Patents Assigned to National Institute of Standards of Technology
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Publication number: 20220349628Abstract: A compact, low power cryo-cooler for cryogenic systems capable of cooling gas to at least as low as 2.5 K. The cryo-cooler has a room temperature compressor followed by filtration. Within the cryostat, four counterflow heat exchangers precool the incoming high-pressure gas using the outflowing low-pressure gas. The three warmest heat exchangers are successively heat sunk to three stages of a pulse tube to absorb residual heat from the slight ineffectiveness of the heat exchangers. The pulse tube cold head also absorbs loads from instrumentation leads and radiation loads. The pulse tube stages operate at around 80 K, 25 K, and 10 K. The entire system—cryo-cooler, drive and control electronics, and detector instrumentation, fits in a standard electronics rack mount enclosure, and requires around 300 W or less of power.Type: ApplicationFiled: July 5, 2022Publication date: November 3, 2022Applicant: National Institute of Standards and Technology (NIST)Inventors: Vincent Kotsubo, Joel Ullom, Sae Woo Nam
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Patent number: 11287334Abstract: An optomechanical pressure-measurement system measures pressure in the range of 10?6 Pa-10?2 Pa by measuring various properties of a vibrational mode of an ultra-thin membrane member. With independent measurements of the thickness and density of the membrane, in addition to the measured vibration mode properties, the system can operate as a primary pressure sensor. The membrane member is mounted on a vibration-isolated mount and is excited by a drive force. A laser beam impinges on the excited membrane, and an optical phase detector detects the amplitude of the oscillations, as well as parameters of the laser beam affected by the membrane vibration. In one embodiment, a mechanical damping is computed based on the amplitude or frequency shift (depending on the pressure range), and the pressure based on the ring-down time of the membrane vibration mode.Type: GrantFiled: June 19, 2019Date of Patent: March 29, 2022Assignees: University of Maryland, College Park, Government of the USA, as represented by the Secretary of Commerce, National Institute of Standards and TechnologyInventors: Stephen Eckel, James Fedchak, Thomas Purdy, Robinjeet Singh
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Publication number: 20210364517Abstract: The invention is directed to methods and systems for early detection of viral diseases, and more specifically to systems and methods for early detection of viral diseases that are capable of detecting very low viral loads, such as for example and not limitation, SARS-CoV-2 loads.Type: ApplicationFiled: May 21, 2021Publication date: November 25, 2021Applicants: The Penn State Research Foundation, The National Institute of Standards and Technology, University of North Carolina at GreensboroInventors: Vyacheslav V. ROTKIN, Ming ZHENG, Tetyana IGNATOVA, Daniel HAYES, Suresh KUCHIPUDI
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Patent number: 11181489Abstract: Provided herein are methods and apparatus for characterizing high aspect ratio (HAR) structures of fabricated or partially fabricated semiconductor devices. The methods involve using small angle X-ray scattering (SAXS) to determine average parameters of an array of HAR structures. In some implementations, SAXS is used to analyze symmetry of HAR structures in a sample and may be referred to as tilted structural symmetry analysis-SAXS (TSSA-SAXS) or TSSA. Analysis of parameters such as tilt, sidewall angle, bowing, and the presence of multiple tilts in HAR structures may be performed.Type: GrantFiled: July 30, 2019Date of Patent: November 23, 2021Assignees: Lam Research Corporation, The Government of the United States of America, represented by the Secretary of Commerce, National Institute of Standards and TechnologyInventors: William Dean Thompson, Regis Joseph Kline, Daniel F. Sunday, Wenli Wu, Osman Sorkhabi, Jin Zhang, Xiaoshu Chen
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Patent number: 11069507Abstract: A sample carrier for in situ transmission electron microscopy (TEM) has a dielectric substrate with a conductive layer that forms a coplanar waveguide. The coplanar waveguide has a first and second leads formed by the conductive layer. The first lead is between an adjacent pair of second leads and is spaced from the second leads by a respective gap. The coplanar waveguide is configured to transmit an electrical signal to a specimen held by the sample carrier, in particular, an electrical signal having a frequency in the radio-frequency (RF) regime (3 kHz-300 GHz), for example, up to 100 GHz. The sample carrier may be mounted to a TEM sample holder, which supports the sample carrier within a vacuum chamber of the microscope and provides electrical connection between the leads of the sample carrier and an RF source external to the vacuum chamber.Type: GrantFiled: March 5, 2020Date of Patent: July 20, 2021Assignees: University of Maryland, College Park, Government of the United States of America, as represented by the Secretary of Commerce, National Institute of Standards and TechnologyInventors: Michael Katz, Karl Schliep, June Lau, Jason J. Gorman
