Patents Assigned to QILU UNIVERSITY OF TECHNOLOGY
  • Patent number: 12043834
    Abstract: The present disclosure relates to a method for constructing a trehalose polyenzyme complex in vitro by mediation of an artificial scaffold protein, which mainly comprises the following steps: constructing a recombinant bacterium WB800n-ScafCCR for self-assembled scaffold protein module; constructing a recombinant bacterium WB800n-P43-phoD -treY-Ccdoc for self-assembled catalytic module; constructing a recombinant bacterium WB800n-P43-phoD-treZ-Ctdoc for self-assembled catalytic module; constructing a recombinant bacterium WB800n-P43-phoD-cgt-Rfdoc for self-assembled catalytic module; secretorily expressing the recombinant bacteria and self-assembling in vitro to obtain a recombinant trehalose multi-enzyme complex. The trehalose multi-enzyme complex constructed by the method of the present disclosure has a higher catalytic efficiency in preparing trehalose than that of mixed free enzymes, and the method can be used for production of high quality trehalose after immobilization with cellulose microspheres.
    Type: Grant
    Filed: November 12, 2021
    Date of Patent: July 23, 2024
    Assignee: Qilu University of Technology
    Inventors: Hongling Liu, Tengfei Wang, Ruiming Wang, Xinyi Zhang
  • Patent number: 12037293
    Abstract: A laminated cermet tool material with self generated micro texture on the surface and a preparation method thereof; first, the tungsten carbide titanium matrix powder is added with molybdenum cobalt nickel rare metal as the bonding phase to form the matrix, then 2.5D braided ceramic fiber preforms are placed on the upper and lower surfaces of the cermet matrix powder, and the laminated cermet tool material with self generated micro texture on the surface is obtained by spark plasma sintering, as the ceramic fiber braid is braided, it has a stable structure, realizing the formation of texture coating on the surface of the tool, and the laminated tool with the cermet as the middle layer.
    Type: Grant
    Filed: May 15, 2023
    Date of Patent: July 16, 2024
    Assignee: Qilu University of Technology
    Inventors: Mingdong Yi, Jianping Wang, Chonghai Xu, Zhaoqiang Chen, Guangchun Xiao
  • Patent number: 12014149
    Abstract: Disclosed is a multi-turn human-machine conversation method and apparatus based on a time-sequence feature screening encoding module, belonging to the technical field of natural language processing and artificial intelligence. The technical problem to be solved by the disclosure is how to screen information for each utterance in a historical conversation so as to obtain semantic information only relevant to candidate responses and how to reserve and extract time-sequence features in the historical conversation, thus improving prediction accuracy of a multi-turn human-machine conversation system.
    Type: Grant
    Filed: August 24, 2023
    Date of Patent: June 18, 2024
    Assignee: Qilu University of Technology (Shandong Academy of Sciences)
    Inventors: Dongfeng Li, Peng Ji, Wanlong Dong
  • Patent number: 11999957
    Abstract: A method of enhancing vanillin resistance of Saccharomyces cerevisiae, including: knocking out SNG1 gene from a genome of Saccharomyces cerevisiae. This application further provides a mutant of SNG1 gene of Saccharomyces cerevisiae including the nucleotide sequence shown in SEQ ID NO: 1, where the sequence shown in SEQ ID NO: 1, from left to right, consists of a ?18˜+203 bp fragment of SNG1 gene of Saccharomyces cerevisiae, a nucleotide fragment of loxp-KanMX4-loxp and a +1446˜+1644 bp fragment of the SNG1 gene of Saccharomyces cerevisiae.
