Abstract: A method for the regeneration of spent pickling acids. Said acid is mixed with such a minor quantity of a stronger acid that the losses of said stronger acid are compensated. The mixture obtained is stripped, whereby the weaker acids are vaporized. The vapor phase containing the weaker acids is passed to a condenser. The condensate obtained forms the regenerated pickling acid. The spent pickling acid can also be passed directly to an evaporator in which a solution containing a stronger acid is circulated. The vapor from the evaporator is passed to an absorption column and thereafter to a condenser, the regenerated acid being formed of the condensate from said condenser.