Patents Assigned to Rolls-Royce High Temperature Composites, Inc.
  • Publication number: 20210070664
    Abstract: A method is provided in which a resin coating is applied to a surface of a preform. The resin coating includes a carbonaceous resin and a particulate. The preform is added to a tooling. The preform, which is positioned in the tooling, is cured. The tooling is removed. The resin coating on the surface of the preform is pyrolyzed to form a resin carbon-char layer on the surface of the preform. The preform and the resin carbon-char layer are infiltrated with silicon to form a ceramic matrix composite (CMC) component including a layer of silicon carbide. During the infiltration, the silicon reacts with carbon in the resin carbon-char layer to form the layer of silicon carbide on the preform.
    Type: Application
    Filed: September 4, 2020
    Publication date: March 11, 2021
    Applicant: Rolls-Royce High Temperature Composites Inc
    Inventors: Pathikumar Sellappan, Sungbo Shim, Kevin Mark Lukhard
  • Publication number: 20210070663
    Abstract: A system of infiltration for producing a ceramic matrix composite (CMC) is provided in which a slurry is applied to an outer surface of a porous preform. The porous preform includes a framework of ceramic fibers. The slurry may include a solvent and a particulate. The porous preform may be infiltrated with the slurry. The particulate in the slurry may include a plurality of coarse particles and a plurality of fine particles. The coarse particles may have a d50 factor of 10-20 microns. The fine particles may have a d50 factor of 0.5-3 microns. A ratio of coarse particles to fine particles in the slurry may be between 1.5:1 and 4:1, inclusively.
    Type: Application
    Filed: September 4, 2020
    Publication date: March 11, 2021
    Applicant: Rolls-Royce High Temperature Composites Inc.
    Inventors: Pathikumar Sellappan, Sungbo Shim
  • Patent number: 10941942
    Abstract: A combustor of a gas turbine engine and a turbine shroud for a turbine of a gas turbine engine are disclosed. The combustor is configured to ignite a mixture of compressed air and fuel in a combustion chamber included therein. The turbine shroud is configured to direct products of the combustion reaction toward a plurality of rotatable turbine blades of the turbine to cause the plurality of turbine blades to rotate.
    Type: Grant
    Filed: December 16, 2015
    Date of Patent: March 9, 2021
    Assignees: Rolls-Royce North American Technologies Inc., Rolls-Royce High Temperature Composites Inc.
    Inventors: Ted J. Freeman, Wayne S. Steffier
  • Patent number: 10941079
    Abstract: In some examples, a method may include depositing, from a slurry comprising particles including silicon metal, a bond coat precursor layer including the particles comprising silicon metal directly on a ceramic matrix composite substrate. The method also may include locally heating the bond coat precursor layer to form a bond coat comprising silicon metal. Additionally, the method may include forming a protective coating on the bond coat. In some examples, an article may include a ceramic matrix composite substrate, a bond coat directly on the substrate, and a protective coating on the bond coat. The bond coat may include silicon metal and a metal comprising at least one of Zr, Y, Yb, Hf, Ti, Al, Cr, Mo, Nb, Ta, or a rare earth metal.
    Type: Grant
    Filed: September 9, 2016
    Date of Patent: March 9, 2021
    Assignees: Rolls-Royce High Temperature Composites, Inc., Rolls-Royce Corporation
    Inventors: Sungbo Shim, Kang N. Lee, Stephen Isaiah Harris, Andrew Joseph Lazur
  • Patent number: 10906842
    Abstract: A method of processing a CMC component includes preparing a fiber preform having a predetermined shape, and positioning the fiber preform with tooling having holes facing one or more surfaces of the fiber preform. After the positioning, a clamping pressure is applied to the tooling to force portions of the one or more surfaces of the fiber preform into the holes, thereby forming protruded regions of the fiber preform. During the application of the clamping pressure, the fiber preform is exposed to gaseous reagents at an elevated temperature, and a matrix material is deposited on the fiber preform to form a rigidized preform including surface protrusions. After removing the tooling, the rigidized preform is infiltrated with a melt for densification, and a CMC component having surface bumps is formed. When the CMC component is assembled with a metal component, the surface bumps may reduce diffusion at high temperatures.