    Type: Grant
    Filed: December 10, 2020
    Date of Patent: June 4, 2024
    Assignee: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Xiaoming Bao, Liyun Song, Xinning Wang, Wenyan Cao, Weiquan Zhao, Zailu Li
  • Publication number: 20240173887
    Abstract: An ultra-fast sintering method and a sintering system for preparing nano-ceramics by ultrasonic-assisted pressurization and high-frequency induction, it belongs to the technical field of nano-ceramics sintering; this method mainly aims at the problem that nano-ceramics are easy to grow during sintering, and develops an ultrasonic-assisted pressurized coupled high-frequency induction sintering system to prepare nano-ceramic materials; in the process of sintering, ultrasonic wave is used to form high frequency, alternating impact and cavitation on nano-ceramic particles, which can quickly exhaust the gas between particles and inhibit the agglomeration of nano-ceramic particles; on the other hand, the rapid sintering of nano-ceramics is realized by using the principle of high-frequency induction to instantaneously heat the graphite mold and generate a lot of heat.
    Type: Application
    Filed: July 18, 2023
    Publication date: May 30, 2024
    Applicant: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Mingdong Yi, Gang Xue, Wenjie Liu, Kaining Liu, Wen Zhang, Yuchen Xu, Chenyang Yi, Chonghai Xu
  • Patent number: 11967180
    Abstract: A dynamic facial expression recognition (FER) method based on a Dempster-Shafer (DS) theory improves a feature extraction effect of an expression video through multi-feature fusion, and deeply learns an imbalanced dynamic expression feature by using the DS theory, multi-branch convolution, and an attention mechanism. Compared with other methods, the dynamic FER method scientifically and effectively reduces an impact of sample imbalance on expression recognition, fully utilizes a spatio-temporal feature to mine potential semantic information of the video expression to perform expression classification, thereby improving reliability and accuracy and meeting a demand for the expression recognition.
    Type: Grant
    Filed: October 18, 2023
    Date of Patent: April 23, 2024
    Assignees: QILU UNIVERSITY OF TECHNOLOGY (SHANDONG ACADEMY OF SCIENCES), SHANDONG COMPUTER SCIENCE CENTER (NATIONAL SUPERCOMPUTING CENTER IN JINAN)
    Inventors: Minglei Shu, Zhenyu Liu, Zhaoyang Liu, Shuwang Zhou, Pengyao Xu
  • Patent number: 11946246
    Abstract: The present invention provides an energy-storing temperature control material, and belongs to the technical field of temperature control materials. In the energy-storing temperature control material provided in the present invention, the organic synthetic fiber based phase-change material has a three-dimensional dispersion effect, and can form a network constraint for remaining phase-change materials to reinforce mechanical properties of the materials, thereby fixing shapes of the materials and avoiding a liquid-crystal phase separation phenomenon in the phase-change process. The phase-change energy storage agent can absorb and release the heat by means of solid-liquid phase conversion of the material, to achieve the temperature control effect; and the phase-change temperature regulator can regulate a phase-change temperature range of the phase-change material, to make the energy-storing temperature control material suitable for climatic features of northern China.
    Type: Grant
    Filed: August 9, 2022
    Date of Patent: April 2, 2024
    Assignee: Qilu University of Technology
    Inventors: Letian Qi, Shoujuan Wang, Xia Meng, Fangong Kong, Ruhe Zhao, Chen Han, Debao Li
  • Publication number: 20240051021
    Abstract: Provided a method for in situ synthesizing ultrafine and highly loaded Ag NPs on the surface of tannin-coated phenolic resin microspheres, the method comprises: (1) preparing phenolic resin microspheres by hydrothermal solvent method; (2) stirring a mixed phase of the phenolic resin microspheres and a tannin solution under a alkaline condition at room temperature to obtain tannin-coated phenolic resin microspheres; (3) adding the tannin-coated phenolic resin microspheres to a silver ammonia solution to obtain a composite that being loaded with Ag NPs on the surface of tannin-coated phenolic resin microspheres. Ag NPs in the composite are ultrafine and highly loaded. The raw materials of the method are low price, and the preparation process is extremely simple and environmentally friendly. In addition, the tannin coating technology is also suitable for other nanomaterials, such as SiO2, TiO2 and Fe3O4, etc., and has good application prospects and market potential.
