Patents Assigned to Novus International, Inc.
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Patent number: 6319525Abstract: A process for formulating a ruminant food ration in which the methionine needs of the ruminant are determined, a plurality of natural or synthetic feed ingredients and the nutrient composition of each of said ingredients are identified wherein one of said ingredients is 2-hydroxy-4-(methylthio)butanoic acid or a salt, amide or ester thereof, and a ration is formulated from the identified feed ingredients to meet the determined methionine needs of the ruminant which comprises one or more grains, a hydroxy analog of methionine, and optionally a bypass fat wherein (i) the hydroxy analog of methionine is selected from the group consisting of 2-hydroxy-4-(methylthio)butanoic acid and the salts, amides and esters thereof, (ii) the hydroxy analog of methionine is added separately from any bypass fat which is included in the ration, and (iii) the ration is formulated on the basis that at least 20% of the hydroxy analog of methionine is assumed to be available for absorption by the ruminant.Type: GrantFiled: October 26, 2000Date of Patent: November 20, 2001Assignee: Novus International, Inc.Inventors: Christopher D. Knight, Karen M. Koenig, Lyle M. Rode, Michael J. Vandenberg, Mercedes Vazquez-Anon
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Patent number: 6320076Abstract: A process for the continuous preparation of 3-(methylthio)propanal. A liquid reaction medium is contacted with a gaseous acrolein feed stream in a gas/liquid contact zone. The reaction medium contains 3-(methylthio)propanal, methyl mercaptan and a catalyst for the reaction between methyl mercaptan and acrolein. The gaseous acrolein feed stream comprises acrolein vapor and non-condensable gas. Acrolein is transferred from the acrolein feed stream to the reaction medium and reacts with methyl mercaptan in that medium to produce a liquid reaction product containing 3-(methylthio)propanal. The non-condensable gas is separated from the liquid reaction product. The reaction product is divided into a product fraction and a circulating fraction, and the circulating fraction is recycled to the gas/liquid contact zone.Type: GrantFiled: December 22, 1999Date of Patent: November 20, 2001Assignee: Novus International, Inc.Inventors: Yung C. Hsu, Dennis A. Ruest
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Patent number: 6268531Abstract: A continuous process for the preparation of 2-hydroxy-4-methylthiobutanoic acid or a salt thereof which includes introducing an aqueous mineral acid into a nitrile hydrolysis reactor including a continuous stirred tank reactor and introducing 2-hydroxy-4-methylthiobutanenitrile into the nitrile hydrolysis reactor. 2-hydroxy-4-methylthiobutanenitrile is continually hydrolyzed within the nitrile hydrolysis reactor to produce a nitrile hydrolysis reactor product stream containing 2-hydroxy-4-methylthiobutanamide. The nitrile hydrolysis reactor product stream is continuously introduced into an amide hydrolysis flow reactor. 2-hydroxy-4-methylthiobutanamide is continually hydrolyzed within the amide hydrolysis flow reactor to produce an aqueous hydrolyzate product containing 2-hydroxy-4-methylthiobutanoic acid. 2-hydroxy-4-methylthiobutanoic acid is recovered from the aqueous hydrolyzate product.Type: GrantFiled: October 2, 1998Date of Patent: July 31, 2001Assignee: Novus International, Inc.Inventors: Yung C. Hsu, Thomas F. Blackburn, Paul F. Pellegrin, Allen H. Kranz, James M. Willock
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Patent number: 6210718Abstract: A nutrient formulation including moisture, a coloring agent, a palatability modifier, and/or an adjuvant which is designed for use in poultry and other animals, and a method of feeding it which improves subsequent livability, cumulative feed efficiency, weight gain, and resistance to disease challenge or other stresses is disclosed.Type: GrantFiled: June 17, 1999Date of Patent: April 3, 2001Assignee: Novus International, Inc.Inventors: Francis J. Ivey, Julia J. Dibner, Christopher D. Knight
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Patent number: 6206203Abstract: Apparatus and process for separating components of a treatment mixture from a waste treatment system comprises feeding the treatment mixture to an endless filtering belt. The filtering belt has a mesh size selected to permit liquid components of the mixture to filter down through the belt while retaining particulate components thereon. The belt is moved by a drive system generally in a circuit between upstream and downstream ends of the apparatus as liquid components are separated from the mixture by filtering through the filtering belt. Unfiltered mixture is passed beneath a press disposed in opposed relation with the belt generally between the upstream and downstream ends of the apparatus. The press is capable of applying a squeezing pressure against the mixture to squeeze the mixture between the press and the filtering belt to separate water and liquified fatty components from the mixture for filtering through the belt.Type: GrantFiled: July 23, 1998Date of Patent: March 27, 2001Assignee: Novus International, Inc.Inventors: Matthew B. Hopkins, William D. Shermer, Jeff R. Herbst, Robert J. DeRosa