    Type: Grant
    Filed: October 18, 2018
    Date of Patent: February 2, 2021
    Assignees: ROLLS-ROYCE HIGH TEMPERATURE COMPOSITES INC., ROLLS-ROYCE CORPORATION
    Inventors: Jun Shi, Sungbo Shim
  • Patent number: 10907493
    Abstract: A segmented turbine shroud for radially encasing a rotatable turbine in a gas turbine engine comprising a carrier, a ceramic matrix composite (CMC) seal segment, and an elongated pin. The carrier defines a pin-receiving carrier bore and the CMC seal segment defines a pin-receiving seal segment bore. The elongated pin extends through the carrier bore and the seal segment bore. The pin-receiving carrier bore includes a cantilevered member such that the carrier bore has a length sufficient to effect radial flexion between the carrier bore and the pin received within the carrier bore during operation of the turbine.
    Type: Grant
    Filed: November 13, 2018
    Date of Patent: February 2, 2021
    Assignees: Rolls-Royce Corporation, Rolls-Royce North American Technologies Inc., Rolls-Royce High Temperature Composites Inc.
    Inventors: Daniel Kent Vetters, David J. Thomas, Douglas David Dierksmeier, Jun Shi, Todd Engel
  • Publication number: 20210024426
    Abstract: A method of forming a barrier layer on a ceramic matrix composite (CMC) is described. The method includes forming a particulate surface layer comprising silicon particles on an outer surface of a fiber preform. The particulate surface layer is nitrided to convert the silicon particles to silicon nitride particles. After the nitriding, the fiber preform and the particulate surface layer are infiltrated with a molten material comprising silicon. Following infiltration, the molten material is cooled, thereby forming a ceramic matrix composite with a barrier layer thereon, where the barrier layer comprises silicon nitride and less than 5 vol. % free silicon. The barrier layer may also include silicon carbide and/or one or more refractory metal silicides.
    Type: Application
    Filed: July 7, 2020
    Publication date: January 28, 2021
    Applicant: Rolls-Royce High Temperature Composites Inc.
    Inventors: Sungbo Shim, Robert Shinavski, Pathikumar Sellappan
  • Publication number: 20210009480
    Abstract: A method of altering a surface of a ceramic matrix composite to aid in nodule removal is described. A fiber preform comprising a framework of ceramic fibers is heated to a temperature at or above a melting temperature of silicon. During the heating, the fiber preform is infiltrated with a molten material comprising silicon. After the infiltration, the fiber preform is cooled, and the infiltrated fiber preform is exposed to a gas comprising nitrogen during cooling. Silicon nitride may be formed by a reaction of free (unreacted) silicon at or near the surface of the infiltrated fiber preform with the nitrogen. Thus, a ceramic matrix composite having a surface configured for easy nodule removal is formed. Any silicon nodules formed on the surface during cooling may be removed without machining or heat treatment.
    Type: Application
    Filed: July 9, 2020
    Publication date: January 14, 2021
    Applicant: Rolls-Royce High Temperature Composites Inc.
    Inventors: Christopher Whitmore, Stephen Harris, Sungbo Shim, Timothy Western
  • Publication number: 20210009479
    Abstract: A method for infiltrating a porous preform for a gas turbine engine is provided, which comprises providing a chamber for infiltrating a porous preform. The porous preform is positioned within a slurry confinement fixture within the chamber. A vacuum is created in the chamber. A solvent is added to the slurry confinement fixture until a pressure in the chamber is substantially equal to an equilibrium partial pressure of the solvent. A slurry is added to the slurry confinement fixture. The slurry includes the solvent and a particulate. The pressure in the chamber is increased, and the slurry is urged into the porous preform.
    Type: Application
    Filed: July 11, 2019
    Publication date: January 14, 2021
    Applicant: Rolls-Royce High Temperature Composites Inc.
