Abstract: A carbonaceous particulate material is provided that is characterized by having a reversible volumetric expansion/contraction in fluid media (“VR”) of greater than or equal to (?)3% between 4,000 psi and 10,000 psi. The porous carbonaceous particulate material of the present disclosure is also characterized by having a true density, (“PT”), of 1.2 g/cc?PT?2.0 g/cc, when milled to ?200 mesh and has a d50 particle size distribution of about 15 ?m. This is the consequence of the instant material exhibiting a high level of closed porosity with very small pores, in contrast with prior art materials that would have a wider range pore sizes for the closed pores.

Abstract: An assembly for the test chamber of a wellbore fluid testing apparatus for simulating fractures in a wellbore is provided comprising base plate of a first diameter having an aperture therethrough configured to be removably secured within the test chamber. A solid end plate of a second diameter smaller than the first diameter is provided that is removably secured to the base plate. One or more intermediate plates is provided that is located between the base plate and the end plate, each intermediate plate also having an aperture therethrough. At least one shim or spacer is provided to space the intermediate plates from any adjacent intermediate plate and/or to space the end plate from the adjacent intermediate plate. The spacer is configured to be removably secured to the assembly and to permit fluid flow in in the assembly through the aperture in the base plate and the opposed face of the intermediate plate and an adjacent intermediate plate or the base plate.

Abstract: A carbonaceous particulate material is provided that is characterized by having a reversible volumetric expansion/contraction in fluid media (“VR”) of greater than or equal to (?)3% between 4,000 psi and 10,000 psi. The porous carbonaceous particulate material of the present disclosure is also characterized by having a true density, (“PT”), of 1.2 g/cc?PT?2.0 g/cc, when milled to?-200 mesh and has a d50 particle size distribution of about 15 ?m. This is the consequence of the instant material exhibiting a high level of closed porosity with very small pores, in contrast with prior art materials that would have a wider range pore sizes for the closed pores.

Abstract: A method for controlling the loss of drilling fluid from an oil well borehole into formations penetrated by a drill bit is disclosed by which resilient graphitic carbon particles having a resiliency greater than about 130% rebound after compression to 10,000 psi; a degree of graphitization greater than 85%, as measured by d002 using XRD; an average pore size larger than 0.035 micron; and an aspect ratio smaller than 0.63 are added to the drilling fluid.

Abstract: A method for controlling the loss of drilling fluid from an oil well borehole into formations penetrated by a drill bit is disclosed by which resilient graphitic carbon particles having a resiliency greater than about 130% rebound after compression to 10,000 psi; a degree of graphitization greater than 85%, as measured by d002 using XRD; an average pore size larger than 0.035 micron; and an aspect ratio smaller than 0.63 are added to the drilling fluid.

Abstract: An assembly for the test chamber of a wellbore fluid testing apparatus for simulating fractures in a wellbore is provided comprising base plate of a first diameter having an aperture therethrough configured to be removably secured within the test chamber. A solid end plate of a second diameter smaller than the first diameter is provided that is removably secured to the base plate. One or more intermediate plates is provided that is located between the base plate and the end plate, each intermediate plate also having an aperture therethrough. At least one shim or spacer is provided to space the intermediate plates from any adjacent intermediate plate and/or to space the end plate from the adjacent intermediate plate. The spacer is configured to be removably secured to the assembly and to permit fluid flow in in the assembly through the aperture in the base plate and the opposed face of the intermediate plate and an adjacent intermediate plate or the base plate.

Abstract: A method for improving the thermal characteristics of cement compositions is provided in which fine resilient graphitic carbon particles (“RGC”) are substituted for a portion of the fine aggregate (typically sand) in the cement formulation. For the purposes of the present disclosure, “fine” is intended to describe particulates having a mesh size of less than about 8 mesh, or a particle size of less than about 2.38 mm, or, more preferably when referring to RGC, a mesh size of less than about 16 mesh and a particle size of less than about 1.19 mm. “Resilient” is intended to describe graphitic carbon particles that exhibit a rebound of at least about 20% after compression to 10,000 psi.

Abstract: An coated particulate is provided with a graphite-impregnated resin coating. The oil field particulates may comprise any of gravel-pack sand, granular betonite, ground Gilsonite, calcium carbonate, glass beads, rock wool, shredded paper, metal spheres, ceramic beads, nut hulls, ground rubber, plastic beads, muscovite mica, calcined petroleum coke, and perlite. The resin may comprise as a binder one or more of a natural, synthetic, water-soluble, and organic resins. More specifically, the resins may comprise an organic film-forming resin such as an alkyd, polyurethane and epoxy. Alternatively, the resin may comprise a film-forming water-soluble polymer, such as a starch, carboxymethyl cellulose, hydroxyethyl cellulose, and xanthan gum. In a further alternative, the resin may comprise a resin-dispersed emulsion, such as a latex or acrylic.

Abstract: Hydrocarbon containing formations can be processed using an in-situ liquefaction technique. This new technique embodies systematic temperature elevation applied to subsurface formation allowing recoverable hydrocarbons to reach a Newtonian fluid viscosity suitable for extraction.