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Patent number: 6183786Abstract: A process for formulating a ruminant food ration in which the methionine needs of the ruminant are determined, a plurality of natural or synthetic feed ingredients and the nutrient composition of each of said ingredients are identified wherein one of said ingredients is 2-hydroxy-4-(methylthio)butanoic acid or a salt, amide or ester thereof, and a ration is formulated from the identified feed ingredients to meet the determined methionine needs of the ruminant which comprises one or more grains, a hydroxy analog of methionine, and optionally a bypass fat wherein (i) the hydroxy analog of methionine is selected from the group consisting of 2-hydroxy-4-(methylthio)butanoic acid and the salts, amides and esters thereof, (ii) the hydroxy analog of methionine is added separately from any bypass fat which is included in the ration, and (iii) the ration is formulated on the basis that at least 20% of the hydroxy analog of methionine is assumed to be available for absorption by the ruminant.Type: GrantFiled: June 15, 1999Date of Patent: February 6, 2001Assignee: Novus International, Inc.Inventors: Christopher D. Knight, Karen M. Koenig, Lyle M. Rode, Michael J. Vandenberg, Mercedes Vazquez-Anon
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Patent number: 6166250Abstract: A continuous process for the preparation of 2-hydroxy-4-methylthiobutanoic acid which includes introducing sulfuric acid into a first reactor including a continuous stirred tank reactor and introducing 2-hydroxy-4-methylthiobutanenitrile into the first reactor. 2-hydroxy-4-methylthiobutanenitrile is continually hydrolyzed within the first reactor to produce an intermediate aqueous hydrolysis solution containing 2-hydroxy-4-methylthiobutanamide. The intermediate aqueous hydrolysis solution is continuously introduced into a plug flow reactor. 2-hydroxy-4-methylthiobutanamide is continually hydrolyzed within the plug flow reactor to produce an aqueous hydrolyzate product solution containing 2-hydroxy-4-methylthiobutanoic acid. 2-hydroxy-4-methylthiobutanoic acid is recovered from the aqueous hydrolyzate product solution.Type: GrantFiled: October 2, 1998Date of Patent: December 26, 2000Assignee: Novus International, Inc.Inventors: Yung C. Hsu, Thomas F. Blackburn, Paul F. Pellegrin, Allen H. Kranz, James M. Willock
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Patent number: 6113800Abstract: A treatment process for recovering protein, fatty and water component products from a float material produced by a waste water treatment system, wherein the protein and fatty components possess improved stability and are suitable for further processing for inclusion in various products, such as animal feed. The recovered water component can also be further processed before discharge into a sewer system.Type: GrantFiled: July 23, 1998Date of Patent: September 5, 2000Assignee: Novus International, Inc.Inventors: Matthew B. Hopkins, Robert J. DeRosa, William D. Shermer
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Patent number: 6031138Abstract: A process for the continuous preparation of 3-(methylthio)propanal. A liquid reaction medium is contacted with a gaseous acrolein feed stream in a gas/liquid contact zone. The reaction medium contains 3-(methylthio)propanal, methyl mercaptan and a catalyst for the reaction between methyl mercaptan and acrolein. The gaseous acrolein feed stream comprises acrolein vapor and non-condensable gas. Acrolein is transferred from the acrolein feed stream to the reaction medium and reacts with methyl mercaptan in that medium to produce a liquid reaction product containing 3-(methylthio)propanal. The non-condensable gas is separated from the liquid reaction product. The reaction product is divided into a product fraction and a circulating fraction, and the circulating fraction is recycled to the gas/liquid contact zone.Type: GrantFiled: June 22, 1998Date of Patent: February 29, 2000Assignee: Novus International, Inc.Inventors: Yung C. Hsu, Dennis A. Ruest
