Patents Assigned to Sandia
  • Patent number: 6797187
    Abstract: Microfluidic devices are disclosed which can be manufactured using surface-micromachining. These devices utilize an electroosmotic force or an electromagnetic field to generate a flow of a fluid in a microchannel that is lined, at least in part, with silicon nitride. Additional electrodes can be provided within or about the microchannel for separating particular constituents in the fluid during the flow based on charge state or magnetic moment. The fluid can also be pressurized in the channel. The present invention has many different applications including electrokinetic pumping, chemical and biochemical analysis (e.g. based on electrophoresis or chromatography), conducting chemical reactions on a microscopic scale, and forming hydraulic actuators.
    Type: Grant
    Filed: January 24, 2003
    Date of Patent: September 28, 2004
    Assignee: Sandia Corporation
    Inventors: Paul C. Galambos, Murat Okandan, Stephen Montague, James H. Smith, Phillip H. Paul, Thomas W. Krygowski, James J. Allen, Christopher A. Nichols, Jerome F. Jakubczak, II
  • Patent number: 6794086
    Abstract: A method for the manufacture of an electrode for an energy storage or conversion device comprises thermally spraying a feedstock mixture comprising an effective quantity of a source of a thermally protective salt and an active material or active material precursor onto a substrate to produce a film of the active material and salt. The film can have a thickness of about 1 to about 1000 microns. In a particularly advantageous feature, the active materials which ordinarily decompose or are unavailable at the high temperatures used during thermal spray processes, such as metal chalcogenides such as pyrite, CoS2, WS2, Ni(OH)2, MnO2, and the like may be thermally sprayed to form an electrode when the feedstock mixture employs an effective amount of a source of the thermally protective salt coating. The active material feedstock may comprise microstructured or nanostructured materials, which after thermal spray results in electrodes having microstructured or nanostructured active materials, respectively.
    Type: Grant
    Filed: February 28, 2001
    Date of Patent: September 21, 2004
    Assignees: Sandia Corporation, U.S. Nanocorp, Inc.
    Inventors: Jinxiang Dai, Ronald A. Guidotti, Tongsan D. Xiao, David E. Reisner
  • Patent number: 6793909
    Abstract: A method is disclosed for directly preparing alkali metal aluminum hydrides such as NaAlH4 and Na3AlH6 from either the alkali metal or its hydride, and aluminum. The hydride thus prepared is doped with a small portion of a transition metal catalyst compound, such as TiCl3, TiF3, or a mixture of these materials, in order to render them reversibly hydridable. The process provides for mechanically mixing the dry reagents under an inert atmosphere followed by charging the mixed materials with high pressure hydrogen while heating the mixture to about 125° C. The method is relatively simple and inexpensive and provides reversible hydride compounds which are free of the usual contamination introduced by prior art wet chemical methods.
    Type: Grant
    Filed: January 29, 2002
    Date of Patent: September 21, 2004
    Assignee: Sandia National Laboratories
    Inventors: Karl J. Gross, Eric Majzoub
  • Patent number: 6790476
    Abstract: A method of controlling the wetting characteristics and increasing the adhesion between a metal and an oxide layer. By introducing a negatively-charged species to the surface of an oxide layer, layer-by-layer growth of metal deposited onto the oxide surface is promoted, increasing the adhesion strength of the metal-oxide interface. The negatively-charged species can either be deposited onto the oxide surface or a compound can be deposited that dissociates on, or reacts with, the surface to form the negatively-charged species. The deposited metal adatoms can thereby bond laterally to the negatively-charged species as well as vertically to the oxide surface as well as react with the negatively charged species, be oxidized, and incorporated on or into the surface of the oxide.
    Type: Grant
    Filed: May 21, 2002
    Date of Patent: September 14, 2004
    Assignee: Sandia Corporation
    Inventors: Dwight R. Jennison, Alexander Bogicevic, Jeffry A. Kelber, Scott A. Chambers
  • Patent number: 6791470
    Abstract: A system and method for transferring wave energy into or out of a periodic structure having a characteristic wave impedance profile at a prime frequency, the characteristic wave impedance profile comprising a real portion and an imaginary portion, comprising: locating one or more energy transfer elements each having a wave impedance at the prime frequency approximately equal to the real portion of the characteristic wave impedance at one or more points on the periodic structure with the imaginary portion approximately equaling zero; and employing the one or more energy transfer elements to transfer wave energy into or out of the periodic structure. The energy transfer may be repeaters. Quarter-wave transformers can be provided at one or more points on the periodic structure with the imaginary portion approximately equaling zero to transmit waves across one or more discontinuities. A terminator can be employed for cancellation of waves.
    Type: Grant
    Filed: June 1, 2001
    Date of Patent: September 14, 2004
    Assignee: Sandia Corporation
    Inventor: Douglas S. Drumheller
  • Patent number: 6786716
    Abstract: A microcombustor comprises a microhotplate and a catalyst for sustained combustion on the microscale. The microhotplate has very low heat capacity and thermal conductivity that mitigate large heat losses arising from large surface-to-volume ratios typical of the microdomain. The heated catalyst enables flame ignition and stabilization, permits combustion with lean fuel/air mixtures, extends a hydrocarbon's limits of flammability, and lowers the combustion temperature. The reduced operating temperatures enable a longer microcombustor lifetime and the reduced fuel consumption enables smaller fuel supplies, both of which are especially important for portable microsystems applications. The microcombustor can be used for on-chip thermal management and for sensor applications, such as heating of a micro gas chromatography column and for use as a micro flame ionization detector.