Abstract: An coated particulate is provided with a graphite-impregnated resin coating. The oil field particulates may comprise any of gravel-pack sand, granular betonite, ground Gilsonite, calcium carbonate, glass beads, rock wool, shredded paper, metal spheres, ceramic beads, nut hulls, ground rubber, plastic beads, muscovite mica, calcined petroleum coke, and perlite. The resin may comprise as a binder one or more of a natural, synthetic, water-soluble, and organic resins. More specifically, the resins may comprise an organic film-forming resin such as an alkyd, polyurethane and epoxy. Alternatively, the resin may comprise a film-forming water-soluble polymer, such as a starch, carboxymethyl cellulose, hydroxyethyl cellulose, and xanthan gum. In a further alternative, the resin may comprise a resin-dispersed emulsion, such as a latex or acrylic.

Abstract: An electrically conductive paving system that has enhanced conductivity of the conductive graphite/asphalt layer. This is achieved by incorporating into the paving mixture a blend of two naturally occurring crystalline flake graphites, one being coarse (generally larger than 40 mesh/425 microns) and the other being fine (generally smaller than 100-200 mesh/150-75 microns). The ratio of course flake graphite to fine flake graphite may be from 1.5:1 and 1:1.5, but is preferably approximately 1:1.

Abstract: A method of preparing graphite intercalation compounds in which graphite particles are immersed in an aqueous electrolyte media comprising both an acid and an oxidizing agent. The immersed graphite particles are subjected to an anodic current and then removed from the electrolyte and rinsed with a solvent. The excess solvent and electrolyte is then removed from the graphite particles. The graphite particles may be placed in a plating barrel which is immersed in the electrolyte and rotated while the graphite particles are subjected to the current. The resultant intercalated graphite has an expansion volume of from between about 100 ml/g to 2000 ml/g when heated to 1000° C.

Abstract: An engineered carbonaceous material (ECM) comprising a mixture of synthetic graphite and one or more other graphite, such as natural flake graphite, natural vein graphite, and/or amorphous graphite. The objects are also achieved by an ECM comprising a mixture of expanded graphite and one or more other graphite materials, such as natural flake graphite, natural vein graphite, amorphous graphite and/or synthetic graphite. The ECM is preferably mixed with 0.01 to 20.0 wt. % MnO2 to create a battery active material. The mixtures may be made by either co-blending or co-grinding the graphites together. An electrochemical cell incorporating the material is also contemplated.

Abstract: A method for making expanded graphite from lamellar flake graphite comprising first providing lamellar flake graphite particles having at least a minimal purity, then intercalating the lamellar flake graphite particles with an expandable graphite intercalation compound, followed by expanding the graphite intercalation compound to exfoliate the flake graphite particles, and finally air milling the exfoliated flake graphite particles to further delaminate them.

Abstract: A method of treating hopper cars to prevent bridging or sticking of bulk commodities during unloading by applying a coating of a mixture comprising pigments including graphite, solvents, resins, a drier/cross-linking/hardening system, and a rheological system. The resin is selected from the group consisting of alkyds, acrylics, polyesters, hydrocarbon resins, rosin-based resins, polyamides, urethanes, and epoxies. The solvent comprises aliphatic and aromatic hydrocarbons. Ranges in weight-percent for each of the components is set forth, as well as a specific formulation.

Abstract: A high-temperature lubricant comprising a water-base and minor effective amounts of borate, dextrin, graphite, xanthan gum, and an organic preservative. A powder for preparing a water-based high temperature lubricant is disclosed in which the powder comprises graphite and minor effective amounts of borate, dextrin, and xanthan gum. A continuous process for making the lubricant is also disclosed.

Abstract: A method of preventing or controlling the loss of well drilling fluid into the pores and fractures of subterranean rock formations by the addition of resilient graphitic carbon particles to the drilling fluid in sufficient amounts to plug the pores and fractures. The graphitic carbon material reduces loss of circulation, lowers torque and drag, prevents casing wear while drilling, and provides a new method for the controlled release of graphite at extreme pressure. The material is non-toxic and imparts the well-known lubricating properties of graphite without contributing to surface sheen development under US EPA offshore cuttings discharge rules.

Abstract: A method of consolidating particulate materials or combinations of such materials into shaped products of very low porosity. High compaction pressures are applied at temperatures in the range of sintering temperature of the materials being consolidated to achieve essentially complete densification at extremely rapid processing rates. Electrothermal heating is utilized to accomplish these results. Difficult materials such as silicon carbide, boron carbide and other very high melting point materials may be densified by these techniques.

Abstract: The present invention comprises an improved method of controlling resistivity in a process for consolidating particular materials or combinations of such materials into shaped products of very low porosity. High compaction pressures are applied at temperatures in the range of sintering temperature of the materials being consolidated to achieve essentially complete densification at extremely rapid processing rates. Electrothermal heating of a medium having controlled resistivity is utilized to accomplish these results. Various difficult materials, such as silicon carbide, boron carbide and other very high melting point materials, may be densified by these techniques.

Abstract: An electrically conductive paving system that has enhanced conductivity of the conductive graphite/asphalt layer. This is achieved by incorporating into the paving mixture a blend of two naturally occurring crystalline flake graphites, one being coarse (generally larger than 40 mesh/425 microns) and the other being fine (generally smaller than 100-200 mesh/150-75 microns). The ratio of course flake graphite to fine flake graphite may be from 1.5:1 and 1:1.5, but is preferably approximately 1:1.