Patents Assigned to QUANTEX RESEARCH CORPORATION
  • Patent number: 10301549
    Abstract: A method of depolymerizing coal includes preparing a high temperature depolymerizing medium consisting of heavy hydrocarbon oils and mixing it with coal to form a mixture, performing an optional first distillation at a temperature below 250° C. to recover naphthalene, heating the mixture to a temperature between 350° C. and 450° C. to create a digested coal, centrifuging the digested coal to remove ash and obtain a centrate, and distillation of the centrate into separate fractions. The high temperature depolymerizing medium may be a heavy hydrocarbon with a hydrogen to carbon (H/C) ratio higher than 7.0% and may include liquids chosen from the group consisting of: coal tar distillate, decant oil, anthracene oil, and heavy aromatic oils. The high temperature depolymerizing medium may be blended with an oil, preferably with H/C ratio higher than 10.
    Type: Grant
    Filed: November 14, 2017
    Date of Patent: May 28, 2019
    Assignee: QUANTEX RESEARCH CORPORATION
    Inventors: Elliot B. Kennel, Gilbert A. Chalifoux
  • Patent number: 9845431
    Abstract: A method of depolymerizing coal includes preparing a high temperature depolymerizing medium consisting of heavy hydrocarbon oils and mixing it with coal to form a mixture, performing an optional first distillation at a temperature below 250° C. to recover naphthalene, heating the mixture to a temperature between 350° C. and 450° C. to create a digested coal, centrifuging the digested coal to remove ash and obtain a centrate, and distillation of the centrate into separate fractions. The high temperature depolymerizing medium may be a heavy hydrocarbon with a hydrogen to carbon (H/C) ratio higher than 7.0% and may include liquids chosen from the group consisting of: coal tar distillate, decant oil, anthracene oil, and heavy aromatic oils. The high temperature depolymerizing medium may be blended with an oil, preferably with H/C ratio higher than 10.
    Type: Grant
    Filed: November 22, 2016
    Date of Patent: December 19, 2017
    Assignee: QUANTEX RESEARCH CORPORATION
    Inventors: Elliot B. Kennel, Gilbert A. Chalifoux
  • Patent number: 9534176
    Abstract: A method of depolymerizing coal includes preparing a high temperature depolymerizing medium consisting of heavy hydrocarbon oils and mixing it with coal to form a mixture, performing an optional first distillation at a temperature below 250° C. to recover naphthalene, heating the mixture to a temperature between 350° C. and 450° C. to create a digested coal, centrifuging the digested coal to remove ash and obtain a centrate, and distillation of the centrate into separate fractions. The high temperature depolymerizing medium may be a heavy hydrocarbon with a hydrogen to carbon (H/C) ratio higher than 7.0% and may include liquids chosen from the group consisting of: coal tar distillate, decant oil, anthracene oil, and heavy aromatic oils. The high temperature depolymerizing medium may be blended with an oil, preferably with H/C ratio higher than 10.
    Type: Grant
    Filed: December 11, 2015
    Date of Patent: January 3, 2017
    Assignee: QUANTEX RESEARCH CORPORATION
    Inventors: Elliot B. Kennel, Gilbert A. Chalifoux
  • Publication number: 20120097519
    Abstract: The present disclosure provides methods and systems of a coated coker. An apparatus for coking includes a coated coking drum that receives a pitch material, wherein the coking drum is coated with a coating comprising at least one of a chromium, an aluminum, a nickel, or an alloy thereof, a heater that heats the pitch material to a coking temperature, and a flash vessel that condenses a liberated volatile matter, wherein a coke formed in the apparatus is readily removable. A coated Archimedes screw or coated plunger may be used with the coker, both of which can remove coke from the coking drum via force of their movement inside the coking drum.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 26, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventor: Alfred H. Stiller
  • Publication number: 20120097579
    Abstract: The present disclosure provides methods and systems for coal liquefaction and obtaining a mesophase pitch. A method of obtaining a quinolone insoluble-free and ash-free mesophase pitch may include exposing a coal to a hydrogenated vegetable oil in the presence of a coal-derived solvent to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, separating the insoluble components from the slurry to obtain a de-ashed coal extract that is quinoline insoluble-free, and distilling the coal extract under vacuum to obtain a mesophase pitch with a softening point in the range of 25 degrees Celsius to 160 degrees Celsius, wherein the mesophase pitch can be coked to obtain an anisotropic coke.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 26, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventors: Alfred H. Stiller, Peter G. Stansberry
  • Publication number: 20120097580
    Abstract: The present disclosure provides methods and systems for coal liquefaction and obtaining a obtaining a high quality coke from a low rank coal extract. A method of obtaining a high quality coke from a low rank coal extract may include exposing a coal to a hydrogenated vegetable oil in the presence of a coal-derived solvent to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, separating the insoluble components from the slurry to obtain a de-ashed coal extract that is quinoline insoluble-free, distilling the coal extract under vacuum to obtain a pitch with a suitable softening point, and coking the pitch to obtain a coke. The coke may be at least one of an anisotropic coke, a metallurgical coke, a graphite coke, an anode coke, and a needle coke.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 26, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventor: Alfred H. Stiller
