Abstract: Disclosed is a preparation method of the lycopene intermediate 3-methyl-4,4-dialkoxy-1-butaldehyde. The preparation method comprises the following steps: (1) reacting 2-methyl-3,3-dialkoxy-1-halopropane with magnesium powder in the solvent of anhydrous tetrahydrofuran at a temperature of 45˜65° C. to generate a mixture of Grignard reagents under the protection of an inert gas; and (2) adding N,N-disubstituted carboxamide to the mixture of Grignard reagents and reacting at a temperature of 10° C.˜35° C. to obtain 3-methyl-4,4-dialkoxy-1-butaldehyde. The process route of the present invention is simple and direct, the operation is easy, the conditions are mild and the yield is good, and thus the invention has commercial value.

Abstract: Provided are a fructosylated mangiferin, a preparation method therefor and a use thereof, wherein the fructosylated mangiferin has a structural formula represented by the following formula (I), the method for preparing the fructosylated mangiferin includes adding a substance with fructosylating enzymatic activity to a transformed liquid containing mangiferin for biotransformation reaction, so as to convert the mangiferin into the fructosylated mangiferin, wherein the transformed liquid contains the mangiferin and a glycosyl donor; as well as a use of the fructosylated mangiferin in preparation of a medicament for treatment of tumor-related diseases.

Abstract: A method for preparing organic-inorganic composite materials is provided. It is a dispersion method that the inorganic phase is introduced into the polymer matrix uniformly. The core-shell structure, in which the inorganic materials are core and the organic materials are shell, is formed by first wrapping the inorganic materials with the organic materials in the same reactor. Therefore, the match between the polarity of inorganic phase and the polarity of polymer phase is increased.

Abstract: Disclosed is a method for separating butanol. The method uses hydrophobic macroporous polymer adsorbent to separate butanol in a mixed solution, and the process comprises the following steps: 1) using macroporous polymer adsorbent to adsorb butanol in a mixed solution; 2) desorbing butanol from macroporous polymer adsorbent. The method is simple; the separation time is short; the efficiency of butanol recovery is high; and the separating cost is low.

Abstract: Provided is a cleaning process of producing lactic acid. Firstly saccharification liquid is prepared through saccharated materials, then fermented with nutritive materials and lactic acid bacteria, and liquid alkali is used to adjust the pH. The fermentation broth is filtrated with porous membrane, and the lactic acid bacteria in the interception liquid are then reintroduced into the porous membrane for recycling. The permeate from porous membrane is subjected to nanofiltration to be decolored and purified. The concentrated solution from nanofiltration and the cleaning liquid from fermentation tank and its affiliated equipment are filtrated and sterilized by using ceramic membrane, and then are reintroduced into the fermentation unit for recycling. The permeate from nanofiltration is then subjected to bipolar electrodialysis system to prepare lactic acid, and the liquid alkali produced at the same time is reintroduced into the fermentation tank for recycling.

Abstract: The invention relates to a method for the determination of the pore-mouth size distribution at the surface of porous materials. (i) While the backside of the sample is purged with a gas, the sample is immersed into a liquid wetting agent. (ii) The gas pressure is gradually decreased, and the gas flowrate is monitored; or, the gas flowrate is gradually decreased, and the gas pressure is monitored. (iii) When the gas flow stops, the remaining pressure in the system corresponds to the largest pore-mouth size. (iv) The pore-mouth size distribution can be calculated through a “dry curve” and a “wet curve”, which are curves of the gas flowrate vs. pressure at the dry and wetted states of the sample. The calculation of the pore-mouth size and the pore-mouth size distribution is the same as that based on the conventional bubble point method. The measurement of the pore-mouth size of the porous materials is of great importance when they are used as the substrates for surface coatings.

Abstract: The present invention relates to a process of controlling crystal form of Alite in Portland cement clinker, wherein the said Portland cement clinker is thermally treated in order to change the crystal form of Alite in Portland cement clinker, so as to improve performance of resulting Portland cement clinker. The said process of present invention is easy and feasible.