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Patent number: 11035792Abstract: A nanohole array (NHA)-based plasmonic sensor (e.g., gas/condensed phase sensor), their preparation, and their use to detect and analyze samples, especially mixtures of chemicals/bio-chemicals.Type: GrantFiled: March 6, 2019Date of Patent: June 15, 2021Assignees: The George Washington University, GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF COMMERCE, NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventors: Yangyang Zhao, Mona Zaghloul, Stephen Semancik, Kurt D. Benkstein
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Patent number: 11018290Abstract: This disclosure describes systems, methods, and apparatus for multilayer superconducting structures comprising electroplated Rhenium, where the Rhenium operates in a superconducting regime at or above 4.2 K, or above 1.8 K where specific temperatures and times of annealing have occurred. The structure can include at least a first conductive layer applied to a substrate, where the Rhenium layer is electroplated to the first layer. A third layer formed from the same or a different conductor as the first layer can be formed atop the Rhenium layer.Type: GrantFiled: July 2, 2020Date of Patent: May 25, 2021Assignees: The Regents of the University of Colorado, a body corporate, The Government of the United States of America, as represented by the Secretary of Commerce National Institute of Standards and TechnologyInventors: Donald David, David Pappas, Xian Wu
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Patent number: 10999109Abstract: Systems, methods, and apparatuses, for transform discrete voltage pulses to a continuous signal. One method may include receiving a pulsed-voltage signal. The method may also include alternately directing the pulsed-voltage signal between a pair of processing channels based on a modulation signal or another signal. The method may further include determining rate voltages corresponding to the pair of processing channels based on a pulse rate of the pulsed-voltage signal. Further, the method may include processing the rate voltages using low pass filters corresponding to the pair of processing channels to form filtered rate voltages. The method may also include determining a normalized differential output for the pair of processing channels based on the filtered rate voltages. The method may also include outputting the normalized differential output to an output connector.Type: GrantFiled: July 23, 2019Date of Patent: May 4, 2021Assignees: UNIVERSITY OF MARYLAND, COLLEGE PARK, NATIONAL INSTITUTE OF STANDARDS & TECHNOLOGYInventors: Kapildeb Ambal, Robert D. McMichael
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Patent number: 10858256Abstract: A method of separating and extracting carbon nanotubes, the method includes introducing the carbon nanotubes into a two-phase system that includes a first component and a second component, the first component being different from the second component. The method includes introducing a chemical agent into the two-phase system, mixing the chemical agent and the carbon nanotubes in the two-phase system, removing the first component to extract a first portion of the carbon nanotubes contained in the first component after the mixing, replenishing the two-phase system with fresh first component, and extracting a second portion of the carbon nanotubes contained in the fresh first component. A bandgap of the carbon nanotubes in the first portion is different from the bandgap of the carbon nanotubes in the second portion.Type: GrantFiled: January 22, 2016Date of Patent: December 8, 2020Assignees: University of Southern California, Government of the United States of America, as Represented by the Secretary of Commerce, National Institute of Standards and TechnologyInventors: Hui Gui, Jason K. Streit, Angela R. Hight Walker, Chongwu Zhou, Ming Zheng
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Patent number: 10741742Abstract: This disclosure describes systems, methods, and apparatus for multilayer superconducting structures comprising electroplated Rhenium, where the Rhenium operates in a superconducting regime at or above 4.2 K, or above 1.8 K where specific temperatures and times of annealing have occurred. The structure can include at least a first conductive layer applied to a substrate, where the Rhenium layer is electroplated to the first layer. A third layer formed from the same or a different conductor as the first layer can be formed atop the Rhenium layer.Type: GrantFiled: February 28, 2019Date of Patent: August 11, 2020Assignees: THE REGENTS OF THE UNIVERSITY OF COLORADO, A BODY CORPORATE, GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF COMMERCE, NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventors: Donald David, David Pappas, Xian Wu
