Patents Assigned to Prayon
  • Patent number: 9287558
    Abstract: The invention relates to lithium-bearing iron phosphate in the form of micrometric mixed aggregates of nanometric particles, to an electrode and cell resulting therefrom and to the method for manufacturing same, which is characterized by a nanomilling step.
    Type: Grant
    Filed: December 23, 2013
    Date of Patent: March 15, 2016
    Assignee: PRAYON
    Inventors: Sébastien Patoux, Sébastien Martinet, Sébastien Launois, Alain Gourgue, Alain Germeau, Isabelle Willems
  • Patent number: 9255006
    Abstract: The invention relates to a method for producing phosphoric acid, including: attacking phosphate rock by means of sulfuric acid between 70° and 90° C. with formation of a first calcium sulfate dihydrate crystal slurry, the aqueous acid phase of said slurry having free P2O5 content between 38 and 50 wt % and free SO3 content that is less than 0.5 wt % and greater than 0.05 wt %; converting said first slurry by means of heating at a temperature greater than 90° C., thus giving rise to a second slurry formed of calcium sulfate hemihydrate crystals; and, within the second slurry, separating a produced phosphoric acid, having a free SO3 content that is less than 2%, and a calcium sulfate hemihydrate filter cake.
    Type: Grant
    Filed: December 2, 2010
    Date of Patent: February 9, 2016
    Assignee: PRAYON TECHNOLOGIES
    Inventors: Antoine Hoxha, Dorina Fati
  • Publication number: 20150259258
    Abstract: The present invention relates to an inorganic solid nutritive composition comprising at least one polyphosphate and at least one source of iron as micronutrient, wherein said composition is water-soluble and comprises an iron content of between 0.1% and 5% by weight of iron relative to the total weight of said solid composition.
    Type: Application
    Filed: September 18, 2013
    Publication date: September 17, 2015
    Applicant: PRAYON
    Inventors: Philippe Jacques Myriam Cappelle, Kurt Thierry S. Verhelst
  • Publication number: 20150251963
    Abstract: The present invention relates to an inorganic liquid nutritive composition comprising at least one aqueous phase, a polyphosphate and at least one source of iron as micronutrient, having a Ppoly/Fetotal molar ratio of between 5 and 50.
    Type: Application
    Filed: September 18, 2013
    Publication date: September 10, 2015
    Applicant: PRAYON
    Inventors: Philippe Jacques Myriam Capelle, Kurt Thierry S. Verhelst
  • Publication number: 20150099076
    Abstract: A process for manufacturing a composite material comprising a functionalization of the substrate, which comprises treatment of said substrate with at least one first alcoholic solvent, functionalization of a first powder and formation of a first colloidal sol of said functionalized first powder in a second solvent, at least one application of a layer of said first colloidal sol of said first powder to the substrate, drying of said layer of said first colloidal sol and formation of a layer of first coating formed by said first colloidal sol, adherent to said substrate, by heating at a temperature above 50° C. and below 500° C.
    Type: Application
    Filed: May 16, 2013
    Publication date: April 9, 2015
    Applicant: PRAYON SA
    Inventors: Dimitri Liquet, Carlos Alberto Paez, Cedric Calberg, David Eskenazi, Jean-Paul Pirard, Benoit Heinrichs
  • Publication number: 20140377138
    Abstract: A method and device for producing polyphosphoric acid burns a fuel in combustion air in a combustion chamber, sprays a spray fluid comprising substantially pure orthophosphoric acid and undertakes polymerization-condensation of the pure orthophosphoric acid. A polyphosphoric acid in the form of an acid mist accompanied by formation of gases which mix with combustion gases resulting from burning of the fuel is formed to reach a predetermined temperature, wherein the mixture causes sudden lowering of combustion gas temperature. The acid mix is separated from the gas mixture and the polyphosphoric acid is collected at a bottom of the combustion chamber and the gas mixture is outputted via a lower part of the combustion chamber separate from the collection of polyphosphoric acid.
    Type: Application
    Filed: September 11, 2014
    Publication date: December 25, 2014
    Applicant: PRAYON TECHNOLOGIES
    Inventors: Alain Germeau, Bernard Heptia
  • Patent number: 8845990
    Abstract: A method and device for producing polyphosphoric acid burns a fuel in combustion air in a combustion chamber, sprays a spray fluid comprising substantially pure orthophosphoric acid and undertakes polymerization-condensation of the pure orthophosphoric acid. A polyphosphoric acid in the form of an acid mist accompanied by formation of gases which mix with combustion gases resulting from burning of the fuel is formed to reach a predetermined temperature, wherein the mixture causes sudden lowering of combustion gas temperature. The acid mix is separated from the gas mixture and the polyphosphoric acid is collected at a bottom of the combustion chamber and the gas mixture is outputted via a lower part of the combustion chamber separate from the collection of polyphosphoric acid.
