Abstract: Microcapsules or macrocapsules have a core composition that includes a phase changing material (PCM) encapsulated within a polymer wall with an outer shell having a siloxane tethered to an exterior surface of the polymer wall by a surfactant. The siloxane may form a crystalline or a sol-gel outer shell. Methods of making such capsules and textile fabrics and clothing incorporating such capsules include treating pre-formed capsules with a surfactant solution followed by treating with a compound containing a siloxane functional group. The surfactant connects or tethers the siloxane to the exterior surface of the polymer wall and the siloxane forms an outer shell of the capsules.
Abstract: Methods for producing microcapsules begin by preparing an emulsion of a surfactant, core material, and water, followed by the addition of a crosslinking agent and a melamine formaldehyde prepolymer, which is subsequently polymerized. The crosslinking agent is added before the melamine formaldehyde prepolymer, with a first addition or a second addition of a melamine formaldehyde prepolymer, or is divided for addition with both a first addition and a second addition of melamine formaldehyde prepolymer.
Type:
Grant
Filed:
August 18, 2016
Date of Patent:
June 26, 2018
Assignee:
Microtek Laboratories, INC
Inventors:
Carl M. Lentz, David R. Virgallito, Jerry K. Lawson
Abstract: The present invention relates to microencapsulated compositions of isothiazolone derivatives and other water insoluble biocides or antifouling agents. In particular, the present invention relates to microencapsulated 4,5 dichloro 2 n-octyl-3(2H)-isothiazolone (DCOIT), useful in marine antifouling coatings and paints.
Type:
Grant
Filed:
April 1, 2009
Date of Patent:
May 10, 2011
Assignee:
Microtek Laboratories Inc.
Inventors:
Ronald Lee Hart, David Russell Virgallito, Dale Ellis Work
Abstract: A flame-resistant microcapsule that comprises a core comprising a phase change material and a wall material encapsulating the core. The microcapsules includes at least one of: a flame retardant applied to the wall material and a phase change material having a boiling point of about 230° C. to about 420° C. to provided enhanced flame resistance. The phase change material may have a boiling point of about 280° C. to about 400° C. or about 300° C. to about 390° C.
Type:
Application
Filed:
October 8, 2009
Publication date:
April 8, 2010
Applicant:
MICROTEK LABORATORIES, INC.
Inventors:
Danny Allen Davis, Dale Ellis Work, Timothy James Riazzi
Abstract: The present invention relates to microencapsulated compositions of isothiazolone derivatives and other water insoluble biocides or antifouling agents. In particular, the present invention relates to microencapsulated 4,5 dichloro 2 n-octyl-3(2H)-isothiazolone(DCOIT), useful in marine antifouling coatings and paints.
Type:
Grant
Filed:
September 14, 2005
Date of Patent:
June 23, 2009
Assignee:
Microtek Laboratories, Inc.
Inventors:
Ronald Lee Hart, David Russell Virgallito, Dale Ellis Work
Abstract: The present invention is directed to a method for producing macrocapsules containing therein a plurality of microcapsules. In accordance with some embodiments of the present invention, the microcapsules contain a phase change material.
Type:
Grant
Filed:
March 8, 2004
Date of Patent:
December 28, 2004
Assignee:
Microtek Laboratories, Inc.
Inventors:
Danny Allen Davis, Ronald Lee Hart, Dale Ellis Work, David Russell Virgallito
Abstract: The present invention is directed to thermal energy storage compositions comprising macrocapsules containing therein a plurality of microcapsules and to methods for producing macrocapsules containing microcapsules. In accordance with some embodiments of the present invention, the microcapsules contain a phase change material.
Type:
Grant
Filed:
September 27, 2001
Date of Patent:
March 9, 2004
Assignee:
Microtek Laboratories, Inc.
Inventors:
Danny Allen Davis, Ronald Lee Hart, Dale Ellis Work, David Russell Virgallito
Abstract: A method for microencapsulating a water-soluble or water-dispersible or water-sensitive material comprising dispersing the water-soluble or water-dispersible or water-sensitive material in an organic continuous phase and adding a polyfunctional isocyanate, a diol or polyol in the presence of an optional polymerization catalyst to the organic continuous phase is described.
Type:
Grant
Filed:
June 18, 1997
Date of Patent:
June 15, 1999
Assignee:
Microtek Laboratories, Inc.
Inventors:
Dale E. Work, Ronald L. Hart, David R. Virgallito
Abstract: A microencapsulated phase change material comprising a microcapsule wall former encapsulating a phase change material as an internal phase, said phase change material being inherently resistant or a flame retardant being admixed with said phase change material.