Abstract: Polycyanate esters of polyhydric phenols are cured with a liquid solution of a metal acetylacetonate in an alkylphenol. Such cured compositions are useful in structural composites, transfer molded-encapsulants, filmed structural adhesives and printed wiring boards.

Abstract: Low viscosity dicyanate esters are made from bisphenols wherein the bridging member between the phenyl groups is unsymmetrical. These dicyanate esters are blended with prepolymers of dicyanate esters to form low viscosity non-crystallizing resins useful in preparing composites.

Abstract: A thermoplastic pelletizable polymer composition comprising an oligomer or degraded polyolefin and an olefinic elastomer. Optionally, the composition can also include a polyolefin thermoplastic polymer. The composition, when converted to a film or fabric meets the criteria or drapability, low hardness on the Shore A scale, high melt flow and reprocessability.

Abstract: A method for the manufacture of polyester polyols is disclosed. The method comprises feeding to a reactor at least one aliphatic carboxylic acid or ester thereof, at least one secondary dihydric alcohol and at least one primary trihydric alcohol, heating the resultant admixture and removing water. When at least 95% of the water has been removed, N-phenyl dialkanolamine and additional primary trihydric alcohol are added and heating is continued. The reactants are selected so that the range of molecular weights thereof is not more than 100. A block polyester polyol is obtained. Polyurethanes obtained from the polyester polyol tend to have more uniform and superior properties. The polyurethanes may be used in variety of end uses.

Abstract: A spin welding apparatus is employed for hermetically sealing seamless overpacks. The seamless overpacks are utilized, for example, for isolating corroding 55 gallon drums which contain hazardous materials. The overpacks include a receiver which contains the 55 gallon drum and a cover which is spin welded onto the receiver. The receiver and cover have circular welding surfaces which oppose one cover which is spin welded onto the receiver. The receiver and cover have circular welding surfaces which oppose one another across a horizontal plane. The welding surfaces have a composition of heat fusible plastic. During the spin welding process, the cover is rotationally driven by the spin welding apparatus while simultaneously being forced downward onto the receiver, which is held stationary. Frictional heat melts the opposing welding surfaces. After the rotational motion stops, the opposing welding surfaces cool and solidify to form a seamless weld joint.

Abstract: A staged mold for stabilizing hazardous wastes for final disposal by molding an agglomerate of the hazardous wastes and encapsulating the agglomerate. Three stages are employed in the process. In the first stage, a first mold body is positioned on a first mold base, a mixture of the hazardous wastes and a thermosetting plastic is loaded into the mold, the mixture is mechanically compressed, heat is applied to cure the mixture to form a rigid agglomerate, and the first mold body is removed leaving the agglomerate sitting on the first mold base. In the second stage, a clamshell second mold body is positioned around the agglomerate and the first mold base, a powdered thermoplastic resin is poured on top of the agglomerate and in the gap between the sides of the agglomerate and the second mold body, the thermoplastic is compressed, heat is applied to melt the thermoplastic, and the plastic is cooled jacketing the agglomerate on the top and sides.

Abstract: This invention provides a process for preparing a viscoelastic aqueous solution which contains divinylsulfone-crosslinked polygalactomannan gum that is formed in situ.An invention thixotropic aqueous medium is characterized by excellent heat/shear stability and high tolerance to the presence of inorganic salts.A unique property of an invention thixotropic aqueous medium is a time-dependent gradual restoration of high viscosity after cessation of high shear deformation.

Abstract: A low smoke and flame retardant composition comprising an acrylate rubber and a polyolefin resin compatibilized with aluminum trihydrate. The composition can be made by dynamically partially curing blends of acrylate rubber and polyolefin resin with compatibilizing amounts of aluminum trihydrate to yield a thermoplastic elastomer with improved properties at elevated temperatures. The acrylate rubber can comprise an acrylate ester polymer or a copolymer of acrylate ester with ethylene. The polyolefin resin is preferably a high molecular weight polymerization product of either ethylene or propylene, preferably propylene.

Abstract: Aqueous solutions of polygalactomannans are cross-linked with the reaction product of titanium tetrachloride and a water-soluble alcohol or diol further reacted with ammonia or a water-soluble amine. Such crosslinked products are useful in fracturing solutions for secondary oil recovery or in gel explosives.

Abstract: A filter device and apparatus for filtering liquid from a collection vessel into a receptacle vessel, including a conduit, a filter in the conduit, and a rim spaced from the filter and forming an interference fit with the interior surface of the collection vessel. The rim has a plurality of openings spaced about its periphery. The device and apparatus further include means for removably securing the conduit to the receptacle vessel and a plurality of gas return passages, arranged about the exterior of the conduit, which connect the receptacle vessel to the openings in the rim.

