Abstract: A process for testing the properties of a rubber sample is provided. This process is suitable for use with current rheometers, curemeters, viscometers, and the like, wherein it is common to change test conditions during the duration of the test, when the rubber sample scorches or reaches full cure. This process provides a method for determining an optimal time for changing the test conditions to which the rubber sample is subjected. With this process specifying times for changing test conditions is no longer required prior to starting the test. Rather, the variable test condition is changed at sample-specific times that closely coincide with the actual scorch time or full cure time of the sample.

Abstract: A method for cutting compounded rubber for reflected light measurement of the disbursement of fillers therein is disclosed. The method includes subjecting a sample of compounded rubber to a dynamic pulling force, and cutting the sample while it is subjected to the dynamic pulling force. The method may further include the step of pressing the sample to remove entrapped air from the sample, and, preferably, the method includes cooling the sample during such a pressing step. Cutting the sample while it is subjected to a dynamic pulling force will reduce, and, preferably, eliminate, the presence of smears on a cut surface of the sample. By reducing the amount of entrapped air within a sample and, further, reducing the occurrence of smearing during cutting of the sample, a subsequent reflected light measurement of the dispersion of fillers within the compounded rubber sample is more accurate.

Abstract: An apparatus for testing polymeric samples is shown in which a polymer specimen is subjected to sinusoidal, oscillatory motion. The oscillatory motion is generated by the use of a continuously variable eccentric cam that is affixed to a drive shaft rotated by a motor. The amplitude of oscillation is determined by the eccentricity of the cam, and verified by measurement of angular deflection. The eccentricity of the cam can be altered, in one embodiment, through the manual manipulation of an adjustable nut, and, in another, automated embodiment, through the motion of the rotating motor. The eccentricity of the cam is continuously variable and can quickly be changed within a single test.