Patents Assigned to NIST
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Publication number: 20220349628Abstract: A compact, low power cryo-cooler for cryogenic systems capable of cooling gas to at least as low as 2.5 K. The cryo-cooler has a room temperature compressor followed by filtration. Within the cryostat, four counterflow heat exchangers precool the incoming high-pressure gas using the outflowing low-pressure gas. The three warmest heat exchangers are successively heat sunk to three stages of a pulse tube to absorb residual heat from the slight ineffectiveness of the heat exchangers. The pulse tube cold head also absorbs loads from instrumentation leads and radiation loads. The pulse tube stages operate at around 80 K, 25 K, and 10 K. The entire system—cryo-cooler, drive and control electronics, and detector instrumentation, fits in a standard electronics rack mount enclosure, and requires around 300 W or less of power.Type: ApplicationFiled: July 5, 2022Publication date: November 3, 2022Applicant: National Institute of Standards and Technology (NIST)Inventors: Vincent Kotsubo, Joel Ullom, Sae Woo Nam
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Publication number: 20190226724Abstract: A compact, low power cryo-cooler for cryogenic systems capable of cooling gas to at least as low as 2.5 K. The cryo-cooler has a room temperature compressor followed by filtration. Within the cryostat, four counterflow heat exchangers precool the incoming high-pressure gas using the outflowing low-pressure gas. The three warmest heat exchangers are successively heat sunk to three stages of a pulse tube to absorb residual heat from the slight ineffectiveness of the heat exchangers. The pulse tube cold head also absorbs loads from instrumentation leads and radiation loads. The pulse tube stages operate at around 80 K, 25 K, and 10 K. The entire system—cryo-cooler, drive and control electronics, and detector instrumentation, fits in a standard electronics rack mount enclosure, and requires around 300 W or less of power.Type: ApplicationFiled: January 24, 2019Publication date: July 25, 2019Applicant: National Institute of Standards and Technology (NIST)Inventors: Vincent Kotsubo, Joel Ullom, Sae Woo Nam
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Patent number: 9580828Abstract: A self-terminating rapid process for controlled growth of platinum or platinum alloy monolayer films from a K2PtCl4—NaCl—NaBr electrolyte. Using the present process, platinum deposition may be quenched at potentials just negative of proton reduction by an alteration of the double layer structure induced by a saturated surface coverage of underpotential deposited hydrogen. The surface may be reactivated for platinum deposition by stepping the potential to more positive values where underpotential deposited hydrogen is oxidized and fresh sites for absorption of platinum chloride become available. Periodic pulsing of the potential enables sequential deposition of two dimensional platinum layers to fabricate films of desired thickness relevant to a range of advanced technologies, from catalysis to magnetics and electronics.Type: GrantFiled: August 28, 2013Date of Patent: February 28, 2017Assignee: The United States of America, as represented by the Secretary of Commerce (NIST)Inventors: Thomas P. Moffat, Yihua Liu
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Patent number: 8680482Abstract: A method for aligning the axis of an atom beam with the orientation of an electric field at a particular location within an enclosure for use in creating a charged particle source by photoionizing a cold atom beam. The method includes providing an atom beam in the enclosure, providing a plurality of electrically conductive devices in said enclosure, evacuating the enclosure to a pressure below about 10?6 millibar, and aligning the axis of the atom beam with the orientation of the electric field, relative to each other, within less than about two degrees. Alignment may be facilitated by applying at least one voltage to the electrically conductive devices, mechanically tilting the atom beam's axis orientation of the electric field relative to each other and/or causing a deflection of the atom beam.Type: GrantFiled: August 8, 2013Date of Patent: March 25, 2014Assignee: The United States of America, as represented by the Secretary of Commerce, NISTInventors: Jabez J. McClelland, Brenton J. Knuffman, Adam V. Steele