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Patent number: 10599007Abstract: Various embodiments of the present technology provide a novel architecture for optical frequency conversion in a waveguide which can be applied to any suitable nonlinear waveguide material and any wavelength. In accordance with some embodiments, phase-matched bends can be used to increase the nonlinear interaction length. For example, the device can begin with a straight waveguide section with a width designed for phase-matching. When the straight waveguide section approaches the end of the chip, a bending waveguide section allows the waveguide to meander back in the opposite direction. Various embodiments of the bend can have a wider or narrower width to eliminate phase-matching for second harmonic generation (SHG) and instead provide a 2? phase-shift between the pump and signal light. Therefore, at the end of the bend, the pump and signal light are in-phase and a phase-matched width will continue the SHG process.Type: GrantFiled: July 17, 2019Date of Patent: March 24, 2020Assignees: The Regents of the University of Colorado, a body corporate, Government of the United States of America, as represented by the Secretary of Commerce National Institute of Standards and TechnologyInventors: Eric Stanton, Jeffrey Chiles
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Publication number: 20190363250Abstract: A method of switching a phase-change device (Device), including changing phase of the Device from a semiconducting 2H phase to a new 2Hd phase with a higher conductivity, the Device having an active material with a thickness including a phase transition material to thereby transition the Device from a high resistive state (HRS) to a low resistive state (LRS) by application of a set voltage and further to return the Device from the LRS back to the HRS by application of a reset voltage.Type: ApplicationFiled: August 23, 2018Publication date: November 28, 2019Applicants: Purdue Research Foundation, National Institute of Standards and TechnologyInventors: Joerg Appenzeller, Feng Zhang, Yuqi Zhu, Albert V. Davydov, Sergiy Krylyuk, Huairuo Zhang, Leonid A. Bendersky
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Patent number: 10444431Abstract: A reticulated resonator includes: a reticulated substrate that includes: a substrate frame; and a phononic structure in mechanical communication with the substrate frame and including a plurality of unit members arranged in a two-dimensional array; and a membrane disposed on the reticulated substrate.Type: GrantFiled: January 14, 2016Date of Patent: October 15, 2019Assignee: NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventors: Raymond W. Simmonds, Katarina Cicak, Cindy A. Regal, Pen-Li Yu, Yeghishe Tsaturyan, Thomas P. Purdy, Nir S. Kampel
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Publication number: 20190226724Abstract: A compact, low power cryo-cooler for cryogenic systems capable of cooling gas to at least as low as 2.5 K. The cryo-cooler has a room temperature compressor followed by filtration. Within the cryostat, four counterflow heat exchangers precool the incoming high-pressure gas using the outflowing low-pressure gas. The three warmest heat exchangers are successively heat sunk to three stages of a pulse tube to absorb residual heat from the slight ineffectiveness of the heat exchangers. The pulse tube cold head also absorbs loads from instrumentation leads and radiation loads. The pulse tube stages operate at around 80 K, 25 K, and 10 K. The entire system—cryo-cooler, drive and control electronics, and detector instrumentation, fits in a standard electronics rack mount enclosure, and requires around 300 W or less of power.Type: ApplicationFiled: January 24, 2019Publication date: July 25, 2019Applicant: National Institute of Standards and Technology (NIST)Inventors: Vincent Kotsubo, Joel Ullom, Sae Woo Nam
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Patent number: 10261032Abstract: A noncontact resonameter includes: a resonator to: produce an excitation signal including a field; subject a sample to the excitation signal; produce a first resonator signal in a presence of the sample and the excitation signal, the first resonator signal including: a first quality factor of the resonator; a first resonance frequency of the resonator; or a combination thereof, the first resonator signal occurring in an absence of contact between the sample and the resonator; and produce a second resonator signal in a presence of the excitation signal and an absence of the sample, the second resonator signal including: a second quality factor of the resonator; a second resonance frequency of the resonator; or a combination thereof; a circuit in electrical communication with the resonator to receive the first resonator signal and the second resonator signal; and a continuous feeder to: provide the sample proximate to the resonator; dispose the sample intermediately in the field of the excitation signal duringType: GrantFiled: December 3, 2015Date of Patent: April 16, 2019Assignee: NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventors: Nathan Daniel Orloff, Christian John Long, Jan Obrzut
