Abstract: An interferometer wherein an incident beam from a radiation source hits a beam splitter at a first oblique angle of incidence and is split into a first, reflected partial beam, and a second, transmitted partial beam, that subsequently travel along separate arms of the interferometer. The first and second partial beams are respectively intercepted, reflected, and re-split to form returning beam portions and reflected and transmitted exit beam portions. A second terminal mirror and a folding mirror, which intercepts the second partial beam at a second oblique angle of incidence, are associated with the second interferometer arm and positioned orthogonal to the reference plane and on opposite sides of the exit path, so that a section of the second partial beam from the folding mirror to the terminal mirror and back to the folding mirror crosses the exit beam twice.

Abstract: An adapter for releasably securing a probe to a reaction vessel. Embodiments of the adapter include a cover plate for mating with a reaction vessel, a body portion extending from the cover plate, and a probe gripping portion secured to the body portion. A collet and at least one anvil resides within the body portion/probe gripping portion assembly. The collet has at least one split conical end that may be divided into a plurality of flexible gripping fingers, the conical end of the collet adapted to mate with the at least one anvil. An o-ring is preferably located in the body portion and surrounds a probe when the probe is passed through the adapter. Pressure from the reaction vessel exerts an axial force on the o-ring which, in turn, exerts a like force on the anvil, thereby causing the gripping fingers of the collet to exert a gripping force on the probe.

Abstract: An adapter for releasably securing a probe to a reaction vessel. Embodiments of the adapter include a cover plate for mating with a reaction vessel, a body portion extending from the cover plate, and a probe gripping portion secured to the body portion. A collet and at least one anvil resides within the body portion/probe gripping portion assembly. The collet has at least one split conical end that may be divided into a plurality of flexible gripping fingers, the conical end of the collet adapted to mate with the at least one anvil. An o-ring is preferably located in the body portion and surrounds a probe when the probe is passed through the adapter. Pressure from the reaction vessel exerts an axial force on the o-ring which, in turn, exerts a like force on the anvil, thereby causing the gripping fingers of the collet to exert a gripping force on the probe.

Abstract: A scraper for an optical surface of a device is disclosed. The scraper includes a blade having an edge that is rigid and non-deforming to withstand high shear stresses. The blade is configured to rotate about a first axis parallel to the optical surface and also configured to move in a line with respect to a second axis perpendicular to the optical surface. This allows the rigid, non-deforming blade to maintain contact with the optical surface. Furthermore, the edge is configured to move across the optical surface to remove any materials adhered to the surface. The scraper can be used to clean the optical surface of an instrument, for example.

Abstract: A scraper for an optical surface of a device is disclosed. The scraper includes a blade having an edge that is rigid and non-deforming to withstand high shear stresses. The blade is configured to rotate about a first axis parallel to the optical surface and also configured to move in a line with respect to a second axis perpendicular to the optical surface. This allows the rigid, non-deforming blade to maintain contact with the optical surface. Furthermore, the edge is configured to move across the optical surface to remove any materials adhered to the surface. The scraper can be used to clean the optical surface of an instrument, for example.

Abstract: A device and method for performing small volume liquid-liquid extraction. A slug of a liquid specimen is aspirated into a tube, such as a pipette or pipette tip. The slug of the liquid specimen is caused to contact a filament array that resides within the tube. The slug of the liquid specimen is caused to spread across and adhere to individual filaments of the filament array as it is drawn through the tube. A slug of an extracting solvent that is immiscible with the liquid specimen is subsequently aspirated into the tube and contacted with the liquid specimen-covered filaments. The extracting solvent is selected to extract a particular solute(s) from the liquid specimen. The extracting solvent within the tube may be caused to repeatedly traverse the filament array in order to enhance the extraction process. The solute-carrying extracting solvent is subsequently expelled from the tube for separation.

Abstract: In delivery of bulk liquefied gas under pressure from portable containers, the claimed invention provides a system and process for directing the evaporated vapor from one or more satellite pressure vessels through a master vessel. The gas transfer operates passively to provide for longer unattended run times for a downstream application. The master vessel serves as a trap for the incoming gas vapor, and thereby improves the overall vapor quality by re-equilibrating the vapor with the colder bulk liquid in the master vessel before delivery to the destination application.

Abstract: The invention is a device and method in a high-pressure chromatography system, such as a supercritical fluid chromatography (SFC) system, that uses a pump as a pressure source for precision pumping of a compressible fluid. The preferred exemplary embodiment comprises a pressure regulation assembly installed downstream from a compressible fluid pump but prior to combining the compressible flow with a relatively incompressible modifier flow stream. The present invention allows the replacement of an high-grade SFC pump in the compressible fluid flow stream with an inexpensive and imprecise pump. The imprecise pump becomes capable of moving the compressible fluid flow stream in a precise flow rate and pattern. The assembly dampens the damaging effects of an imprecise pump, such as large pressure oscillations caused by flow ripples and noisy pressure signals that do not meet precise SFC pumping requirements.