    Type: Application
    Filed: September 28, 2021
    Publication date: February 15, 2024
    Applicant: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Weikun JIANG, Shuo ZHANG, Yu LIU, Guolong LIU, Honglei CHEN
  • Patent number: 11860608
    Abstract: The present invention discloses an industrial equipment operation, maintenance and optimization method and system based on a complex network model. The method includes the following steps: obtaining data of all sensors of industrial equipment, and calculating a Spearman correlation coefficient between data of every two of the sensors within the same time period; using each sensor as a node, and using the Spearman correlation coefficient as a weight of a network edge, to construct a fully connected weighted network; and obtaining, when an adjustment instruction for a target feature is received, a currently optimal parameter adjustment path of the target feature based on the fully connected weighted network. In the present invention, production equipment in reality is digitized to construct a complex network oriented to industrial big data. An optimal path for equipment parameter tuning may be found by using the network, thereby reducing dependence of an enterprise on a domain expert.
    Type: Grant
    Filed: January 3, 2020
    Date of Patent: January 2, 2024
    Assignee: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Xuesong Jiang, Chao Meng, Xiumei Wei, Qingcun Zhu, Dapeng Hu
  • Patent number: 11834784
    Abstract: The present disclosure relates to a method for preparing an unbleached biomechanical pulp and fully utilizing by-products by treating wheat straws with heat steam in synergy with biological enzymes, which belongs to the technical field of papermaking technology and waste comprehensive utilization. The present disclosure provides a method for preparing an unbleached biomechanical pulp by treating whole wheat straws with heat steam in synergy with biological enzymes, where the prepared high-strength biomechanical pulp can meet the requirements of producing unbleached packaging paper and paper-based materials. At the same time, the by-products are recycled to prepare a biomass compound fertilizer, which turns solid waste into treasure and realizes the high-value full utilization of wheat straw. Therefore, the method in the present disclosure is simple, green, clean and efficient, which has good practical application value and broad application prospects.
    Type: Grant
    Filed: December 23, 2021
    Date of Patent: December 5, 2023
    Assignee: Qilu University of Technology
    Inventors: Xingxiang Ji, Jiachuan Chen, Zhongjian Tian, Ruiming Wang, Dongxing Wang, Yu Liu
  • Publication number: 20230340225
    Abstract: A method for manufacturing a flexible sensor, including: dispersing graphene in a polymeric material; adding a carbon nanotube into the polymeric material; applying an alternating electric field to the polymeric material added with the carbon nanotube to obtain a composite material; attaching a polymeric material film to the obtained composite material; pre-embedding carbon fibers; and heating and curing to obtain a sensor. A CNT bridging effect and an electric field induced arrangement are introduced at an appropriate ratio of polymeric materials such as graphene-PDMS or PMMA to improve a dry-blended method. The flexible sensor manufactured by the improved dry-blended method improves electrical conductivity, a piezoresistive property and a mechanical property of CNT-graphene-PDMS or PMMA and other polymeric materials.
    Type: Application
    Filed: July 3, 2023
    Publication date: October 26, 2023
    Applicant: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Li WANG, Jun CHEN, Weiguang SU, Chonghai XU, Wenhong ZHANG, Junlei HAN, Xingyuan XU
  • Patent number: 11795533
    Abstract: A heat-resistant and soluble magnesium alloy, and a preparation method having an elemental composition at the following atomic percentage: Lu 0.10% to 8.00%, Ce 0.001 to 0.05%, Al 0.10% to 0.60%, Ca 0.001% to 0.50%, Cu 0.01% to 1.00%, Ni 0.01% to 1.00%, impurity elements <0.30%, and the rest is Mg, and formed in magnesium alloys are high temperature phase of Lu5Mg24, Mg2Cu, Mg2Ni, Mg12Ce, Al11Ce3 and (Mg, Al)2Ca, and Long Period Stacking Ordered (LPSO) phases as Mg—Lu—Al and Mg—Ce—Al. The magnesium alloy has good mechanical performances at 150° C., and a dissolution rate of 30 to 100 mg·cm?2h?1 in a 3% KCl solution at 93° C.
