Patents Assigned to Polymetrix AG
  • Patent number: 11839996
    Abstract: A method for processing a mixture of recycled polyester material and a polyester prepolymer from a polyester manufacturing process, wherein a recycled polyester material is mixed with a polyester prepolymer, from a polyester manufacturing process, and treated in a bulk thermal treatment reactor (7) with a process gas which flows in a counter-current or a cross-current flow direction to the flow direction of the mixture. In this process, the process gas, before entering a catalyst vessel (14), is passed through a protective bed (11) containing a solid adsorbent material that removes high-boiling organic substances or organic substances, with a high combustion temperature, from the process gas stream.
    Type: Grant
    Filed: February 5, 2021
    Date of Patent: December 12, 2023
    Assignee: Polymetrix AG
    Inventors: Andreas Christel, Karl Schöpf
  • Patent number: 11566104
    Abstract: The present invention relates to a process for continuous production of partly crystalline polycondensate pellet material, comprising the steps of forming a polycondensate melt into pellet material; separating the liquid cooling medium from the pellet material in a first treatment space, wherein the pellets after exit from the first treatment space exhibit a temperature TGR, and crystallizing the pellet material in a second treatment space, wherein in the second treatment space fluidized bed conditions exist, and in the second treatment space the pellets are heated by supply of energy from the exterior by means of a process gas.
    Type: Grant
    Filed: June 23, 2020
    Date of Patent: January 31, 2023
    Assignee: POLYMETRIX AG
    Inventors: Andreas Christel, Brent Allan Culbert
  • Patent number: 11286365
    Abstract: A process for recycling polyolefins comprising the steps of extruding used polyolefin material, producing granules from the polyolefin material exiting from the extrusion into a liquid cooling medium, separating the cooling medium to obtain a dry polyolefin granulate, and treating the dry polyolefin granulate in a treatment space with a treatment gas, preferably by counter-current flow, immediately after separation of the cooling medium, the dry polyolefin granules still have a granule temperature (T2) which is above a temperature (T1) of the liquid cooling medium and in the range of 71° C.-200° C., preferably 80° C.-160° C., but below the melting point of the granules, and at least 75% of the dry polyolefin granules, in the treatment space, have a dry temperature (T3) which is in the range of granule temperature (T2)±20° C., but below the melting point of the granules.
    Type: Grant
    Filed: February 27, 2020
    Date of Patent: March 29, 2022
    Assignee: POLYMETRIX AG
    Inventor: Andreas Christel
  • Patent number: 10745517
    Abstract: The present invention relates to a process for continuous production of partly crystalline polycondensate pellet material, comprising the steps of forming a polycondensate melt into pellet material; separating the liquid cooling medium from the pellet material in a first treatment space, wherein the pellets after exit from the first treatment space exhibit a temperature TGR, and crystallizing the pellet material in a second treatment space, wherein in the second treatment space fluidized bed conditions exist, and in the second treatment space the pellets are heated by supply of energy from the exterior by means of a process gas.
    Type: Grant
    Filed: February 17, 2017
    Date of Patent: August 18, 2020
    Assignee: POLYMETRIX AG
    Inventors: Andreas Christel, Brent Allan Culbert
  • Patent number: 10604620
    Abstract: A method and an apparatus for solid-state polycondensation of polyesters, preferably polyethylene terephthalate and/or copolymers thereof. The method and apparatus are both characterized by a solid-state polycondensation being performed with polyester prepolymer particles in a reaction chamber in which an absolute pressure is in the range from 10 mbar to 200 mbar, and a process gas flow in the range of an R-value of 0.005 to 0.05. The polycondensation is carried out over a time of from 2 to 30 hours and at a temperature of from 180° C. to 5° below a crystalline melting point of the polyester prepolymer particles in order to achieve an intrinsic viscosity of from 0.70 to 0.95 dl/g. The R value is defined as a ratio of an hourly amount of process gas (in kg) flowing through the reaction space to an hourly amount of polymer (in kg) flowing through the reaction space: R = m ? ( gas ) ? / ? h m ? ( polymer ) ? / ? h .
    Type: Grant
    Filed: December 18, 2012
    Date of Patent: March 31, 2020
    Assignee: Polymetrix AG
    Inventor: Andreas Christel
  • Patent number: 9943817
    Abstract: An apparatus for continuous pelletization and crystallization of a polymer includes a unit for forming a polymer pellet material and cooling the pellet material in a liquid cooling medium. An after-connected drying unit has an exit opening for exporting gas and a crystallizer for crystallizing the pellet material. The crystallizer communicates via a connection line with the pre-connected unit for separating the liquid cooling medium from the pellet material and drying the pellet material. The crystallizer communicates with an inert gas tank, whereby the pressure in the crystallizer can be increased relative to the pressure in the drying unit. A related process is also disclosed.
    Type: Grant
    Filed: September 20, 2013
    Date of Patent: April 17, 2018
    Assignee: POLYMETRIX AG
    Inventors: Andreas Christel, Brent Allan Culbert, Fernando Eusebio
  • Patent number: 9133303
    Abstract: The method for the production of a polyester with improved melting properties and crystallization properties comprises the steps of (a) production of a pre-polyester melt with an average molecular weight (Mn) of 2000 to 16000 g/mol, (b) solidifying and shaping the melt into pre-polyester particles, and (c) thermally treating the pre-polyester particles in a solid phase in the presence of a transesterification catalyst whereby a molecular weight increase (?Mn) of more than 2000 g/mol occurs. In addition, the prepolyester particles have a carboxyl end group content (XCOOH) of between 0.25 and 0.6 before step c and during the thermal treatment step c, the proportion of the esterification reaction (E) to the polycondensation reaction (E+T) is between 0.5 and 1.
    Type: Grant
    Filed: January 19, 2006
    Date of Patent: September 15, 2015
    Assignee: POLYMETRIX AG
    Inventors: Andreas Christel, Allan Brent Culbert
  • Patent number: 9101963
    Abstract: A device for obtaining a material from a mixed fraction (including particles of a desired material and particles of another material with different optical properties) has a first sorting apparatus and at least two further sorting apparatuses below the first sorting apparatus. From the first sorting apparatus, a major fraction is introduced into a first further sorting apparatus and purified further there, while a minor fraction is passed into a second further sorting apparatus and processed further there.
    Type: Grant
    Filed: August 1, 2013
    Date of Patent: August 11, 2015
    Assignee: Polymetrix AG
    Inventor: Andreas Christel