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Patent number: 8642964Abstract: A terahertz generation system that emits pulsed THz radiation and incorporates a rapidly oscillating, high voltage bias across electrodes insulated from a photoconductive material. The system includes an ultrafast optical pulse source configured to generate an optical pulse having a duration between about ten picoseconds and ten femtoseconds, the pulse further having a repetition rate of about one megahertz or higher. The system further includes a photoconductor configured to receive the optical pulse from the ultrafast optical pulse source and to generate a terahertz frequency pulse, the photoconductor having insulated electrodes. The system still further includes a radio frequency generator configured to apply an electric field to the photoconductor via the insulated electrodes.Type: GrantFiled: August 22, 2011Date of Patent: February 4, 2014Assignee: The United States of America, as represented by the Secretary of Commerce, NISTInventors: Steven Cundiff, Jared Wahlstrand, Haipeng Zhang, Soobong Choi
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Patent number: 8642982Abstract: A fast switching arbitrary frequency light source for broadband spectroscopic applications. The light source may operate near 1.6 um based on sideband tuning using an electro-optic modulator driven by an arbitrary waveform generator. A Fabry-Perot filter cavity selects a single sideband of the light source. The finesse (FSR/??FWHM) of the filter cavity may be chosen to enable rapid frequency switching at rates up to 5 MHz over a frequency range of 40 GHz (1.3 cm?1). The bandwidth, speed and spectral purity are high enough for spectroscopic applications where rapid and discrete frequency scans are needed. Significant signal-to-noise advantages may be realized using the rapid and broadband scanning features of this system in many areas of spectroscopy, e.g., process monitoring and control, reaction dynamics, and remote sensing (e.g., greenhouse gas monitoring, biological/chemical agent screening).Type: GrantFiled: March 14, 2013Date of Patent: February 4, 2014Assignee: The United States of America, as represented by the Secretary of Commerce, NISTInventors: David F. Plusquellic, Kevin O. Douglass, Stephen E. Maxwell, Joseph T. Hodges, David A. Long, Gar-Wing Truong
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Patent number: 8641798Abstract: A one-step process for synthesizing gold-copper bimetallic nanocubes. The process comprises the step of simultaneously reducing a copper II salt and a gold halide by 1,2-hexadecanediol in diphenyl ether, and 1-dodecanethiol as well as surfactants 1-adamantanecarboxylic acid and 1-hexadecylamine. The copper II salt may be copper (II) acetylacetonate, copper chloride, copper sulfate, or copper phosphate. The gold halide may be chloroauric acid, gold chloride, gold bromide, or tetrabromoauric acid. The reduction may occur at a temperature between about 160 and 180 degrees Celsius. The copper II salt may be copper (II) acetylacetonate and the gold halide may be chloroauric acid.Type: GrantFiled: July 12, 2011Date of Patent: February 4, 2014Assignee: The United States of America, as represented by the Secretary of Commerce, NISTInventors: Angela R. Hight-Walker, Yonglin Liu
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Publication number: 20130320202Abstract: A method for aligning the axis of an atom beam with the orientation of an electric field at a particular location within an enclosure for use in creating a charged particle source by photoionizing a cold atom beam. The method includes providing an atom beam in the enclosure, providing a plurality of electrically conductive devices in said enclosure, evacuating the enclosure to a pressure below about 10?6 millibar, and aligning the axis of the atom beam with the orientation of the electric field, relative to each other, within less than about two degrees. Alignment may be facilitated by applying at least one voltage to the electrically conductive devices, mechanically tilting the atom beam's axis orientation of the electric field relative to each other and/or causing a deflection of the atom beam.Type: ApplicationFiled: August 8, 2013Publication date: December 5, 2013Applicant: United States of America, as represented by the Secretary of Commerce, NISTInventors: Jabez McClelland, Brenton Knuffman, Adam Steele
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Patent number: 8554009Abstract: A simple matrix method and computer program product for stray-light correction in imaging instruments is provided. The stray-light correction method includes receiving raw signals from an imaging instrument and characterizing the imaging instrument for a set of point spread functions. For high resolution imaging instruments, the raw signals may be compressed to reduce the size of the correction matrix. Based on stray-light distribution functions derived from the point spread functions, a correction matrix is derived. This fast correction is performed by a matrix multiplication to the measured raw signals, and may reduce stray-light errors by more than one order of magnitude. Using the stray-light corrected instrument, significant reductions may be made in overall measurement uncertainties in radiometry, colorimetry, photometry and other applications. Because the PSFs may include other types of undesired responses, the stray-light correction also eliminates other types of errors, e.g.Type: GrantFiled: August 13, 2008Date of Patent: October 8, 2013Assignee: The United States of America as represented by the Secretary of Commerce (NIST)Inventors: Yuqin Zong, Steven W. Brown, Keith R. Lykke, Yoshihiro Ohno