Abstract: An improved method and composition for repairing cementitious surfaces is provided. A polymerizable urethane composition having an excess of isocyanate groups to account for water present in the reaction environment is utilized. The method utilizes water, e.g. surface moisture, to foam the polymer and provide a long-lived repair of the surface. The method is particularly applicable in the repair of concrete roadways.

Abstract: The viscosity of thickened aqueous solutions of water-soluble polymers is reduced by the addition of alkali metal and alkaline earth metal salts of hypochlorous acid and tertiary amines. The combination of the salt and the tertiary amine is much more efficient in speed of reduction in viscosity and in the completeness of the degradation of the polymer than the use of the metal salt alone. The process of this invention is particularly useful in fracturing of oil wells.

Abstract: An apparatus for collecting sputum including: a sputum container having an open end and a closed end; and a funnel which includes a mouth at one end and a discharge portion at the other end. The discharge portion is removably attachable to the container to establish fluid communication between the funnel and the container. A cap is provided for removably covering the container opening. Further provided is a base having a top which includes a recess for receiving the closed end of the container to support at least a portion of the container above the base and a chamber with an opening at its lower end. The cap is releasably held within the chamber with the inside of the cap facing the opening.

Abstract: Laminated skin-foamed core sandwich structures characterized by an excellent stiffness and load-bearing capability to weight ratio are prepared by heating in a closed mold a sandwich construction that comprises skin layers that comprise a thermoplastic polymer having a glass transition temperature in the range of 75.degree. to 85.degree. C. and reinforcing fibers and a core that comprises a thermoplastic polymer that is compatible with the polymer in the skin layers and that has a glass transition temperature that is 10.degree. to 20.degree. C. lower than that of the polymer in the skin layers and a blowing agent at a temperature sufficient to fuse and expand the core and to fuse the skin layers and bond them to the expanded core.

Abstract: An improved method of removing a seal unit from a process vessel bottom entering agitator assembly and reinstalling a seal unit therein wherein a selectively elevatable table which is movably mounted on a pair of horizontal rails is utilized in lowering and raising seal units during the removal and reinstallation thereof.

Abstract: A plant stake and clasp is provided in which one or more clasps molded from plastic resin are provided at the top of the stake, each clasp including a pair of cooperating resilient arms and a mouth through which the stem of the plant can be introduced.

Abstract: A unitary, i.e., one-piece, flower pot is described having a water reservoir at the bottom thereof defined by a bottom wall and a soil support plate positioned above the bottom wall and being hinged to the pot along a hinge line located above the bottom wall. The soil support plate is hinged to the pot by means of the plastic resin from which the pot is formed. Through this means, the soil support plate and pot are all formed integrally from the same material with the support plate at a vertical position in alignment with the axis of the pot so that it can be removed from the mold and then swung downwardly about the hinge to a horizontal position when soil is to be placed in the pot.

Abstract: A combination flower pot and tray is described which can be quickly assembled without visually orienting the tray with respect to the pot. It includes a lug located at the center of the tray and extending upwardly therefrom and adapted to snap fit into an opening in the bottom of the pot. Three provisions are made for helping to orient or locate the tray with respect to the pot including side walls on the tray which conform generally to adjacent side walls on the pot, a cylindrical skirt on the bottom of the pot which fits telescopically into a mating wall between the side and bottom walls of the tray and a blunt conical point at the top of the lug to help guide it into the opening.

Abstract: A structure for protectively supporting and spacing rolls of web material in a multi-layer stack. The structure includes an elongated member of expandable polystyrene material having a pair of opposed surfaces. A first of the surfaces has a plurality of spaced parallel generally semi-cylindrical indentations disposed to receive rolls of web material. The radius of each of the semi-cylindrical indentations being greater than the depth of the indentation so that the rolls will be snugly retained within indentations in a pair of members and the members will be out of contact with each other. The member has a plurality of cavities located on the lateral edge surfaces thereof extending transversely of the axis of the semi-cylindrical indentation to render the expanded foam material substantially uniformly thick throughout to enhance uniform curing thereof.

Abstract: The polymerization of a monomer component that comprises vinyl chloride in an aqueous medium in the presence of a free radical generating polymerization initiator is terminated by introducing into the polymerization reaction mixture when from 70% to 95% of the monomer component has been polymerized from 0.01% to 0.10% by weight, based on the weight of the monomer component, of a chain-terminating agent that is an alkyl-substituted trisphenol, such as 1,1,3-tris(2-methyl-4-hydroxy-5-tert.butylphenyl)butane.