Abstract: A method of separating soap fibers from the liquid phase component of grease to prepare the fibers for microscopic analysis includes the steps of admixing a sample of the grease with a solvent to remove the liquid phase component from the fibers and provide a final liquid product having the fibers in suspension therein, contacting the final product with a pair of spaced electrodes, applying a direct voltage across the electrodes to charge the same positive and negative respectively, and withdrawing for analysis a small quantity of the final product from a region thereof proximate the negative electrode after the voltage has been applied for a predetermined energization period. The withdrawn quantity may be deposited on a polished carbon stub and further prepared for analysis by a scanning electron microscope.
Type:
Grant
Filed:
September 23, 1996
Date of Patent:
December 30, 1997
Assignee:
Semtech, Inc.
Inventors:
Michael R. Funk, Larry E. Irwin, Michael D. Foster