Patents Assigned to Nippon Soda Co., Ltd.
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Publication number: 20170267810Abstract: It is to provide a more stable crystal polymorph of a clathrate compound consisting of 1,1,2,2-tetrakis(4-hydroxyphenyl)ethane and 2-phenyl-4-methyl-5-hydroxymethylimidazole (molar ratio 1:2). A novel crystal polymorph of a clathrate compound, consisting of 1,1,2,2-tetrakis(4-hydroxyphenyl)ethane and 2-phenyl-4-methyl-5-hydroxymethylimidazole (molar ratio 1:2) and has diffraction peaks at diffraction angles (2?) of 11.20°, 13.36°, 14.36°, 18.16°, 19.20°, 19.68°, 20.84°, 21.48°, 22.56°, 23.76° and 24.08° in a powder X-ray diffraction pattern as measured using a CuK? ray, can be obtained by, for example, further recrystallizing a crystal obtained by a conventionally known method or the like.Type: ApplicationFiled: August 27, 2015Publication date: September 21, 2017Applicant: NIPPON SODA CO., LTD.Inventor: Kazuo ONO
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Patent number: 9758468Abstract: The present invention provides a halogenated aniline represented by formula (I) (wherein each of X1 and X2 independently represents a chlorine atom, a bromine atom or an iodine atom), a method for producing the halogenated aniline, and other aspects.Type: GrantFiled: October 14, 2016Date of Patent: September 12, 2017Assignee: Nippon Soda Co., Ltd.Inventors: Hiroki Inoue, Yuzuru Sakata, Shinichi Kobayashi, Yoshikazu Ito, Takashi Kitayama
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Publication number: 20170251648Abstract: An object of the invention is to provide a fishhook for fishing or the like, the fishhook being easily stuck to a fish or the like and being also excellent in durability. The surface of a fishhook is treated with a compound selected from the group consisting of a metallic surfactant having at least one or more hydroxyl groups or hydrolyzable groups, a fluorine-based surface treating agent, a thiol compound and a disulfide compound.Type: ApplicationFiled: August 28, 2015Publication date: September 7, 2017Applicants: NIPPON SODA CO., LTD., GLOBERIDE, IncInventors: Tomoya HIDAKA, Tokuo ICHIKAWA, Yukio OKISHIMA, Yasuhisa SHIBATA
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Publication number: 20170226046Abstract: The present invention provides a method for producing a benzaldehyde in which an amino group is bonded in the 2 position, a halogeno group or an alkoxy group is bonded in the 3 position, and a hydrogen atom, an alkyl group, a halogeno group, an alkoxy group, or a cyano group is bonded independently in each of the 4, 5, and 6 positions, the method including: preparing a benzaldehyde in which a halogeno group or an alkoxy group is bonded in the 3 position, a hydrogen atom is bonded in the 2 position, and a hydrogen atom, an alkyl group, a halogeno group, an alkoxy group, or a cyano group is bonded independently in each of the 4, 5, and 6 positions so that a lithiation reaction is most active at the 2 position; acetal-protecting a formyl group in the benzaldehyde; sequentially performing lithiation, azidation, and amination of the 2 position; and the performing acetal deportection.Type: ApplicationFiled: August 25, 2015Publication date: August 10, 2017Applicant: Nippon Soda Co., Ltd.Inventor: Shinichi KOBAYASHI
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Publication number: 20170223958Abstract: The present invention provides a compound represented by formula (I) or salt thereof (in the formula, A1 and A2 each independently represents a nitrogen atom or the like, B1, B2, B3 and B4 each independently represents a carbon atom or nitrogen atom, X1 represents an unsubstituted or substituted C1-6 alkyl group or the like, n represents a number of X1 and represents an integer of 0-4, R1 represents a halogeno group or the like, R2 represents an unsubstituted or substituted C1-6 alkyl group or the like, m represents a number of the oxide group bonding with the nitrogen atom which does not bond with R2 on the imidazole ring, and represents 0 or 1, R3 represents a hydrogen atom or the like, Ar represents an unsubstituted or substituted C6-10 aryl group.Type: ApplicationFiled: August 11, 2015Publication date: August 10, 2017Applicant: Nippon Soda Co., Ltd.Inventors: Hikaru AOYAMA, Maki MATSUI, Takao IWASA, Kazushige FUJII, Tomomi KOBAYASHI, Keita SAKANISHI