    Type: Grant
    Filed: March 25, 2010
    Date of Patent: September 30, 2014
    Assignee: Prayon Technologies
    Inventors: Alain Germeau, Bernard Heptia
  • Publication number: 20140155359
    Abstract: A clear and nutritive microemulsion comprising an aqueous phase in which at least one liposoluble active ingredient is dispersed, a first surfactant included in the group consisting of non-ionic surfactants with a high HLB and non-ionic surfactants with medium HLBs; and a second surfactant, characterized in that said second surfactant is chosen from the group consisting of anionic surfactants which have an HLB ?25.
    Type: Application
    Filed: July 13, 2012
    Publication date: June 5, 2014
    Applicant: PRAYON
    Inventors: Guy Broze, Claire Pucci, Adeline Navarro
  • Publication number: 20140120020
    Abstract: A method for producing phosphoric acid, comprising attack in an aqueous medium of phosphated rock with sulfuric acid, with formation of a first dihydrate slurry suspended in an aqueous phase having a free P2O5 content between 38 and 50% and a free SO3 content of less than 0.5%, conversion of this first slurry by heating with recrystallization of the solubilized calcium sulfate giving rise to a second hemihydrate slurry, and separation in the second slurry between a production phosphoric acid and a hemihydrate cake, characterized in that it comprises during the attack, addition of a fluorine source in the first slurry in a content from 1% to 5% by weight of F relatively to the P2O5 contained in the phosphated rock.
    Type: Application
    Filed: June 1, 2011
    Publication date: May 1, 2014
    Applicant: PRAYON TECHNOLOGIES
    Inventors: Antoine Hoxha, Dorina Fati
  • Patent number: 8703332
    Abstract: The invention relates to lithium-bearing iron phosphate in the form of micrometric mixed aggregates of nanometric particles, to an electrode and cell resulting therefrom and to the method for manufacturing same, which is characterized by a nanomilling step.
    Type: Grant
    Filed: January 28, 2011
    Date of Patent: April 22, 2014
    Assignees: Prayon, Commissariat à l'Énergie Atomique
    Inventors: Sébastien Patoux, Sébastien Martinet, Sébastien Launois, Alain Gourgue, Alain Germeau, Isabelle Willems
  • Publication number: 20130095150
    Abstract: Stable solid compositions have a first carrier and an adsorbate having at least one active component, such as, a vitamin D derivative and a hydrophobic stabilizer thereof, wherein the first carrier is a calcium phosphate or derivatives thereof having a solubility in water lower than 0.1 wt % at room temperature.
    Type: Application
    Filed: June 24, 2011
    Publication date: April 18, 2013
    Applicant: PRAYON S.A.
    Inventors: Khadija Tantaoui Elaraqi, Guy Broze, Audrey Leruite
  • Patent number: 8206587
    Abstract: The invention relates to a filtration cell that comprises a tank with a bottom wall (2) and four side walls extending upwards from the bottom wall as well as an upward opening, the four side walls including two opposite longitudinal walls (3, 5) as well as a front facing wall (4) and a rear facing wall connecting them, a filtration bed (7) supported in the tank, an outlet opening for discharging the filtrate, and a covering flap (24) protruding outwards from the top of one of said longitudinal walls, the longitudinal wall (5) opposed to that fitted with the flap including a lower portion (25) extending upwards from the bottom wall (2) and an upper portion (26) extending slantedly upwards and inside the tank from the top of said lower portion (25), and/or the front facing wall (4) comprises a bottom portion (27) extending upwards from the bottom wall (2) and a top portion (28) extending slantedly upwards and inside the tank from the top of said bottom portion (27).
    Type: Grant
    Filed: March 6, 2008
    Date of Patent: June 26, 2012
    Assignee: Prayon Technologies
    Inventor: Serge Kurowski
  • Publication number: 20040089599
    Abstract: A continuous fluid filtration device having filtration cells disposed in a carousel around a rotation axis so as to be able to pivot about a tilt axis including apparatus for discharging the filtrate from the cells with at least one outlet orifice at the bottom of each cell, a central collector and a connection allowing flow of the filtrate between the outlet orifice and the collector, where the connection for each cell includes a flexible conduit in which, in the filtration position of the cell, no area of the flexible conduit is lower than another area of the conduit situated downstream with respect to the flow of the filtrate, the flexible conduit being arranged so as not to undergo any elongation during tilting of the cell.
    Type: Application
    Filed: October 29, 2003
    Publication date: May 13, 2004
    Applicant: PRAYON TECHNOLOGIES
    Inventor: Serge Kurowski
  • Patent number: 4777027
    Abstract: There is described a process which comprises adjusting on the one hand the flow rates of a circulating mixture relative to a base flow rate according to very specific specifications, and on the other hand so adjusting the reaction conditions in succeeding reaction zones as to obtain a production phosphoric acid with a P.sub.2 O.sub.5 concentration between 33 and 52%, and a H.sub.2 SO.sub.4 concentration between 0.25 and 2.5%, and calcium sulphate in the form of dihydrate, hemihydrate, anhydrite or a mixture of at least two said crystalline forms.