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Patent number: 6017563Abstract: A process for formulating a ruminant food ration in which the methionine needs of the ruminant are determined, a plurality of natural or synthetic feed ingredients and the nutrient composition of each of the ingredients are identified wherein one of the ingredients is 2-hydroxy-4-(methylthio)butanoic acid or a salt, amide or ester thereof, and a ration is formulated from the identified feed ingredients to meet the determined methionine needs of the ruminant which comprises one or more grains, a hydroxy analog of methionine, and optionally a bypass fat wherein (i) the hydroxy analog of methionine is selected from the group consisting of 2-hydroxy-4-(methylthio)butanoic acid and the salts, amides and esters thereof, (ii) the hydroxy analog of methionine is added separately from any bypass fat which is included in the ration, and (iii) the ration is formulated on the basis that at least 20% of the hydroxy analog of methionine is assumed to be available for absorption by the ruminant.Type: GrantFiled: July 25, 1997Date of Patent: January 25, 2000Assignee: Novus International, Inc.Inventors: Christopher D. Knight, Karen M. Koenig, Lyle M. Rode, Michael J. Vandenberg, Mercedes Vazquez-Anon
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Patent number: 5998664Abstract: A continuous process for the preparation of 2-hydroxy-4-methylthiobutanoic acid which includes introducing sulfuric acid into a first reactor including a continuous stirred tank reactor and introducing 2-hydroxy-4-methylthiobutanenitrile into the first reactor. 2-hydroxy-4-methylthiobutanenitrile is continually hydrolyzed within the first reactor to produce an intermediate aqueous hydrolysis solution containing 2-hydroxy-4-methylthiobutanamide. The intermediate aqueous hydrolysis solution is continuously introduced into a plug flow reactor. 2-hydroxy-4-methylthiobutanamide is continually hydrolyzed within the plug flow reactor to produce an aqueous hydrolyzate product solution containing 2-hydroxy-4-methylthiobutanoic acid. 2-hydroxy-4-methylthiobutanoic acid is recovered from the aqueous hydrolyzate product solution.Type: GrantFiled: June 13, 1997Date of Patent: December 7, 1999Assignee: Novus International, Inc.Inventors: Yung C. Hsu, Thomas F. Blackburn, Paul F. Pellegrin, Allen H. Kranz, James M. Willock
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Patent number: 5985336Abstract: A nutrient formulation including moisture which is designed for use in poultry and other animals, and a method of feeding it which improves subsequent livability, cumulative feed efficiency and weight gain is disclosed. The method comprises making available for consumption ad libitum a high moisture material containing at least about 20% by weight water to the poultry or other animals before they are offered dry food ad libitum.Type: GrantFiled: May 24, 1996Date of Patent: November 16, 1999Assignee: Novus International, Inc.Inventors: Francis J. Ivey, Julia J. Dibner, Christopher D. Knight
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Patent number: 5983198Abstract: The system and method include a fleet of vehicles to provide material to a plurality of tanks at various customer locations. An inventory indicator associated with each of the tanks provides a quantity signal to the central station indicating the quantity and temperature of each of the tanks. A processor at the central station monitors the quantity signals of each of the tanks to determine past usage rates of the contents of each of the tanks. The processor projects future tank quantities based on the past usage pattern and determines possible routes for each of the vehicles to each of the tanks. The processor optimizes the routes, delivery amounts, and delivery schedule to minimize total delivered cost for the products based on the projected future tank levels and the possible routes to dispatch each of the vehicles.Type: GrantFiled: April 23, 1996Date of Patent: November 9, 1999Assignee: Novus International, Inc.Inventors: Kevin M. Mowery, John P. Bartley, Robert J. Hantak, Richard E. Etling, Joseph R. Read
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Patent number: 5980754Abstract: A process for recovering protein, fatty and water components from a float material produced by a waste water treatment system, wherein the protein and fatty components can be further processed for inclusion in various products, such as animal feed. The recovered water component can also be further processed before discharged into a sewer system.Type: GrantFiled: January 23, 1997Date of Patent: November 9, 1999Assignee: Novus International, Inc.Inventors: Matthew B. Hopkins, Robert J. DeRosa
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Patent number: 5976580Abstract: A nutrient formulation including moisture, a coloring agent, a palatability modifier, and/or an adjuvant which is designed for use in poultry and other animals, and a method of feeding it which improves subsequent livability, cumulative feed efficiency, weight gain, and resistance to disease challenge or other stresses is disclosed.Type: GrantFiled: December 6, 1996Date of Patent: November 2, 1999Assignee: Novus International, Inc.Inventors: Francis J. Ivey, Julia J. Dibner, Christopher D. Knight