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Publication number: 20170209905Abstract: A method for cleaning a storage tank to which sodium metal is adherent, the method containing: filling, with an inert oil, the storage tank to which sodium metal is adherent; subsequently adding water, water vapor, or a humidified inert gas to the inert oil; providing a gas discharge line to the storage tank and measuring the hydrogen gas concentration in the gas discharge line; regulating the amount of the water, water vapor, or humidified inert gas to be added per hour in accordance with the level of the hydrogen gas concentration; regulating the temperature of the inert oil to 0-98° C.; and converting the sodium metal into caustic soda while changing the liquid surface level of the inert oil in parallel with addition of the water, water vapor, or humidified inert gas to the inert oil.Type: ApplicationFiled: May 29, 2015Publication date: July 27, 2017Applicant: Nippon Soda Co., Ltd.Inventors: Hideaki ITO, Toru ARAKAWA, Takahiro AIBA
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Patent number: 9701780Abstract: A polybutadiene having a hydroxyl group at a terminal end thereof is reacted with a lactone compound such as an ?-caprolactone to obtain a polymer polyol represented by formula (I): HO—X1—Y—X2—OH (wherein X1 and X2 each independently represents a polyester component and Y represents a polybutadiene component), the polymer polyol is reacted with an unsymmetric diisocyanate to obtain a urethane prepolymer, and then the urethane prepolymer is reacted with a chain extender to obtain a polyurethane.Type: GrantFiled: February 24, 2016Date of Patent: July 11, 2017Assignee: NIPPON SODA CO., LTD.Inventors: Akihiro Shirai, Yasunori Miyashita, Shinichi Kimizuka, Mitsuhiro Nakamura
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Patent number: 9701779Abstract: A polybutadiene having a hydroxyl group at a terminal end thereof is reacted with a lactone compound such as an ?-caprolactone to obtain a polymer polyol represented by formula (I): HO—X1—Y—X2—OH (wherein X1 and X2 each independently represents a polyester component and Y represents a polybutadiene component), the polymer polyol is reacted with an unsymmetric diisocyanate to obtain a urethane prepolymer, and then the urethane prepolymer is reacted with a chain extender to obtain a polyurethane.Type: GrantFiled: May 23, 2013Date of Patent: July 11, 2017Assignee: NIPPON SODA CO., LTD.Inventors: Akihiro Shirai, Yasunori Miyashita, Shinichi Kimizuka, Mitsuhiro Nakamura
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Patent number: 9693562Abstract: A liquid insecticide composition is provided containing a neonicotinoid-based compound, a silicone-based surfactant, and a water-soluble organic solvent. Furthermore, a method is provided for enhancing an insecticidal effect which includes using a silicone-based surfactant in combination with a neonicotinoid-based compound as an insecticidal active ingredient.Type: GrantFiled: May 8, 2012Date of Patent: July 4, 2017Assignee: Nippon Soda Co., Ltd.Inventors: Kaoru Nishimura, Rieko Nakamura, Rie Sakamoto
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Patent number: 9686993Abstract: The present invention provides a method for prominently inhibiting the production in fungi of mycotoxin, which has serious effects on health of humans and other animals, and provides a mycotoxin production inhibitor. Mycotoxin content such as deoxinivalenol (DON) in harvested crops can be reduced without a correlation with the control effects against fungi by spraying a fungicide containing a benzimidazole-type fungicidal compound such as thiophanate-methyl as an active ingredient onto food crops such as wheat, barley, and the like. Concomitant use of the benzimidazole-type fungicidal compound and a sterol biosynthesis inhibitor (SBI agent) such as tebuconazole can further enhance the effect.Type: GrantFiled: March 29, 2006Date of Patent: June 27, 2017Assignee: Nippon Soda Co., Ltd.Inventor: Herbert Buschhaus