    Type: Grant
    Filed: February 18, 2003
    Date of Patent: September 7, 2004
    Assignee: Sandia Corporation
    Inventors: Timothy J. Gardner, Ronald P. Manginelli, Patrick R. Lewis, Gregory C. Frye-Mason, Chris Colburn
  • Patent number: 6787762
    Abstract: Methods and apparatus are described for time dispersive spectroscopy. In particular, a modulated flow of ionized molecules of a sample are introduced into a drift region of an ion spectrometer. The ions are subsequently detected by an ion detector to produce an ion detection signal. The ion detection signal can be modulated to obtain a signal useful in assaying the chemical constituents of the sample.
    Type: Grant
    Filed: March 20, 2003
    Date of Patent: September 7, 2004
    Assignee: Sandia National Laboratories
    Inventors: Edward E. Tarver, III, William F. Siems
  • Patent number: 6783653
    Abstract: A new class of solar selective absorption coatings are disclosed. These coatings comprise a structured metallic overlayer such that the overlayer has a sub-micron structure designed to efficiently absorb solar radiation, while retaining low thermal emissivity for infrared thermal radiation. A sol-gel layer protects the structured metallic overlayer from mechanical, thermal, and environmental degradation. Processes for producing such solar selective absorption coatings are also disclosed.
    Type: Grant
    Filed: December 4, 2002
    Date of Patent: August 31, 2004
    Assignee: Sandia Corporation
    Inventors: Alan R. Mahoney, Scott T. Reed, Carol S. Ashley, F. Edward Martinez
  • Patent number: 6782746
    Abstract: A cast-in-place and lithographically shaped mobile, monolithic polymer element for fluid flow control in microfluidic devices and method of manufacture. Microfluid flow control devices, or microvalves that provide for control of fluid or ionic current flow can be made incorporating a cast-in-place, mobile monolithic polymer element, disposed within a microchannel, and driven by either fluid or gas pressure against a retaining or sealing surface. The polymer elements are made by the application of lithographic methods to monomer mixtures formulated in such a way that the polymer will not bond to microchannel walls. The polymer elements can seal against pressures greater than 5000 psi, and have a response time on the order of milliseconds. By the use of energetic radiation it is possible to depolymerize selected regions of the polymer element to form shapes that cannot be produced by conventional lithographic patterning and would be impossible to machine.
    Type: Grant
    Filed: October 24, 2000
    Date of Patent: August 31, 2004
    Assignee: Sandia National Laboratories
    Inventors: Ernest F. Hasselbrink, Jr., Jason E. Rehm, Timothy J. Shepodd
  • Publication number: 20040168173
    Abstract: A method and/or system and/or apparatus providing deception and/or execution alteration in an information system. In specific embodiments, deceptions and/or protections are provided by intercepting and/or modifying operation of one or more system calls of an operating system.
    Type: Application
    Filed: October 3, 2003
    Publication date: August 26, 2004
    Applicant: Sandia National Labs
    Inventors: Fred Cohen, Deanna T. Rogers, Vicentiu Neagoe
  • Patent number: 6782372
    Abstract: Latent effects on a system are broken down into components ranging from those far removed in time from the system under study (latent) to those which closely effect changes in the system. Each component is provided with weighted inputs either by a user or from outputs of other components. A non-linear mathematical process known as ‘soft aggregation’ is performed on the inputs to each component to provide information relating to the component. This information is combined in decreasing order of latency to the system to provide a quantifiable measure of an attribute of a system (e.g., safety) or to test hypotheses (e.g., for forensic deduction or decisions about various system design options).
    Type: Grant
    Filed: September 28, 2000
    Date of Patent: August 24, 2004
    Assignee: Sandia Corporation
    Inventors: J. Arlin Cooper, Paul W. Werner
  • Publication number: 20040162994
    Abstract: A method and/or system providing and/or indicating configurable and selectable strategies for responding to data units.
    Type: Application
    Filed: May 13, 2003
    Publication date: August 19, 2004
    Applicant: Sandia National Laboratories
    Inventors: Fred Cohen, Anthony George Carathimas, Eric Daniel Thomas
  • Patent number: 6777568
    Abstract: A new crystalline maganese phosphate composition having an empirical formula: Mn3(PO4)4.2(H3NCH2CH2)3N.6(H2O). The compound was determined to crystallize in the trigonal space group P-3c1 with a=8.8706(4) Å, c=26.1580(2) Å, and V (volume)=1783 Å3. The structure consists of sheets of corner sharing Mn(II)O4 and PO4 tetrahedra with layers of (H3NCH2CH2)3N and water molecules in-between. The pronated (H3NCH2CH2)3N molecules provide charge balancing for the inorganic sheets. A network of hydrogen bonds between water molecules and the inorganic sheets holds the structure together.
