Abstract: A plating chemical replenishment system is described having a tank for supporting a chemical solution used in a plating fluid, a container having a pre-determined volume, a first valve for selectively coupling the chemical solution from the tank to the container to form a pre-determined volume of the chemical solution within the container, and a second valve for selectively dispensing the pre-determined volume of the chemical solution from the container to a plating fluid reservoir. Also disclosed is a method of dispensing a plating solution to a plating fluid reservoir, comprising the steps of forming a pre-determined volume of the plating solution; and dispensing the pre-determined volume of the plating solution to the plating fluid reservoir.

Abstract: A plating apparatus, anode assembly, and method therefor are disclosed herein that improves the uniformity of the plating deposition across the surface of a wafer, substrate or article. This improvement is accomplished by compensating for the uneven plating deposition caused by a seed layer disposed on the article. The seed layer typically has a high resistance. As a result of the high resistance characteristic of the seed layer, plating currents that flow through substantial portion of the seed layer to the cathode contact encounter more resistance than plating currents that flow through less seed layer. This produces non-uniformity in the plating currents across the surface of the wafer, which results in an uneven plating deposition across the surface of the wafer. The plating apparatus, anode, and method therefor provide an anode having a plurality of separate anode sections designed to plate different surface regions of the wafer.

Abstract: The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy sulfate electroplating baths has a number of unexpected benefits including wider useful current density range, improved appearance and in the case of tin improved oxidative stability. The metals and alloys include but are not limited to tin, nickel, copper, chromium, cadmium, iron, rhodium, ruthenium, iron/zinc and tin/zinc.

Abstract: The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy halide electroplating baths has a number of unexpected benefits including wider useful current density range and improved appearance. The metals and metal alloys include but are not limited to tin, lead, copper, nickel, zinc, cadmium, tin/zinc, zinc/nickel and tin/nickel.

Abstract: Methods of making a graphite material are provided. A flexible graphite is ground into a powder. The graphite powder is mixed with a resin and the mixture is hot pressed. A second method of making a graphite material is provided where the graphite is ground into a powder; the graphite powder is soaked in a cryogenic liquid; the soaked graphite powder is then expanded; the expanded soaked graphite powder is mixed with a graphite powder; and the graphite powder mixed with a resin are hot pressed. According to a third method, the flexible graphite is ground into a powder; the graphite powder is soaked into a cryogenic liquid, the soaked graphite powder is expanded; and the expanded soaked graphic powder is ground into a fine powder. The resulting graphite powder is mixed with a resin. The graphite powder mixed with the resin is hot pressed. According to a fourth method, graphite flakes are soaked into an acid; the soaked graphite flakes are expanded; and the expanded soaked graphite flakes are precompacted.

Abstract: A plating apparatus and methodology is disclosed that is particularly useful in improving the plating rate, improving the plating of via holes, improving the uniformity of the plating deposition across the surface of the wafer, and minimizing damage to the wafer. With regard to improving the plating rate and the plating of via holes, the plating apparatus and method immerses a wafer in a plating fluid bath and continuously directs plating fluid towards the surface of the wafer. Immersing the wafer in a plating fluid bath reduces the occurrence of trapped gas pockets within via holes which makes it easier to plate them. The continuous directing of plating fluid towards the surface of the wafer increases the ion concentration gradient which is, in turn, increases the plating rate.

Abstract: The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy sulfonic acid electroplating baths has a number of unexpected benefits including wider useful current density range, improved appearance and in the case of tin improved oxidative stability. An additional significant appearance is to reduce the overall costs of this type of bath with the more economical salts of alkyl and alkanol sulfonic acids. The metals and metal alloys include but are not limited to tin, lead, copper, nickel, zinc, tin/lead, tin/lead/copper, tin/zinc and zinc/nickel.

Abstract: Abrasion resistant, high strength, high temperature, flexible thermocouple cable comprising two thermocouple wires, a pultrusion of a plurality of aramid fibers, sintered tape, shield, and a water impervious food safe fluoroelastomer outer insulation.

Abstract: The use of alkali metal, alkaline earth metal, ammonium and substituted ammonium salts of alkyl and alkanol sulfonic acids as additives in pure metal and metal alloy fluoroborate electroplating baths has a number of unexpected benefits including wider useful current density range and improved appearance. The metals and metal alloys include but are not limited to tin, lead, copper, cadmium, indium, iron, tin/lead and tin/lead copper.

Abstract: An electroplating system includes a tank that holds an electrolytic bath solution. An anode within the tank receives a first voltage having a first potential. A substrate cathode, immersible in the solution within the tank, spaced from the anode, receives a second voltage having a second potential, opposite to that of the first potential. A shield is immersible in the solution within the tank between the anode and cathode. The level of shielding provided by the shield is variable and controllable. In one embodiment, the shield includes a conductive element that receives a third voltage having the first potential, the magnitude of the third voltage being controllable. In another embodiment, the shield includes at least one louver, the physical orientation of which is controllably adjustable. The shield is sufficiently spaced from the substrate cathode to be substantially outside an area of sparging and is fixed between the anode and cathode.