  • Publication number: 20120090510
    Abstract: The present disclosure provides methods and systems for coal liquefaction and obtaining a cement by-product. A method of obtaining a cement by-product of coal liquefaction may include exposing a coal to a hydrogenated vegetable oil in the presence of a coal-derived solvent to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, separating the insoluble components from the slurry, heating the insoluble components to liberate a volatile matter and an entrained solvent, blending the insoluble components with a calcareous material and roasting the blend in a kiln at a temperature greater than 1000 degrees Celsius to obtain a clinker, and grinding the clinker to obtain a cement.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 19, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventor: Alfred H. Stiller
  • Publication number: 20120091042
    Abstract: The present disclosure provides methods and systems for coal liquefaction using a hydrogenated vegetable oil. A method of obtaining a de-ashed coal extract includes exposing a coal to a hydrogenated vegetable oil in the presence of a coal-derived solvent to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, and separating the insoluble components from the slurry to obtain a de-ashed coal extract, wherein the coal extract is suitable for downstream processing.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 19, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventors: Alfred H. Stiller, Elliot B. Kennel
  • Publication number: 20120091044
    Abstract: The present disclosure provides methods and systems for coal liquefaction using a sewage material. A method of obtaining a de-ashed coal extract includes exposing a coal to a sewage material in the presence of a coal-derived solvent to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, and separating the insoluble components from the slurry to obtain a de-ashed coal extract, wherein the coal extract is suitable for downstream processing.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 19, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventor: Alfred H. Stiller
  • Publication number: 20120091043
    Abstract: The present disclosure provides methods and systems for coal liquefaction using a rubber material. A method of obtaining a de-ashed coal extract includes exposing a coal to a rubber material in the presence of a coal-derived solvent to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, and separating the insoluble components from the slurry to obtain a de-ashed coal extract, wherein the coal extract is suitable for downstream processing.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 19, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventor: Alfred H. Stiller
  • Publication number: 20120082593
    Abstract: The present disclosure relates to a coal liquefaction system for utilizing a hydrogenated vegetable oil to liquefy coal. The system includes a reactor for exposing a coal to a hydrogenated vegetable oil in the presence of a coal-derived solvent to form a slurry, a heater that elevates the temperature of the slurry in the reactor to facilitate liquefying the coal and liberating a volatile matter, and a centrifuge that separates the insoluble components from the slurry to obtain a de-ashed coal extract, wherein the coal extract is suitable for downstream processing. The system may also include a distillation column that distills the de-ashed coal extract to obtain a pitch.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 5, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventors: Alfred H. Stiller, Elliot B. Kennel
  • Publication number: 20120080358
    Abstract: The present disclosure provides methods and systems for coal liquefaction using a pipeline crude oil. A method of obtaining a de-ashed coal extract includes exposing a coal to a pipeline crude oil to form a slurry, elevating the temperature of the slurry to facilitate liquefying the coal and liberating a volatile matter, and separating the insoluble components from the slurry to obtain a de-ashed coal extract, wherein the coal extract is suitable for downstream processing.
    Type: Application
    Filed: June 22, 2011
    Publication date: April 5, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventors: Alfred H. Stiller, Ernest Gordon Eberth
  • Publication number: 20120076703
    Abstract: The present disclosure provides methods and systems of a modular coal liquefaction system. A modular coal liquefaction system may include a reactor for exposing a coal to a hydrogenated vegetable oil in the presence of a coal-derived solvent to form a slurry, a heater that elevates the temperature of the slurry in the reactor to facilitate liquefying the coal and liberating a volatile matter, and a centrifuge that separates the insoluble components from the slurry to obtain a de-ashed coal extract, wherein the coal extract is suitable for downstream processing, wherein the reactor, heater, and centrifuge are adapted to be modular. The system may further include a distillation column that distills the de-ashed coal extract to obtain a pitch. The system may further include a coker that cokes at least one of the de-ashed coal extract and the pitch to obtain a coke. The system may be adapted to be modularly disposed on a rail car. The system may be adapted to be modularly disposed on a semi-truck trailer.
    Type: Application
    Filed: June 22, 2011
    Publication date: March 29, 2012
    Applicant: QUANTEX RESEARCH CORPORATION
    Inventors: Alfred H. Stiller, Gilbert A. Chalifoux