Abstract: Analytic sensors and methods utilize an attenuated total reflection (ATR) crystal to detect volatile compounds in an arrangement that reduces interference from compounds other than the one of interest. In particular, the components in the measurement stream are limited to those having volatilities close to that of the analyte of interest, which may be identified based on, for example, the temperature of the ATR crystal and the “dwell time”—i.e., an interval of substantially constant temperature as the ATR crystal is heated.
Abstract: Analytic sensors and methods utilize an attenuated total reflection (ATR) crystal to detect volatile compounds in an arrangement that reduces interference from compounds other than the one of interest. In particular, the components in the measurement stream are limited to those having volatilities close to that of the analyte of interest, which may be identified based on, for example, the temperature of the ATR crystal and the “dwell time”—i.e., an interval of substantially constant temperature as the ATR crystal is heated.
Abstract: In accordance with embodiments of the present invention, a terpene-rich sample is prepared for terpene analysis using liquid chromatography via an extraction method that takes little time, uses minimal external equipment, and permits direct injection of extracted terpenes into a liquid chromatography instrument for analysis. An embodiment of the invention involves preparing a terpene-containing sample for analysis by liquid chromatography by liquid extraction; heating the liquid extract in a vial that contains a filter medium or solvent; collecting the terpenes in the medium by the vapor pressure forced through the filter from heating; and eluting the collected terpenes into a vial or directly into a chromatography injector.
Abstract: A cannabinoid analysis system includes a solvent input port configured to receive a flow of a solvent, a sample input port configured to receive a chemical mixture including a sample, a pump configured to move the solvent and chemical mixture, an extraction cartridge coupled to the pump and configured to separate a combination of the chemical mixture and the flow of the solvent into two or more partially-separated chemical components, a spectroscopy cell configured to generate a chromatogram including two or more overlapping absorption peaks corresponding to the two or more partially-separated chemical components, and a controller configured to determine a chemical concentration of each partially-separated chemical component of the two or more partially-separated chemical components.