    Type: Grant
    Filed: June 18, 2002
    Date of Patent: August 17, 2004
    Assignee: Sandia Corporation
    Inventors: Steven G. Thoma, Francois R. Bonhomme
  • Patent number: 6775054
    Abstract: A device for optical parametric amplification utilizing four mirrors oriented in a nonplanar configuration where the optical plane formed by two of the mirrors is orthogonal to the optical plane formed by the other two mirrors and with the ratio of lengths of the laser beam paths approximately constant regardless of the scale of the device. With a cavity length of less than approximately 110 mm, a conversion efficiency of greater than 45% can be achieved.
    Type: Grant
    Filed: August 12, 2002
    Date of Patent: August 10, 2004
    Assignee: Sandia Corporation
    Inventors: Arlee V. Smith, Darrell J. Armstrong
  • Patent number: 6772513
    Abstract: A method for forming electro-fluidic interconnections in microfluidic devices comprises forming an electrical connection between matching bond pads on a die containing an active electrical element and a microfluidic substrate and forming a fluidic seal ring that circumscribes the active electrical element and a fluidic feedthrough. Preferably, the electrical connection and the seal ring are formed in a single bonding step. The simple method is particularly useful for chemical microanalytical systems wherein a plurality of microanalytical components, such as a chemical preconcentrator, a gas chromatography column, and a surface acoustic wave detector, are fluidically interconnected on a hybrid microfluidic substrate having electrical connection to external support electronics.
    Type: Grant
    Filed: June 27, 2002
    Date of Patent: August 10, 2004
    Assignee: Sandia Corporation
    Inventors: Gregory C. Frye-Mason, David Martinez, Ronald P. Manginell, Edwin J. Heller, Rajen Chanchani
  • Patent number: 6774532
    Abstract: A self-powered microthermionic converter having an internal thermal power source integrated into the microthermionic converter. These converters can have high energy-conversion efficiencies over a range of operating temperatures. Microengineering techniques are used to manufacture the converter. The utilization of an internal thermal power source increases potential for mobility and incorporation into small devices. High energy efficiency is obtained by utilization of micron-scale interelectrode gap spacing. Alpha-particle emitting radioisotopes can be used for the internal thermal power source, such as curium and polonium isotopes.
    Type: Grant
    Filed: December 20, 2001
    Date of Patent: August 10, 2004
    Assignee: Sandia Corporation
    Inventors: Albert C. Marshall, Donald B. King, Kevin R. Zavadil, Stanley H. Kravitz, Chris P. Tigges, Gregory A. Vawter
  • Patent number: 6775314
    Abstract: A supported distributed Bragg reflector or superlattice structure formed from a substrate, a nucleation layer deposited on the substrate, and an interlayer deposited on the nucleation layer, followed by deposition of (Al,Ga,B)N layers or multiple pairs of (Al,Ga,B)N/(Al,Ga,B)N layers, where the interlayer is a material selected from AlN, AlxGa1-xN, and AlBN with a thickness of approximately 20 to 1000 angstroms. The interlayer functions to reduce or eliminate the initial tensile growth stress, thereby reducing cracking in the structure. Multiple interlayers utilized in an AlGaN/GaN DBR structure can eliminate cracking and produce a structure with a reflectivity value greater than 0.99.
    Type: Grant
    Filed: November 29, 2001
    Date of Patent: August 10, 2004
    Assignee: Sandia Corporation
    Inventors: Karen E. Waldrip, Stephen R. Lee, Jung Han
  • Patent number: 6772611
    Abstract: The present invention provides a simple method for fabricating fiber-optic glass preforms having complex refractive index configurations and/or dopant distributions in a radial direction with a high degree of accuracy and precision. The method teaches bundling together a plurality of glass rods of specific physical, chemical, or optical properties and wherein the rod bundle is fused in a manner that maintains the cross-sectional composition and refractive-index profiles established by the position of the rods.
    Type: Grant
    Filed: June 25, 2003
    Date of Patent: August 10, 2004
    Assignee: Sandia National Laboratories
    Inventors: Dahv A. V. Kliner, Jeffery P. Koplow
  • Publication number: 20040153574
    Abstract: A method and/or system providing and/or indicating configurable and selectable strategies for responding to data units.
    Type: Application
    Filed: May 13, 2003
    Publication date: August 5, 2004
    Applicant: Sandia National Laboratories
    Inventors: Fred Cohen, Anthony George Carathimas, Eric Daniel Thomas
  • Patent number: 6771083
    Abstract: A new class of highly sensitive piezoconductive strain sensor elements and sensors has been invented. The new elements function under conditions such that electrical conductivity is dominated by Poole-Frenkel transport. A substantial piezoconductive effect appears in this regime, allowing the new sensors to exhibit sensitivity to applied strain as much as two orders of magnitude in excess of prior art sensors based on doped silicon.
    Type: Grant
    Filed: March 19, 2002
    Date of Patent: August 3, 2004
    Assignee: Sandia Corporation
    Inventor: Scott D. Habermehl