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Patent number: 8535761Abstract: A method of forming a coating comprising the steps of dissolving an silsesquioxane (e.g., one that is primarily a cage compound with 8, 10, 12, 14 or related complete cages or with partially condensed cages containing primarily Si(O)4 units in the cage) in a solvent to form an silsesquioxane solution; introducing (e.g., dissolving) an additive in the solution (e.g., the additive being selected from a rare earth compound, an acid, an organic moiety, a precious metal or compound thereof, a transition metal compound, or any combination thereof, or any of their ionic constituents); and optionally mixing a diluent with the solution to form a coating that is applied to a substrate, wherein the resulting coating forms crosslinks between resulting pendant Si(OH)x groups and a substrate surface. The present invention also contemplates coatings and coated articles consistent with the present teachings.Type: GrantFiled: February 12, 2010Date of Patent: September 17, 2013Assignees: Mayaterials, Inc., NISTInventors: Richard M. Laine, Christopher L. Soles, David J. Krug, III, Hyun Wook Ro, Vera Nikolova Popova-Gueorguieva
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Patent number: 8530853Abstract: A system for producing a charged particle beam from a photoionized cold atom beam. A vapor of neutral atoms is generated. From these atoms, an atom beam having axial and transverse velocity distributions controlled by the application of laser light is produced. The produced atom beam is spatially compressed along each transverse axis, thus reducing the cross-sectional area of the produced beam and reducing a velocity spread of the produced beam along directions transverse to the beam's direction of propagation. Laser light is directed onto at least a portion of the neutral atoms in the atom beam, thereby producing ions and electrons. An electric field is generated at the location of the produced ions and electrons, thereby producing a beam of ions traveling in a first direction and electrons traveling in substantially the opposite direction. A vacuum chamber contains the atom beam, the ion beam and the electron beam.Type: GrantFiled: February 8, 2012Date of Patent: September 10, 2013Assignee: The United States of America, as represented by the Secretary of Commerce, NISTInventors: Adam V. Steele, Brenton J. Knuffman, Jabez J. McClelland
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Patent number: 8350556Abstract: An integrated optical element and Faraday cup that can measure charged particle beam currents, manipulate light and analyze charged particle beam energy distribution. One boundary of the cup is formed by a lens or other suitable optical element which can be used for manipulating light along the axis of the Faraday cup. The surface of the optical element interior to the cup is coated with a transparent conductor in order to establish the simultaneous functions of taking charged particle beam current measurements, taking energy distribution measurements and manipulating light for such applications as focusing or imaging. A suppressor/blanker/retarder electrode is designed to eliminate spurious current signals that can result from production of secondary electrons by the charged particle beam impinging on the electrode surface.Type: GrantFiled: January 21, 2010Date of Patent: January 8, 2013Assignee: The United States of America as represented by the Secretary of Commerce, NISTInventors: Brenton J. Knuffman, Adam V. Steele, Jabez J. McClelland
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Patent number: 7994027Abstract: The present invention grows nanostructures using a microwave heating-based sublimation-sandwich SiC polytype growth method comprising: creating a sandwich cell by placing a source wafer parallel to a substrate wafer, leaving a small gap between the source wafer and the substrate wafer; placing a microwave heating head around the sandwich cell to selectively heat the source wafer to a source wafer temperature and the substrate wafer to a substrate wafer temperature; creating a temperature gradient between the source wafer temperature and the substrate wafer temperature; sublimating Si- and C-containing species from the source wafer, producing Si- and C-containing vapor species; converting the Si- and C-containing vapor species into liquid metallic alloy nanodroplets by allowing the metalized substrate wafer to absorb the Si- and C-containing vapor species; and growing nanostructures on the substrate wafer once the alloy droplets reach a saturation point for SiC.Type: GrantFiled: May 11, 2009Date of Patent: August 9, 2011Assignees: George Mason Intellectual Properties, Inc., NISTInventors: Yonglai Tian, Rao V. Mulpuri, Siddharth G. Sundaresan, Albert V. Davydov