    Type: Grant
    Filed: October 29, 1985
    Date of Patent: October 11, 1988
    Assignee: Prayon Developpment, Societe Anonyme
    Inventors: Armand L. Davister, Francis A. Thirion
  • Patent number: 4752390
    Abstract: Vacuum rotary filter with horizontal filtering plane comprising a distributor consisting of a distributor part, a collector part and a gas separation chamber. The collector part (110) consists of a single vat divided into three compartments (139, 140, 141, respectively), for the mother water, the first washing liquid and the second washing liquid. The compartments may be interconnected so as to enable a fluid circulation in an imposed direction. The collector part also comprises a sector for annex operations and presuction.
    Type: Grant
    Filed: November 14, 1985
    Date of Patent: June 21, 1988
    Assignee: Prayon Developpement S.A.
    Inventors: Georges-Francois Martin, Armand L. Davister
  • Patent number: 4588570
    Abstract: The present invention provides a continuous method for preparing phosphoric acid and calcium sulphate by reacting calcium phosphate with a mixture of sulphuric acid and phosphoric acid. Our method uses at least three successive crystallization steps: a first step of reacting the phosphate with the mixture of phosphoric and sulphuric acids and forming a-hemihydrate calcium sulphate, a second step of recrystallizing the a-hemihydrate into dihydrate and a third step of transforming the dehydrated calcium sulfate into a hemihydrate or anhydrite II or a mixture of the two. Where desired recycling of the products from the above steps can be used for increasing the efficiency of the above method.
    Type: Grant
    Filed: November 20, 1984
    Date of Patent: May 13, 1986
    Assignee: Prayon Development
    Inventors: Armand L. Davister, Andre R. Dubreuco, Francis A. Thirion
  • Patent number: 4330404
    Abstract: A cell filter having a series of filtering cells and a distributor for collecting and adjusting the distribution of fluids passing through the cell filtering surface. Each cell has a planar filtering bed composed of a filtering cloth bearing on a rigid apertured support. Fluid passes through the cloth onto the cell bottom which slants toward a drain channel. The drain channel slants toward a discharge duct connected to a distributor. Guide members in the distributor fractionate, divide, and direct the fluid flowing towards the discharge duct into two parallel adjacent streams. The guide members are a series of baffle plates, located along the top length of the drain channel. The baffle plates are slanted, the plate farthest from the low end of the drain channel having the steepest slant.
    Type: Grant
    Filed: August 21, 1978
    Date of Patent: May 18, 1982
    Assignee: Societe de Prayon
    Inventor: Armand L. Davister
  • Patent number: 4252775
    Abstract: The present invention relates to a process for treating residues from a primary leaching of ferriferous zinc ores by sulphuric acid, with a view to recover a leadbearing by-product, such process comprising a secondary leaching of said residues, by sulphuric acid, within several countercurrent stages, at a temperature comprised between 85.degree. and 100.degree. C., the solid residues of the successive stages being circulated from the first to the last stage, the residue of this last stage being the said lead bearing by-product, whereas the various solutions separated from the second to the last stage are each recycled within the leaching operation of the respectively foregoing stage, and the dual zinc and iron sulphates solution, as separated from the first stage, being the principal product of the treatment.
    Type: Grant
    Filed: December 29, 1978
    Date of Patent: February 24, 1981
    Assignee: Societe de Prayon
    Inventors: Armand L. Davister, Wilhem E. Pavonet, Renaud F. Quatpers
  • Patent number: 4188366
    Abstract: A multi-compartment reaction system for the manufacture of phosphoric acid by the wet process having a recirculation slurry flash cooler. The removal of heat from the reaction system is accomplished by circulating reaction zone slurry through an elevated vacuum flash cooler under the combined effect of differential liquid levels maintained in the system, and the vacuum in the flash cooler. The amount of reaction zone slurry passed to the flash cooler is sufficiently large so that the temperature differential experienced by the slurry is low and crystallization of calcium sulfate from the slurry liquid occurs in a favorable manner. There is also a substantial reduction in the pumping requirements compared with conventional operations in which the slurry is pumped to an elevated flash cooler, even though the large amount of slurry is passed to the flash cooler in accordance with the invention.
    Type: Grant
    Filed: November 18, 1977
    Date of Patent: February 12, 1980
    Assignee: Societe de Prayon
    Inventor: Samuel V. Houghtaling
  • Patent number: 4176160
    Abstract: Process for purifying an iron containing zinc sulfate solution which comprises precipitating iron from said solution as a slurry in at least one of the following forms at a pH which is maintained lower than 4: basic sulfate, jarosite or goethite; filtering said slurry on a planar horizontal filter and forming a cake on said planar filter; washing the cake directly on the planar filter with water supplied onto the cake without forming a newslurry with washing water and thus freeing the cake from water soluble zinc and copper compounds promptly before hydrolysis thereof insolubilizes said compounds as basic sulfates, whereby the solid residue in the cake does not contain substantially more insoluble zinc content than it contained in the slurry being fed to the filtration.
    Type: Grant
    Filed: March 6, 1978
    Date of Patent: November 27, 1979
    Assignee: Societe de Prayon
    Inventor: Engelhard Pavonet