Abstract: The present invention relates to a process of controlling crystal form of Alite in Portland cement clinker, wherein the said Portland cement clinker is thermally treated in order to change the crystal form of Alite in Portland cement clinker, so as to improve performance of resulting Portland cement clinker. The said process of present invention is easy and feasible.

Abstract: Dry dust removal method in organic chlorosilane production is provided, in which the detailed steps are as follows: delivering high-temperature flue gas (a) from fluidized bed reactor (I) into inorganic film cross-flow filter (E) to remove dust for the first time; delivering the concentrated dust gas (c) trapped by inorganic film cross-flow filter (II) into bag filter (III) to remove dust for the second time; returning the gas mixture (f) of passing through bag filter (EI) to the air intake of inorganic film cross-flow filter (II); condensing the residual clean gas (b) from the osmotic side of inorganic film in condenser (A), and then rectifying in rectifying column (B) to separate the products of chloromethane (g) and methyl chlorosilane (h) to obtain the product of methyl chlorosilane (h); returning chloromethane to fluidized bed reactor to take part in reaction; retreating the dust (e) trapped by inorganic film cross-flow filter and bag filter, and then returning it to fluidized bed reactor (I) to take par

Abstract: The invention relates to a method for the fabrication of composite palladium or palladium alloy membranes. The surface of the porous ceramic substrate is modified with pencil to create a uniform and smooth layer, and the membrane is deposited via electroless plating. The advantages of the pencil modification are a reduction of the substrate surface roughness and a repair of substrate surface defects, which leads to a great improvement in the membrane uniformity and hydrogen permeation performances. This method is facile and economic, and it is especially effective on low-cost macroporous ceramic substrate materials. Furthermore, this method generates almost no pollution and therefore is environmentally benign.

Abstract: A method for secondarily synthesizing calcium sulphoaluminate mineral in Portland cement clinker is provided. The method includes adding gypsum into raw Portland cement, calcination, then heating twice to re-form calcium sulphoaluminate mineral that has decomposed at high temperature in the clinker. This method can increase the content of calcium sulphoaluminate mineral in the clinker. As a result, the advantages of the calcium sulphoaluminate mineral in the clinker may be obtained, such as improvement of the early stage performance and long-term performance of the cement clinker and increase in the quantity of mixture in the cement.

Abstract: A method for secondarily synthesizing calcium sulphoaluminate mineral in Portland cement clinker is provided. The method includes adding gypsum into raw Portland cement, calcination, then heating twice to re-form calcium sulphoaluminate mineral that has decomposed at high temperature in the clinker. This method can increase the content of calcium sulphoaluminate mineral in the clinker. As a result, the advantages of the calcium sulphoaluminate mineral in the clinker may be obtained, such as improvement of the early stage performance and long-term performance of the cement clinker and increase in the quantity of mixture in the cement.

Abstract: A method for preparing titania or precursor thereof with a controllable structure from micropore to mesopore is provided. The method is characterized in that the alkali metal titanate as raw material is reacted for 0.5˜72 hours in the wet atmosphere with humidity of 2˜100% at temperature of 20˜250° C., then washed with water or acid, finally performed by air roasting or solvent thermal treatment. The method has advantages that the raw material is easy to be obtained, the conditions and preparation are controllable, the pore structure may be adjusted from micropore to mesopore, crystal mixing and doping are easy, reacting time is short, preparing cost is low, and the said method is suitable for large scale production and so on. The most probable aperture of titanium oxide or precursor thereof with a controllable structure from micropore to mesopore is in the range of 1˜20 nm, the pore volume thereof is in the range of 0.05˜0.4 cm3/g, and the specific surface area thereof is more than 30 m2/g.

Abstract: The present invention provides a catalytic activity accelerant. The accelerant is added to stock oil for increasing the catalyst activity, the depth of catalytic hydrogenation and the yield of catalytic hydrogenation product, degrading the reaction conditions of catalytic hydrogenation, and improving the quality of product. The catalytic activity accelerant is consisted of an alkyl succinimide derivative, an alkyl phenol and a surfactant. The amount of the alkyl succinimide derivative in the accelerant is 5-70 wt. %. The amount of the alkyl phenol in the accelerant is 2-70 wt. %. The amount of the surfactant in the accelerant is 2-70 wt. %.