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Publication number: 20170137564Abstract: A method includes mixing a clathrate compound with an epoxy resin to form a curable epoxy resin composition, and may further include heating the curable epoxy resin composition to cure the curable epoxy resin composition. The clathrate compound includes (a1) a carboxylic acid compound represented by the formula A(COOH)k; and (a2) a xylylene diamine compound. In the formula A(COOH)k, A represents a C1-C6 linear hydrocarbon group optionally having a substituent, a C3-C10 monocyclic hydrocarbon group optionally having a substituent, or a C6-C10 bicyclic hydrocarbon group optionally having a substituent; and k represents 2 or 3.Type: ApplicationFiled: January 31, 2017Publication date: May 18, 2017Applicant: NIPPON SODA CO., LTD.Inventors: Kazuo ONO, Tomoya NOMURA
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Patent number: 9650250Abstract: The present invention provides an industrially advantageous method for producing bis(halosulfonyl)amine that makes it possible to inhibit the rapid generation of gas and reduce the amount of halogenating agent used by controlling the reaction rate among sulfamic acid, the halogenating agent and a halosulfonic acid to nearly a constant rate from the initial stage to the final stage of the reaction. The method for producing bis(halosulfonyl)amine of the present invention allows the obtaining of a bis(halosulfonyl)amine such as N-(fluorosulfonyl)-N-(chlorosulfonyl)amine or bis(chlorosulfonyl)amine by a production method that includes heating a mixture containing sulfamic acid and a halosulfonic acid to a temperature higher than room temperature, adding a halogenating agent thereto, and allowing to react while adjusting to a prescribed temperature.Type: GrantFiled: July 24, 2013Date of Patent: May 16, 2017Assignee: NIPPON SODA CO., LTD.Inventor: Michiaki Maruyama
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Patent number: 9648879Abstract: A co-crystal composed of a diamide-based insecticidal-active ingredient and a neonicotinoid-based insecticidal-active ingredient is provided as a co-crystal which exhibits excellent insecticidal effects over a long period of time while reducing the occurrence of chemical damage on useful plants. The co-crystal is obtained by a method including heating and stirring of a suspension obtained by suspending the diamide-based insecticidal-active ingredient and the neonicotinoid-based insecticidal-active ingredient in a solvent such as water.Type: GrantFiled: October 31, 2014Date of Patent: May 16, 2017Assignee: Nippon Soda Co., Ltd.Inventors: Akihiko Ito, Tomohiro Amano, Rieko Masaki
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Publication number: 20170128926Abstract: A method for producing a photocatalyst-carrying structure includes coating a carrier with a composition for forming an adhesive layer, followed by drying, to form the adhesive layer; and coating the adhesive layer with a composition for forming a photocatalyst layer. The composition for forming the adhesive layer is formed by mixing an aqueous silicone-modified resin, 2% by weight to 15% by weight of a deposition assistant, 10% by weight to 40% by weight of an organic solvent, and water. The aqueous silicone-modified resin is formed by emulsion polymerization of a monomer in the presence of an emulsifier in an aqueous medium, and by further modification with silicone using a compound having a silicone structure.Type: ApplicationFiled: January 26, 2017Publication date: May 11, 2017Applicant: NIPPON SODA CO., LTD.Inventor: Kazunori SAITO
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Patent number: 9647258Abstract: A current collector is covered with sodium metal through: (1) applying a sodium dispersion containing sodium metal and at least one substance selected from the group consisting of an imide salt and a binder, on a current collector in an inert gas environment (with an oxygen concentration of not more than 0.01% and a dew point of not more than ?10° C.), followed by heating and drying; (2) pressure bonding a piece of solid sodium metal having a surface which exhibits a metallic luster onto a current collector in the aforementioned inert gas environment; (3) vapor-depositing sodium metal on a current collector in a reduced pressure environment; or (4) immersing a current collector having a surface fired at a temperature ranging from 150 to 300° C. in molten sodium metal after removing a coating film which is generated on a surface and formed from impurities, in the aforementioned inert gas environment.Type: GrantFiled: September 27, 2012Date of Patent: May 9, 2017Assignee: NIPPON SODA CO., LTD.Inventors: Hideaki Ito, Hitoshi Kobayashi, Toshiaki Yamashita, Shinichi Maruyama
