, and mixtures thereof.
    Type: Grant
    Filed: April 8, 1983
    Date of Patent: November 19, 1985
    Assignee: Melamine Chemicals, Inc.
    Inventor: Donald E. Freepons
  • Patent number: 4526651
    Abstract: This invention is a process for maintaining pulp viscosity while enhancing brightness during the oxygen bleaching stage or stages of pulp preparation in the manufacture of paper comprising adding an effective amount of melamine to paper pulp prior to the oxygen bleaching stage.
    Type: Grant
    Filed: September 24, 1984
    Date of Patent: July 2, 1985
    Assignee: Melamine Chemicals, Inc.
    Inventor: G. Graham Allan
  • Patent number: 4487656
    Abstract: A process for maintaining pulp viscosity while enhancing brightness during the bleaching stage or stages of pulp preparation in the manufacture of paper comprising adding an effective amount of melamine to paper pulp prior to or during the bleaching stage. One example adds melamine to one bleach stage of a chlorine bleaching sequence. One example adds melamine to one bleach stage of a chlorine bleaching sequence.
    Type: Grant
    Filed: September 30, 1983
    Date of Patent: December 11, 1984
    Assignee: Melamine Chemicals, Inc.
    Inventor: G. Graham Allan
  • Patent number: 4484980
    Abstract: A process for maintaining pulp viscosity during the bleaching stage or stages of pulp preparation in the manufacture of paper comprising adding an effective amount of caffeine or guanine prior to or during the bleaching stage. One example adds caffeine or guanine to one bleach stage of a chlorine bleaching sequence.
    Type: Grant
    Filed: September 30, 1983
    Date of Patent: November 27, 1984
    Assignee: Melamine Chemicals, Inc.
    Inventor: G. Graham Allan