Abstract: A method for fluorinating a filter for a pipette tip, the filter being made of a solid porous structure made of polyolefin. The method comprises the following steps: (a) placing the filter in an enclosure, (b) creating a vacuum in the enclosure, and (c) bringing the filter into contact with a fluorination agent injected into the enclosure in a gaseous state, the fluorination agent being made up of difluorine F2, the difluorine F2 being injected into the enclosure at a partial pressure between 100 Pa and 10000 Pa and step (c) being done at a temperature between 0° C. and 100° C. A pipette tip comprising a filter modified by the fluorination method, a method for producing such a tip, as well as a withdrawing pipette equipped with such a tip.
Type:
Grant
Filed:
February 18, 2019
Date of Patent:
June 11, 2024
Assignees:
GILSON SAS, UNIVERSITE CLERMONT AUVERGNE, SIGMA CLERMONT, CENTRE NATIONAL DE LA RECHERCHE
Inventors:
Nicolas Batisse, Marc Dubois, Jérémy Peyroux, Béatrice Guieu Presle
Abstract: A method of manufacturing nanoparticles of a photoluminescent material, including the successive steps of: a) forming nanometer-range particles of said photoluminescent material; b) forming a dispersion containing the particles in a non-aqueous solvent, the dispersion further containing at least one surface agent; c) placing the dispersion in an autoclave at a pressure in the range from 2 MPa to 100 MPa; and d) recovering the particles.
Type:
Grant
Filed:
June 30, 2017
Date of Patent:
December 14, 2021
Assignees:
Aledia, Université Clermont Auvergne, Centre National de la Recherche Scientifique, Sigma Clermont
Abstract: A method for producing a photo-luminescent material, including the following steps: (1) producing, according to a sol-gel method, a sol and then a gel of first precursors of a first substance from the sol; (2) crushing the gel; (3) optionally, annealing the gel in order to form first particles of the first substance of which the average size is between 1 pm and 20 um; (4) producing a colloidal dispersion of second particles of a second substance, different from the first substance or identical to the first substance, of which the average size is between 5 nm and 400 nm; (5) mixing the colloidal dispersion with the sol in step (1) before forming the gel or with the first particles after step (3); and (6) annealing the mixture obtained in step (5), resulting in an increase in the compactness of the mixture, the average size of the second particles after annealing being between 100 nm and 900 nm.
Type:
Grant
Filed:
August 12, 2015
Date of Patent:
April 28, 2020
Assignees:
Aledia, Universite Clermont Auvergne, Centre National de la Recherche Scientifique, Sigma Clermont
Abstract: A method for producing a photo-luminescent material, including the following steps: (1) producing, according to a sol-gel method, a sol and then a gel of first precursors of a first substance from the sol; (2) crushing the gel; (3) optionally, annealing the gel in order to form first particles of the first substance of which the average size is between 1 pm and 20 um; (4) producing a colloidal dispersion of second particles of a second substance, different from the first substance or identical to the first substance, of which the average size is between 5 nm and 400 nm; (5) mixing the colloidal dispersion with the sol in step (1) before forming the gel or with the first particles after step (3); and (6) annealing the mixture obtained in step (5), resulting in an increase in the compactness of the mixture, the average size of the second particles after annealing being between 100 nm and 900 nm.
Type:
Application
Filed:
August 12, 2015
Publication date:
October 5, 2017
Applicants:
Aledia, Universite Blaise Pascal-Clermont II, Centre National de la Recherche Scientifique, Sigma Clermont