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Patent number: 9635856Abstract: The present invention provides a method for producing a co-crystal including thiophanate-methyl and a triazole-based compound such as tebuconazole and a method for producing an agricultural and horticultural chemical preparation using the co-crystal as a raw material. As one example, the agricultural and horticultural chemical preparation can be obtained by a method including the steps of obtaining a sol including a co-crystal by stirring a suspension including thiophanate-methyl, a triazole compound such as a tebuconazole, a surfactant, a defoaming agent and water at a mixing degree of 0.1-1.0 while holding the temperature of the suspension at 60° C.; and adding auxiliary components such as silica, calcium carbonate and the like to the sol.Type: GrantFiled: December 10, 2014Date of Patent: May 2, 2017Assignee: Nippon Soda Co., Ltd.Inventor: Satoru Yamamura
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Publication number: 20170112134Abstract: A composition for preparing an emulsion or microemulsion, the composition including the following components (A) to (D): component (A): an active ingredient having a solubility in water at 20° C. of 200 ppm or less; component (B): a water-insoluble solvent having no alcohol group; component (C): at least one nonionic surfactant selected from the group consisting of a polyoxyalkylene alkyl ether, a polyoxyalkylene alkenyl ether, a polyoxyalkylene alkyl amino ether, and a polyoxyalkylene alkenyl amino ether; and component (D): a monohydric alcohol having 8 to 12 carbon atoms.Type: ApplicationFiled: March 25, 2015Publication date: April 27, 2017Applicant: Nippon Soda Co., Ltd.Inventors: Hiroshi Dairiki, Minoru SAKATANI
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Patent number: 9630933Abstract: The present invention provides a method for producing a 1H-tetrazole derivative by reacting an azide compound represented by general formula (II) and a cyanide compound represented by general formula (III) in a flow reactor to produce a compound represented by general formula (I) (wherein, Y represents an alkyl group, aryl group, arylalkyl group, substituted silyl group or substituted silylalkyl group, Z represents —CO—, —SO2— or —CRaRb— (wherein, Ra and Rb respectively and independently represent a hydrogen atom, alkyl group or unsubstituted or substituted aryl group), p represents 0 or 1, q represents 0 or 1, r represents 0 or 1 (provided that q is 1 in the case p is 0 or r is 0), R1 represents an alkyl group or hydrogen atom in the case q is 0 or an alkylene group in the case q is 1, and R2 represents an unsubstituted or substituted aryl group).Type: GrantFiled: June 7, 2013Date of Patent: April 25, 2017Assignee: Nippon Soda Co., Ltd.Inventor: Hidekazu Miyazaki
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Patent number: 9603365Abstract: The present invention provides a method for producing a co-crystal including thiophanate-methyl and a triazole-based compound such as tebuconazole and a method for producing an agricultural and horticultural chemical preparation using the co-crystal as a raw material. As one example, the agricultural and horticultural chemical preparation can be obtained by a method including the steps of obtaining a sol including a co-crystal by stirring a suspension including thiophanate-methyl, a triazole compound such as a tebuconazole, a surfactant, a defoaming agent and water at a mixing degree of 0.1-1.0 while holding the temperature of the suspension at 60° C.; and adding auxiliary components such as silica, calcium carbonate and the like to the sol.Type: GrantFiled: December 10, 2014Date of Patent: March 28, 2017Assignee: Nippon Soda Co., Ltd.Inventor: Satoru Yamamura
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Patent number: 9580384Abstract: The present invention provides a pest control agent, acaricide or fungicide that contains, as the active ingredient thereof, at least one type of compound selected from the aryloxyurea compounds represented by formula (V) (wherein R1 to R5 each independently represents an alkyl group or the like, X is a halogen atom or the like, n is an integer of 0 to 5, and Z is an oxygen atom or sulfur atom) or salts thereof.Type: GrantFiled: April 2, 2015Date of Patent: February 28, 2017Assignee: Nippon Soda Co., Ltd.Inventors: Hironori Furukawa, Takehiko Nakamura, Tetsuo Tamai, Daisuke Hanai