Abstract: A reel-to-reel aerosol collection and storage system for capturing and storing a plurality of separate samples of aerosol particles using electrostatic precipitation technology for collecting such particles onto a tape mechanism for analysis at a future time. The particles are collected onto a region of the collection tape for a defined period of time and then that portion of the collection tape is advanced out of the collection zone and manipulated so as to form sealed pouches or pockets which can be either severed from the collection tape for individual storage in a temperature controlled storage container, or which can be stored on a take-up reel in a temperature controlled environment. The collected aerosol particles are stored with a buffer fluid to preserve and maintain the viability of the collected particles for future extraction and analysis. Several embodiments for forming sealed pouches or pockets and methods of storing the collected particles are disclosed.

Abstract: A compact electrostatic particulate collector for sampling contaminants has a collection chamber defined by a titanium inner surface of a wall. A potential inducer is disposed within the chamber to create a field potential between itself and the wall of the chamber. A blower is disposed to propel air to be sampled through the chamber. At least one rinse channel is disposed to wet the inner surface of the wall of the chamber substantially 100%. The rinse channel is angled to direct a rinse liquid in a spiral direction around the inner surface of the wall. Contaminants in the air being sampled are electro statically biased into the rinse liquid on the wall and rinsed out of the chamber for collection.

Abstract: A portable multi-tube air sampler device for capturing samples of trace elements in a suspected contaminated environment which includes a plurality of sample tubes for collecting sample trace elements, parallel inlet and outlet manifolds which minimize the length of the sample inlet path while utilizing short straight sample tubes, a hinged retainer bar mechanism which allows for easy removal and replacement of the various sample tubes, and a removably attachable controller unit which can be installed on the exterior portion of the carrying case for controlling the operation of the sampling protocol. Other embodiments include heated inlet manifold and sample intake paths to prevent contamination accumulation and carryover, a clean cycle option with a filter valved into the inlet flow path to enhance the purging cycle, and a mechanism for converting the present device to a desorbing auto sampler configuration. The present system likewise incorporates a purging cycle prior to each sampling cycle.

Abstract: A reel-to-reel aerosol collection and storage system for capturing and storing a plurality of separate samples of aerosol particles using electrostatic precipitation technology for collecting such particles onto a tape mechanism for analysis at a future time. The particles are collected onto a region of the collection tape for a defined period of time and then that portion of the collection tape is advanced out of the collection zone and manipulated so as to form sealed pouches or pockets which can be either severed from the collection tape for individual storage in a temperature controlled storage container, or which can be stored on a take-up reel in a temperature controlled environment. The collected aerosol particles are stored with a buffer fluid to preserve and maintain the viability of the collected particles for future extraction and analysis. Several embodiments for forming sealed pouches or pockets and methods of storing the collected particles are disclosed.

Abstract: A portable multi-tube air sampler device for capturing samples of trace elements in a suspected contaminated environment which includes a plurality of sample tubes for collecting sample trace elements, parallel inlet and outlet manifolds which minimize the length of the sample inlet path while utilizing short straight sample tubes, a hinged retainer bar mechanism which allows for easy removal and replacement of the various sample tubes, and a removably attachable controller unit which can be installed on the exterior portion of the carrying case for controlling the operation of the sampling protocol. Other embodiments include heated inlet manifold and sample intake paths to prevent contamination accumulation and carryover, a clean cycle option with a filter valved into the inlet flow path to enhance the purging cycle, and a mechanism for converting the present device to a desorbing auto sampler configuration. The present system likewise incorporates a purging cycle prior to each sampling cycle.

Abstract: A compact electrostatic particulate collector for sampling contaminants has a collection chamber defined by a titanium inner surface of a wall. A potential inducer is disposed within the chamber to create a field potential between itself and the wall of the chamber. A blower is disposed to propel air to be sampled through the chamber. At least one rinse channel is disposed to wet the inner surface of the wall of the chamber substantially 100%. The rinse channel is angled to direct a rinse liquid in a spiral direction around the inner surface of the wall. Contaminants in the air being sampled are electro statically biased into the rinse liquid on the wall and rinsed out of the chamber for collection.