Abstract: An actuating device operated by a hookstick is attached to an existing ring on a manually operated fused cutout switch or oil circuit recloser switch. The device comprises a cantilever and a clamp for attaching the cantilever about the existing ring. The cantilever a pair of lever arms, each having a hook-shaped receptacle for receiving a hookstick that is used to alternatively open or close the switch. Methods of actuating a manually operated recloser and lock-out switch and modifying such a switch to facilitate manual operation are disclosed.

Abstract: An actuating device operated by a hookstick is attached to a manually operated oil circuit recloser switch. The device comprises a cantilever and an affixed switch lever. The cantilever includes a pair of lever arms, each having a hook-shaped receptacle for receiving a hookstick that is used to alternatively open or close the switch. Methods of actuating a manually operated switch in a recloser and lock-out device and modifying such a switch to facilitate manual operation are disclosed.

Abstract: A battery drain limitation circuit for use in engine powered vehicles and equipment which rely upon a battery to start the engine and also to operate accessories. When the engine is not running, the circuit disconnects the battery from all loads when battery charge, as measured by either one of two complementary means responsive to high and low drain rates, respectively, falls to a level below which the battery charge may not be sufficient to start the engine. High drain rates exaggerate battery voltage reduction below no load voltage levels, and are detected by a low cutoff voltage level after which the battery voltage recovers to reflect sufficient charge to start the engine. Battery dissipation from low drain rates is prevented by a long timing delay following detection of a high cutoff voltage level. The circuit is rendered inoperable if the engine is running, by means of a microphone which detects engine noise. The device is simple to install at the battery.

Abstract: The present invention provides novel water-soluble diphosphines having the formula ##STR1## wherein X, Y, R.sub.1-18 and n are defined herein, and which can be complexed with a transition metal to form a novel catalyst useful in such applications as hydroformylation.

Abstract: A method for producing a novel yeast and mold inhibiting products (FIC) from a Lactobacillus, particularly a Lactobacillus casei having the yeast and mold producing characteristics of Lactobacillus casei var. rhamnosus NRRL-B-15972 is described. The products (FIC) are particularly useful in retarding yeast and mold growth in foods and other materials in need thereof.

Abstract: This invention relates generally to a solution for electroless deposition of gold, and more particularly to a cyanide-free electroless gold solution that can be replenished by the addition of a solution of a non-cyanide complex of gold. The operating temperature range for the plating solution of the present invention ranges from about 40.degree. to about 70.degree. C. The opportunity to deposit gold at such low operating temperatures is especially beneficial for plating devices which cannot withstand the higher temperatures required for existing electroless gold solutions. The relatively low operating temperatures also provide for significant energy savings and increased operator comfort and safety as compared to existing electroless gold solutions.

Abstract: The water heating apparatus is formed by a container having spaced upper and lower walls and a cylindrical side wall having upper and lower portions extending between the upper and lower walls defining an interior of the container. An inlet opening is formed through the central portion of the upper wall. An elongated hollow flame tube is located within the interior of the container and has an upper end coupled to the inlet opening of the upper wall and extends downward. A combustion device is coupled to the inlet opening of the upper wall for directing a flame into the flame tube by way of the upper opening.

Abstract: The present invention relates to an inexpensive material and method of making the material having superior heat insulation capacity for use in furnaces and other apparatus. The method comprises grinding flexible graphite foil, preferably recycled material, to a small particle size, thermally shocking the particles to expand them, mixing the expanded graphite with a thermoset phenolic resin, heating the mixture under pressure to form a solid sheet and then heat treating the solid sheet. The present invention also includes a method for making a plastic material by using a thermoplastic material mixed with re-expanded graphite. The compound of thermo plastic material and re-expanded graphite is fed into an injection molding system at a relatively high temperature and injected into a mold where a plastic material is formed. The plastic material is then removed from the mold when the material is still very hot but hard set.

Abstract: A bacteriocin produced by Lactococcus lactis NRRL-B-18535 is described. The bacteriocin is useful in foods and other materials and has a wide spectrum of activity against Gram-positive bacteria in a pH range between 2 and 8.

Abstract: A device for removing a contaminant from a fluid stream flowing within a conduit is disclosed. The device includes a container and a barrier. The container has a first wall generated about an axis and a second wall generated about the same axis. The first wall defines a first volume therewithin, while the first and second walls define an annular second volume therebetween. Both the first and second volumes are sealed at one end of the device, while at the other end of the device the second volume only is sealed. A filter material occupies the second volume. The first and second walls are permeable to the fluid stream and are capable of retaining the filter material in the second volume. The barrier is impermeable to the fluid stream and creates a seal between the second wall and the conduit wall.