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Patent number: 7967507Abstract: A dimensional reference system for tomography, including X-ray computed tomography and MRI tomography. The system includes a dimensional reference apparatus that comprises plurality of spheres composed of a material having an X-ray absorption property between approximately +500 Hounsfield units and +1200 Hounsfield units. The spheres are spaced apart at a known distance by support structure/spacer unit that has an X-ray absorption property between approximately ?100 Hounsfield units and +400 Hounsfield units. After an image that incorporates the dimensional reference apparatus and a measurement subject has been reconstructed, the dimensional reference apparatus provides for measurement of the resultant image voxels in three dimensions. Because solid structural elements such as plastic or glass spheres may not be visible in an MRI, an MRI implementation of the apparatus may be disposed in a fluid-tight enclosure along with water, a contrast-enhancing agent and ethanol.Type: GrantFiled: March 5, 2009Date of Patent: June 28, 2011Assignee: The United States of America as represented by the Secretary of Commerce, NISTInventors: Zachary H. Levine, Steven Grantham
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Patent number: 7894074Abstract: A laser Doppler vibrometer for vibration measurement that employs active feedback to cancel the effect of large vibration excursions at low frequencies, obviating the need to unwrap phase data. The Doppler shift of a reflective vibrating test object is sensed interferometrically and compensated by means of a voltage-controlled oscillator driving an acousto-optic modulator. For frequencies within the servo bandwidth, the feedback signal provides a direct measurement of vibration velocity. For frequencies outside the servo bandwidth, feedback biases the interferometer at a point of maximal sensitivity, thus enabling phase-sensitive measurement of the high-frequency excursions. Using two measurements, one with a low bandwidth and one with a high bandwidth, more than five decades of frequency may be spanned.Type: GrantFiled: December 19, 2008Date of Patent: February 22, 2011Assignee: The United States of America as represented by the Secretary of Commerce, NISTInventor: John Lawall
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Patent number: 6201638Abstract: A low-loss comb-generating optical cavity including an optical amplifier and a microwave-driven electro-optic modulator crystal, produces a comb of optical frequency sidebands having spectral lines equally spaced around the frequency of an input laser beam incident on the comb-generating cavity. The comb-generating cavity includes an input mirror movable along the beam propagation direction, and a fixed position output mirror located at time synchronous distances of both the input laser wavelength and modulation wavelength. The comb-generating cavity and its microwave driven modulator are in resonance with the input laser beam, and provide iterative or recirculating beam action that transfers the input optical frequency of the laser, sideband by sideband, to remote and precisely known comb frequencies offset from, and centered on, the input laser frequency.Type: GrantFiled: January 13, 1999Date of Patent: March 13, 2001Assignees: University Technology Corporation, NISTInventors: John Lewis Hall, Scott Alan Diddams, Long-Sheng Ma, Jun Ye
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Patent number: 4305412Abstract: The improved eyelash curler of the present invention comprises a blade, a pad, support means holding the pad substantially horizontally below the substantially horizontal blade and means for vertically controllably opposing the pad and blade to curl eyelashes therebetween. The surface of the blade and/or pad which contacts the eyelashes during curling thereof is substantially curved and/or sloped from the horizontal to impart varying degrees of curl to various portions of the eyelashes for an improved natural appearance. The pad and/or blade can be made removable from the curler and, preferably, reversible. The curler may, if desired, be adapted for primary use for one eye, specifically the eyelashes of the upper lid of one eye, and a pair of such curlers can be used, one for each eye. The curler is simple, inexpensive and effective.Type: GrantFiled: May 19, 1980Date of Patent: December 15, 1981Assignee: Donald E. NistInventor: Margaret E. Nist