Abstract: A large capacity centrifugal vacuum concentrator includes a rotor assembly mounting a plurality of vertical spaced rotors mounted on a drive shaft and intervened with spacers between each lower rotor and a rotor next above, the rotors and spacers having interengaging drive transmission means for transmitting drive to the rotors and spacers when the drive shaft is driven. The rotor assembly is enclosed by a, e.g., cylindrical stainless steel cover which sits on a base and with the base defines a vacuum chamber. When the cover is elevated to open position, four quadrant access is available for loading and unloading of samples on the rotors. The rotor assembly is made up of interchangeable rotors, spacers and vessel holder frames which are selected from families of such dependent on particular vessel capacity and holder frame requirements.

Abstract: Thin film thermal oxidative engine oil or other oleaginous liquid deposit device has an oleaginous test liquid placement volume; a heatable depositor surface in liquid communication with the volume; a supply for at least one of an oxidant and another substance which can adversely affect the test liquid; and a relatively thin film forming unit which delivers the test liquid to the depositor surface in a relatively thin film. Thin film thermal oxidative engine oil or other oleaginous fluid deposit method is also provided, which includes providing an oleaginous test liquid in an oleaginous test liquid placement volume; providing a depositor surface and heating said surface; delivering the test liquid as a relatively thin film to the heated depositor surface; providing to the test liquid an oxidizing and/or other substance which can adversely affect the test liquid; and observing any deposits or other activity thereabout. The invention is useful in oil testing.

Abstract: A condenser cold trap unit for recovering as separate primary and secondary condensate fractions solvents contained in an effluent drawn from products being dried in a vacuum chamber includes inner and outer shell vessels, the inner shell vessel be disposed coaxially with the outer shell vessel inside said outer shell vessel with a space being present in the outer shell vessel under the bottom of the inner shell vessel and in a course surrounding the exterior of the inner shell vessel. A cover closes off the open tops of the two shell vessels and the interior space of the outer shell vessel is sealed from communication with outside atmosphere, and the interior space of the inner shell vessel is sealed from any communication with the interior space of the outer shell vessel. A common refrigeration coil encircles the exterior of the inner shell vessel and extends down therefrom to effect solvents condensing temperature levels cooling in both shell vessels.

Abstract: Device can include an array of stators placed in a carousel which can hold the stators in the array apart from one another while precisely cooled by a suitable source. For example, the device can be provided with cooling in conjunction with an instrument having a highly circulated, cold liquid bath for temperature control such as by insertion of the stators in the carousel through housing of a versatile sensitive rotating viscometer instrument into its bath. The sample carousel has a lower base containing a plurality of stator accommodating orifices in a first array, and an upper base connected to the lower base. The upper base can have a plurality of rotor control pin accommodating orifices in a second array, and the upper base is mounted to the lower base such that the second array of orifices in the upper base is disposed in registry with the first array of orifices in the lower base.