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Patent number: 5973200Abstract: A process for the free-radical addition of a mercaptan to a nonconjugated olefinic substrate having a terminal carbon-carbon double bond is disclosed. 2-Hydroxy-4-(ethylthio)butanoic acid (HMBA) or methionine can be prepared using this method. The nonconjugated olefinic substrate has the general formula: ##STR1## wherein R is selected from the group consisting of --COOH, --COOR.sup.2, --CONR.sup.3 R.sup.4, --CN and --CCl.sub.3, R.sup.1 is selected from the group consisting of --OH, --OCOR.sup.2, --NHCOR.sup.2 and --NH.sub.2, R.sup.2 is selected from the group consisting of alkyl, cycloalkyl and aryl and R.sup.3 and R.sup.4 are independently selected from the group consisting of --H and R.sup.2.Type: GrantFiled: January 20, 1998Date of Patent: October 26, 1999Assignee: Novus International, Inc.Inventor: Karl E. Koenig
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Patent number: 5928686Abstract: A nutrient formulation including moisture which is designed for use in very young poultry, and a method of feeding it which improves subsequent livability, cumulative feed efficiency and weight gain is disclosed. The method includes feeding a high moisture solid containing at least about 20% by weight water to the poultry before the poultry is allowed to eat dry food ad libitum.Type: GrantFiled: June 7, 1995Date of Patent: July 27, 1999Assignee: Novus International, Inc.Inventors: Francis J. Ivey, Julia J. Dibner, Christopher D. Knight
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Patent number: 5925794Abstract: A process for the continuous preparation of 3-(methylthio)propanal. A liquid reaction medium is contacted with a gaseous acrolein feed stream in a gas/liquid contact zone. The reaction medium contains 3-(methylthio)propanal, methyl mercaptan and a catalyst for the reaction between methyl mercaptan and acrolein. The gaseous acrolein feed stream comprises acrolein vapor and non-condensable gas. Acrolein is transferred from the acrolein feed stream to the reaction medium and reacts with methyl mercaptan in that medium to produce a liquid reaction product containing 3-(methylthio)propanal. The non-condensable gas is separated from the liquid reaction product. The reaction product is divided into a product fraction and a circulating fraction, and the circulating fraction is recycled to the gas/liquid contact zone.Type: GrantFiled: June 20, 1996Date of Patent: July 20, 1999Assignee: Novus International, Inc.Inventors: Yung C. Hsu, Dennis A. Ruest
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Patent number: 5905171Abstract: A process for the continuous preparation of 3-(methylthio)propanal. A liquid reaction medium is contacted with a gaseous acrolein feed stream in a gas/liquid contact zone. The reaction medium contains 3-(methylthio)propanal, methyl mercaptan and a catalyst for the reaction between methyl mercaptan and acrolein. The gaseous acrolein feed stream comprises acrolein vapor and non-condensable gas. Acrolein is transferred from the acrolein feed stream to the reaction medium and reacts with methyl mercaptan in that medium to produce a liquid reaction product containing 3-(methylthio)propanal. The non-condensable gas is separated from the liquid reaction product. The reaction product is divided into a product fraction and a circulating fraction, and the circulating fraction is recycled to the gas/liquid contact zone.Type: GrantFiled: June 20, 1996Date of Patent: May 18, 1999Assignee: Novus International, Inc.Inventor: Yung C. Hsu
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Patent number: 5878767Abstract: A system for transferring fluid from a filling reservoir to a receiving tank. The system includes a fluid transfer line for conveying fluid from the filling reservoir outlet to the receiving tank inlet, and couplings for selectively connecting the fluid transfer line to a filling reservoir outlet and a receiving tank inlet. The system further includes a vapor return line for conveying vapor from a receiving tank vent to a filling reservoir inlet to simultaneously prevent pressure from building in the tank and a vacuum from developing in the reservoir as fluid is transferred from the reservoir to the tank, and couplings for selectively connecting the vapor return line to the filling reservoir inlet and the receiving tank vent.Type: GrantFiled: December 13, 1996Date of Patent: March 9, 1999Assignee: Novus International, Inc.Inventors: Richard E. Etling, Samuel J. Jenkins, Stephen J. Lorbert, Philip H. Allen, Anthony F. DeJohn