Abstract: Techniques are generally described herein for the purification of glycerin. Embodiments include, but are not limited to, methods, systems, and articles of manufacture. Other embodiments may also be disclosed and claimed. Some techniques described herein include adding methyl alcohol and acid to crude glycerin to form a solution, filtering the solution to remove at least one salt of the acid from the solution, separating the solution into a first layer of free fatty acids and a second layer of at least partially purified glycerin, and distilling off the methyl alcohol from second layer of the solution. The second layer may then undergo one or more additional operations including neutralizing, further filtering to remove an excess of the neutralizing agent, passing through a plurality of ion-exchange columns, deodorizing, and dewatering.
Type:
Application
Filed:
May 5, 2010
Publication date:
January 6, 2011
Applicant:
S.I.I., LLC
Inventors:
Rico O. Cruz, Maryana Z. Pavlova, Nikolay I. Zamfirov, Dimitar Y. Zamfirov