Abstract: A high-efficiency filter for removing or collecting trace levels of chemical compounds includes a randomly oriented glass substrate, a primer coating and a carbon coating. The present filter is operable to sample or remove chemical compounds from the air with a high volumetric capacity while maintaining a low pressure drop across the filter substrate. A method for making the present filter includes providing a glass substrate with randomly oriented glass fibers which is treated to remove any glue or other substances; the substrate is then coated with a primer including polydimethylsiloxane; and the primed substrate is then coated with a carbonaceous compound including polydimethylsiloxane.

Abstract: An igniter assembly for a pulsed flame photometric detector having a filament comprising a resistive heating wire between about 0.08 millimeter and about 0.40 millimeter in diameter wound into a coil having an inner diameter between about 0.40 millimeter and about 3.2 millimeters. The filament has an applied protective coating of an alloy of gold and palladium. The filament is detachably connected to a cable and connector assembly that connects the filament to a source of power in the pulsed flame photometric detector.

Abstract: A system and method for tuning a pulsed-flame photometric detector including providing a carrier gas within a predetermined gas flow range to the pulsed-flame photometric detector, providing at least one combustible fuel to the pulsed-flame photometric detector, applying voltage to an igniter coil associated with the pulsed-flame photometric detector, verifying that the pulsed-flame photometric detector is pulsing above a lower predetermined frequency and above a higher predetermined frequency, adjusting the gas flow of the at least one combustible fuel to the pulsed-flame photometric detector so that at least one cycle of ignition, propagation and then termination is present, heating a container to a predetermined temperature, allowing the at least one carrier gas to flow within the container, housing a tuning compound, and monitoring a width of a sulfur emission resulting from the combustion of the tuning compound to evaluate the width of sulfur emission signal all through a controller.

Abstract: A low-power gas chromatograph is provided including an optional air sampler module, an injector, an analytical column, a pulsed-flame photometric detector, and a computer system. The gas chromatograph of the present invention is designed for portable use such that the sensitive components of the system are mounted in a way that they are at least partially insulated against shock applied to the instrument. A rugged housing is provided such that the instrument can be used during field operations without destruction of sensitive components due to dropping and the like.

Abstract: The present invention provides a biological particle analogue, or biological analogue, that simulates a chosen biological organism or compound. The biological analogue includes a first portion that is not, in and of itself, recognized by the biological detection system, and a second portion, which provides the properties necessary for recognition by the detection system, carried by the first portion. The biological analogue is constructed in such a way as to include some important characteristics of the chosen biological organism or compound, while excluding other undesirable characteristics of the chosen biological organism or compound. The present invention is useful in testing a variety of biological detection systems.

Abstract: A low-power gas chromatograph is provided including an optional air sampler module, an injector, an analytical column, a pulsed-flame photometric detector, and a computer system. The gas chromatograph of the present invention is designed for portable use such that the sensitive components of the system are mounted in a way that they are at least partially insulated against shock applied to the instrument. A rugged housing is provided such that the instrument can be used during field operations without destruction of sensitive components due to dropping and the like.

Abstract: A system and method for tuning a pulsed-flame photometric detector including providing a carrier gas within a predetermined gas flow range to the pulsed-flame photometric detector, providing at least one combustible fuel to the pulsed-flame photometric detector, applying voltage to an igniter coil associated with the pulsed-flame photometric detector, verifying that the pulsed-flame photometric detector is pulsing above a lower predetermined frequency and above a higher predetermined frequency, adjusting the gas flow of the at least one combustible fuel to the pulsed-flame photometric detector so that at least one cycle of ignition, propagation and then termination is present, heating a container to a predetermined temperature, allowing the at least one carrier gas to flow within the container, housing a tuning compound, and monitoring a width of a sulfur emission resulting from the combustion of the tuning compound to evaluate the width of sulfur emission signal all through a controller.

Abstract: An igniter assembly for a pulsed flame photometric detector having a filament comprising a resistive heating wire between about 0.08 millimeter and about 0.40 millimeter in diameter wound into a coil having an inner diameter between about 0.40 millimeter and about 3.2 millimeters. The filament has an applied protective coating of an alloy of gold and palladium. The filament is detachably connected to a cable and connector assembly that connects the filament to a source of power in the pulsed flame photometric detector.