    Type: Grant
    Filed: May 13, 2020
    Date of Patent: October 24, 2023
    Assignees: QILU UNIVERSITY OF TECHNOLOGY, ADVANCED MATERIALS INSTITUTE, SHANDONG ACADEMY OF SCIENCES
    Inventors: Jixue Zhou, Yunteng Liu, Dongqing Zhao, Baichang Ma, Meifang Wang, Peiliang Li, Cong Liu, Shouqiu Tang
  • Patent number: 11744903
    Abstract: A method for preparing a cyclodextrin metal organic framework (CD-MOF) stable in aqueous phase, including: dissolving ?-cyclodextrin and solid potassium hydroxide in deionized water followed by magnetic stirring and ultrasonic treatment at room temperature, addition of methanol and stirring to obtain a reaction mixture; filtering the reaction mixture with a polytetrafluoroethylene membrane filter in a beaker; placing the beaker in methanol vapor to form a ?-CD-MOF crystal; washing the ?-CD-MOF crystal with ethanol followed by centrifugation and vacuum drying to obtain ?-CD-MOF; preparing a ?-CD-MOF-active substance complex by impregnation; and preparing an active substance-loaded ?-CD-MOF-Tween 80 complex by physical adsorption modification followed by washing with anhydrous ethanol and vacuum drying.
    Type: Grant
    Filed: March 22, 2023
    Date of Patent: September 5, 2023
    Assignee: Qilu University of Technology
    Inventors: Chao Yuan, Bo Cui, Meng Zhao, Lu Lu, Jianpeng Li, Yaqi Liu
  • Patent number: 11746368
    Abstract: The present invention provides a Lactococcus lactis subsp. lactis A32, derived product and use thereof, the present invention falls in the technical field of microorganisms. In the present invention, the Lactococcus lactis subsp. lactis A32 is obtainable by compound mutation on the basis of the original strain L. lactis lxl. Experiments showed that, compared with nisin titre of the original strain L. lactis lxl, the Lactococcus lactis subsp. lactis A32 has high nisin yield, and the nisin titre has been improved for 3˜4 times (over 5066.58 IU/mL); in the meanwhile, the growth curve of the Lactococcus lactis subsp. lactis A32 is slightly longer than the original strain L. lactis lxl and biomass peaks of them are basically consistent. The present invention has laid a foundation for large scale production of nisin.
    Type: Grant
    Filed: September 2, 2022
    Date of Patent: September 5, 2023
    Assignee: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Deqiang Zhu, Xinli Liu, Yujie Lian, Leshan Han, Shuo Peng
  • Patent number: 11749467
    Abstract: A carbon cloth/gallium oxynitride has a chemical formula of GaOxNy, where x=0.1-0.3 and y=0.7-0.9; and has a N/O molar ratio of 2.3 to 9. The carbon cloth/gallium oxynitride is a composite formed by loading gallium oxynitride nanoparticles on carbon cloth fibers, wherein the gallium oxynitride nanoparticles have a size range of 10 to 70 nm, and the carbon cloth/gallium oxynitride has a discharge specific capacitance of 30 to 865 mF cm?2 at current densities ranging from 0.5 to 100 mA cm?2. The working electrode is made from the carbon cloth/gallium oxynitride; and the supercapacitor is composed of the carbon cloth/gallium oxynitride working electrodes, a separator, an electrolyte, and an outer package.
    Type: Grant
    Filed: November 3, 2021
    Date of Patent: September 5, 2023
    Assignee: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Ligang Gai, Qing Ban, Jiayu Wang, Haihui Jiang, Libin Liu
  • Patent number: 11734435
    Abstract: In the field of image encryption and decryption, in order to solve the problem of small key space in the encryption process caused by low dimension of one-dimensional chaotic map and few initial values and control parameters, the present disclosure provides an image encryption and decryption communication algorithm based on two-dimensional lag complex Logistic map, which expands the variables of one-dimensional Logistic map from the real number domain to the complex number domain, improves the dimension of the mapping system, increases the number of keys, and expands the mapping range, wherein the new mapping system is more sensitive to small disturbances of initial values and parameters, which can break the strong correlation between pixels in the original image, so that the pixels of the encrypted image are uniformly distributed in the whole plane, and the features of the original image are hidden.