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Patent number: 10247814Abstract: A phase shift detector includes: an interferometer; and a microwave probe in electrical communication with the interferometer, the microwave probe including: a primary shield electrode; and a transmission electrode disposed proximate to the primary shield electrode, the transmission electrode and the primary shield electrode being exposed and arranged to produce an electric field, wherein the transmission electrode is isolated electrically from the primary shield electrode.Type: GrantFiled: January 14, 2016Date of Patent: April 2, 2019Assignee: NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventors: Kin P. Cheung, Jason T. Ryan, Jason Campbell
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Patent number: 10174981Abstract: A system to make ice includes a refrigeration unit and an icemaker disposed in the refrigeration unit. The refrigeration unit is configured to be subjected to a refrigeration cycle; the icemaker is configured to be subjected to a freeze cycle; and the system is configured such that the freeze cycle is synchronized with the refrigeration cycle, asynchronized with the refrigeration cycle, or a combination comprising at least one of the foregoing. A process for controlling an icemaker includes providing a freeze cycle to an icemaker; providing a refrigeration cycle to a refrigeration unit; and constraining the freeze cycle and the refrigeration cycle to control the icemaker.Type: GrantFiled: September 25, 2014Date of Patent: January 8, 2019Assignee: NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventor: David Yashar
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Patent number: 10082553Abstract: A magnetic resonance imaging (MRI) phantom includes an outer container that includes a first portion comprising a first wall; a second portion opposingly disposed to the first portion and sealingly engaged to the first portion, the second portion including a second wall; and an internal volume bounded by the first wall and the second wall, the internal volume being hollow and configured to receive a fluid; and a sample holder disposed in the internal volume of the outer container, wherein the MRI phantom is configured to maintain a constant temperature of the internal volume. A process for acquiring an MRI image includes providing an MRI; disposing a sample member in the sample holder; disposing a fluid in the MRI phantom; disposing the MRI phantom in an MRI device; achieving thermal equilibrium in the MRI phantom at a selected temperature; and subjecting the MRI phantom to MRI imaging at the selected temperature to acquire the MRI image of the sample.Type: GrantFiled: July 17, 2015Date of Patent: September 25, 2018Assignee: NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventor: Michael A. Boss
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Patent number: 10078898Abstract: Disclosed is a noncontact metrology probe including: a first camera including a first field of view; a second camera including a second field of view and arranged such that the second field of view overlaps the first field of view to form a prime focal volume; a third camera including a third field of view and arranged such that the third field of view overlaps the prime focal volume to form a probe focal volume; and a tracker including a tracker field of view to determine a location of the probe focal volume in the tracker field of view.Type: GrantFiled: November 3, 2015Date of Patent: September 18, 2018Assignee: NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGYInventor: Joshua Gordon
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Patent number: 10067088Abstract: Gradient elution isotachophoretic apparatus, and systems for performing gradient elution isotachophoresis to separate, purify, concentrate, quantify, and/or extract charged analytes from a sample. The isotachophoretic apparatus include an electrophoretic assembly, a sampling assembly connected to the electrophoretic assembly, and/or a support structure connected to the electrophoretic assembly and/or to the sampling assembly. The system includes an isotachophoretic apparatus, and a controller communicatively coupled to the isotachophoretic apparatus. The controller includes a storage medium and a processor for executing computer readable and executable instructions.Type: GrantFiled: June 22, 2015Date of Patent: September 4, 2018Assignees: Applied Research Associates, Inc., The United States of America, as Represented by the Secretary of Commerce National Institute of Standards and TechnologyInventors: Alyssa Henry, Christopher Konek, David Ross, Elizabeth Strychalski