    Inventors: Thomas E. Krause, Robert Shinavski, Kevin Mark Lukhard
  • Publication number: 20200378265
    Abstract: A bladed disk preform system is provided. Multiple sheets are formed or provided. Each of the sheets may include multiple ceramic fibers. Slots may be cut in each of the sheets before or after forming. The slots extend from an outer edge of the sheets inward toward a center of the sheets. The sheets are stacked on top of each other to form a bladed disk preform. The bladed disk preform is porous. The bladed disk preform may include a plurality of blade portions extending outward from a root portion. Each of the slots is positioned between adjacent blade portions.
    Type: Application
    Filed: June 3, 2019
    Publication date: December 3, 2020
    Applicants: Rolls-Royce Corporation, Rolls-Royce High Temperature Composites Inc.
    Inventors: Jun Shi, Steffan Brown
  • Patent number: 10851026
    Abstract: A method of forming an impurity barrier layer on a CMC substrate may include introducing, to a heated plume of a thermal spray gun, a composite feedstock that includes a first coating material including a plurality of first particles; and a second coating material that may be different from the first coating material, where the second coating material at least partially encapsulates at least a portion of respective surfaces of the plurality of first particles; and directing, using the heated plume, at least the first coating material to a surface of a CMC substrate to deposit an impurity barrier layer including at least the first coating material.
    Type: Grant
    Filed: June 21, 2018
    Date of Patent: December 1, 2020
    Assignees: Rolls-Royce Corporation, Rolls-Royce High Temperature Composites, Inc.
    Inventors: Li Li, Sungbo Shim, Sunny Chang
  • Patent number: 10834790
    Abstract: A method of melt infiltrating a green ceramic matrix composite (CMC) article, wherein the green CMC article includes a ceramic reinforcing structure. The method includes heating a localized region of the green CMC article; melting a metal alloy infiltrant to form a molten metal alloy; and introducing the molten metal alloy into the localized region to infiltrate the reinforcing structure of the green CMC article with the metal alloy infiltrant and form the CMC article.
    Type: Grant
    Filed: December 18, 2015
    Date of Patent: November 10, 2020
    Assignee: Rolls-Royce High Temperature Composites, Inc.
    Inventor: Stephen Isaiah Harris
  • Patent number: 10822279
    Abstract: In some examples, a technique for infiltrating a porous preform with a slurry to form an infiltrated-preform, where the slurry includes a plurality of solid particles, where the plurality of solid particles include a plurality of fine ceramic particles defining an average fine particle diameter, a plurality of coarse ceramic particles defining an average coarse particle diameter, and a plurality of diamond particles, where the average fine particle diameter is less than the average coarse particle diameter, and infiltrating the infiltrated-preform with a molten metal infiltrant to form a ceramic matrix composite (CMC) article.
    Type: Grant
    Filed: April 28, 2017
    Date of Patent: November 3, 2020
    Assignee: Rolls-Royce High Temperature Composites, Inc.
    Inventors: Sungbo Shim, Robert Shinavski
  • Patent number: 10822280
    Abstract: A method of making a fiber preform for ceramic matrix composite (CMC) fabrication comprises laminating an arrangement of fibers between polymer sheets comprising an organic polymer, which may function as a fugitive binder during fabrication, to form a flexible prepreg sheet. A plurality of the flexible prepreg sheets are laid up in a predetermined geometry to form a stack, and the stack is heated to soften the organic polymer and bond together the flexible prepreg sheets into a bonded prepreg structure. Upon cooling of the bonded prepreg structure, a rigid preform is formed. The rigid preform is heated at a sufficient temperature to pyrolyze the organic polymer. Thus, a porous preform that may undergo further processing into a CMC is formed.
    Type: Grant
    Filed: August 29, 2018
    Date of Patent: November 3, 2020
    Assignee: ROLLS-ROYCE HIGH TEMPERATURE COMPOSITES INC.
