Abstract: A method for operating a power-compensated fusion furnace that includes a power control system having one switching device per heating element, power measurement circuitry, a master temperature sensor, and a controller. Each switching device is electrically connected to a respective heating element. The controller, in conjunction with the switching devices, is able to individually control the electrical energy flowing to each heating element, thereby controlling the duty cycle of each heating element. The duty cycles are corrected for one or more of variations in the electrical resistance of each heating element and position-dependent variations in furnace cavity temperature.

Abstract: A method for operating a power-compensated fusion furnace that includes a power control system having one switching device per heating element, power measurement circuitry, a master temperature sensor, and a controller. Each switching device is electrically connected to a respective heating element. The controller, in conjunction with the switching devices, is able to individually control the electrical energy flowing to each heating element, thereby controlling the duty cycle of each heating element. The duty cycles are corrected for one or more of variations in the electrical resistance of each heating element and position-dependent variations in furnace cavity temperature.

Abstract: A heating element includes a filament that conducts electricity. In some embodiments, the filament is encapsulated in a silicon nitride cover. The heating element provides a heating zone located relatively closer to the tip of the heating element and relatively further from a connection where electrical leads connect to the filament.

Abstract: A fluxer includes a single, wide furnace enclosure that is sufficiently large and prewired to accommodate multiple fusion positions. The furnace includes at least one movable insulated partition that defines the actual insulated volume of the furnace.

Abstract: In a process for the preparation of inorganic sample disks for analysis, the sample, in powdered form, is mixed with a powdered reagent flux which has been pre-melted. In an inert gas atmosphere, the mixture is placed in a graphite crucible and heated to a temperature slightly above 1000° C. After the flux dissolves the sample, a homogenous mix is produced. This mix is then poured into a graphite mold, the bottom of which contains a molten pool of an inert metal, such as gold, which acts as a smooth receiving surface. Upon cooling, the material in the mold solidifies, resulting in a glassy disk that can be analyzed. Cooling can be accelerated by making use of a cooling fluid that has a substantially higher thermal capacity than air.

Abstract: A vial and impactor combination for use in a cryogenic mill is disclosed. The impactor includes a steel or similar core, and a surrounding exterior of polycarbonate or similar inert material. The vial is made preferably of polycarbonate with endcaps also made of polycarbonate.