    Type: Grant
    Filed: May 13, 2021
    Date of Patent: August 22, 2023
    Assignee: Qilu University of Technology
    Inventors: Fangfang Zhang, Fengying Ma, Maoyong Cao, Xue Zhang, Zhengfeng Li
  • Patent number: 11710604
    Abstract: A supercapacitor contains the zwitterionic polymer hydrogel electrolyte. A change rate of a capacitance retention of the supercapacitor, relative to a specific area capacity at 25° C. is less than 25% at extreme temperature. When temperature is increased to 60° C. or reduced to ?30° C. the specific area capacity is changed to 178 mF cm?2 and 134 mF cm?2, which are 104% and 78% of that at 25° C. indicating an excellent electrochemical property at the extreme temperature.
    Type: Grant
    Filed: November 3, 2021
    Date of Patent: July 25, 2023
    Assignee: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Libin Liu, Jianbo Yang, Qing Ban, Ligang Gai, Xuelin Li, Mei Li
  • Publication number: 20230185865
    Abstract: A personalized comment recommendation method based on a link prediction model of a graph bidirectional aggregation network. In a user-comment bipartite graph, comment features are aggregated into a user feature. A social network is used to fuse a neighbor feature of a user to obtain an embedding representation of the user. The embedding representation of the user is aggregated into a comment after an original feature of the user is removed, and the embedding representation of the user is adjusted based on a difference before and after comment aggregation. On this basis, a forwarding network is used to calculate a score of an edge based on an inner product of user node features at both ends of the edge, and finally make a recommendation based on the score. Furthermore, a recommendation system converts a comment recommendation task into a link prediction task between users in a small range.
    Type: Application
    Filed: February 6, 2023
    Publication date: June 15, 2023
    Applicants: SHANDONG ARTIFICIAL INTELLIGENCE INSTITUTE, QILU UNIVERSITY OF TECHNOLOGY, SHANDONG COMPUTER SCIENCE CENTER (NATIONAL SUPERCOMPUTER CENTER IN JINAN)
    Inventors: Minglei SHU, Muchen WANG, Yinglong WANG, Zhao LI, Tianlei GAO
  • Publication number: 20230183853
    Abstract: A bismuth ferrite film material, a method for integrally preparing a bismuth ferrite film on a silicon substrate at a low temperature, and an application, includes: magnetron sputtering a bottom electrode, a buffer layer and a bismuth ferrite film on one surface of a Si substrate in sequence from bottom to top at a processing temperature of 300-400° C.; reducing the temperature to room temperature; and a top electrode is deposited via magnetron sputtering on the surface of the bismuth ferrite film; the buffer layer mentioned hereof is a conductive oxide which matches the lattice of bismuth ferrite and is of a perovskite structure (AB03). According to the present invention, the temperature for preparing the bismuth ferrite film material can be reduced to 450° C. or below, and the bismuth ferrite film material has a high spontaneous electric polarization.
    Type: Application
    Filed: July 13, 2020
    Publication date: June 15, 2023
    Applicant: QILU UNIVERSITY OF TECHNOLOGY
    Inventor: Jun OUYANG
  • Publication number: 20230152786
    Abstract: The present invention discloses an industrial equipment operation, maintenance and optimization method and system based on a complex network model. The method includes the following steps: obtaining data of all sensors of industrial equipment, and calculating a Spearman correlation coefficient between data of every two of the sensors within the same time period; using each sensor as a node, and using the Spearman correlation coefficient as a weight of a network edge, to construct a fully connected weighted network; and obtaining, when an adjustment instruction for a target feature is received, a currently optimal parameter adjustment path of the target feature based on the fully connected weighted network. In the present invention, production equipment in reality is digitized to construct a complex network oriented to industrial big data. An optimal path for equipment parameter tuning may be found by using the network, thereby reducing dependence of an enterprise on a domain expert.
    Type: Application
    Filed: January 3, 2020
    Publication date: May 18, 2023
    Applicant: QILU UNIVERSITY OF TECHNOLOGY
    Inventors: Xuesong JIANG, Chao MENG, Xiumei WEI, Qingcun ZHU, Dapeng HU