    Inventors: Stephen Harris, David Smolenski
  • Patent number: 10787917
    Abstract: A multi-piece disk for use in a turbine of a gas turbine engine. The multi-piece disk includes a fore disk segment and an aft disk segment coupled with the fore disk segment for movement with the fore disk segment. The fore disk segment and the aft disk segment are formed to define slots that extend through the disk segments and are configured to receive turbine blades therein.
    Type: Grant
    Filed: May 4, 2018
    Date of Patent: September 29, 2020
    Assignees: Rolls-Royce North American Technologies Inc., Rolls-Royce High Temperature Composites Inc.
    Inventors: Ted J. Freeman, Christopher Barrett
  • Patent number: 10774010
    Abstract: Techniques for infiltrating a CMC substrate may include infiltrating the CMC substrate with a first slurry to at least partially fill at least some inner spaces of the CMC substrate, where the first slurry includes first solid particles, drying the first slurry to form an infiltrated CMC including the first solid particles, depositing a second slurry including a carrier material and second solid particles on a surface of the infiltrated CMC, where the second solid particles include a plurality of fine ceramic particles, a plurality of coarse ceramic particles, and a plurality of diamond particles, drying the second slurry to form an article having an outer surface layer including the second solid particles on the infiltrated CMC, and infiltrating the article with a molten infiltrant to form a composite article.
    Type: Grant
    Filed: April 28, 2017
    Date of Patent: September 15, 2020
    Assignee: Rolls-Royce High Temperature Composites, Inc.
    Inventors: Sungbo Shim, Andrew Joseph Lazur, Robert Shinavski
  • Patent number: 10767502
    Abstract: A turbine vane made from ceramic matrix composite material and adapted for use in a gas turbine engine. The turbine vane is made from ceramic matrix composite materials with three-dimensionally woven or braided reinforcing tows and includes an inner band, an outer band, and an airfoil that extends between the inner band and the outer band.
    Type: Grant
    Filed: March 17, 2017
    Date of Patent: September 8, 2020
    Assignees: Rolls-Royce Corporation, Rolls-Royce North American Technologies Inc., Rolls-Royce High Temperature Composites Inc.
    Inventors: Tara G. Schetzel, Ted J. Freeman, Jun Shi, Jeffrey A. Walston, Steven Clarke, Sean Kroszner
  • Patent number: 10767498
    Abstract: A blade assembly for use in a gas turbine engine. The blade assembly includes a blade, a platform distinct from the blade and configured to extend around the blade, and a pin that couples the platform with the blade.
    Type: Grant
    Filed: April 3, 2018
    Date of Patent: September 8, 2020
    Assignee: Rolls-Royce High Temperature Composites Inc.
    Inventor: Stephen Harris
  • Patent number: 10752556
    Abstract: A method of processing a ceramic matrix composite (CMC) component includes extracting silicon from a surface region of the CMC component such that free silicon is present in the surface region at a reduced amount of about 5 vol. % or less. The extraction comprises contacting the surface region with a wicking medium comprising an element reactive with silicon. The extraction is carried out at an elevated temperature prior to assembling the CMC component with a metal component.
    Type: Grant
    Filed: October 18, 2018
    Date of Patent: August 25, 2020
    Assignees: ROLLS-ROYCE HIGH TEMPERATURE COMPOSITES INC., ROLLS-ROYCE CORPORATION
    Inventors: Sungbo Shim, Jun Shi
  • Patent number: 10745325
    Abstract: A method including infiltrating a porous fiber preform with a slurry including a carrier fluid and a first plurality of solid particles wherein the first plurality of solid particles includes at least a first ceramic material, drying the slurry to form a greenbody preform, machining the greenbody preform to a target dimension, depositing a protective layer precursor including a second plurality of solid particles on the machined greenbody preform wherein the second plurality of solid particles includes at least a second ceramic material, and infiltrating the machined greenbody preform with a molten infiltrant to form a composite article including an integral protective layer.
    Type: Grant
    Filed: December 18, 2017
    Date of Patent: August 18, 2020
    Assignee: Rolls-Royce High Temperature Composites, Inc.
    Inventors: Sungbo Shim, Michael Abbott