Abstract: Carbon fiber composites containing lignin carbon fibers are described. The lignin carbon fibers can be derived from organosolv lignin obtained from single source lignocellulosic feedstocks or combinations of such feedstocks or lignin obtained via other pulping or extraction methods. Also described are methods of preparing the carbon fiber composites.
Type:
Grant
Filed:
October 31, 2017
Date of Patent:
November 29, 2022
Assignees:
University of Tennessee Research Foundation, TennEra, LLC
Inventors:
David Paul Harper, Omid Hosseinaei, Dayakar Penumadu, Nathan Kieran Meek, Daniel Webb, James Mynes, Nicole Labbe, Joseph John Bozell, Timothy G. Rials, Stephen Andrew Young
Abstract: A process for stabilizing lignin fibers, stabilized lignin fibers made by the process and carbonized fibers made from stabilized lignin fibers. The process includes heating lignin fibers to a temperature ranging from about 100° to about 220° C. while the fibers are in an atmosphere of air and HCl gas, generated as air is bubbled through concentrated hydrochloric acid for a period of time sufficient to stabilize the lignin fibers.