Patents Assigned to The Ishizuka Research Institute, Ltd.
  • Patent number: 6500557
    Abstract: This invention provides a composite product and an effective method for producing the same, based on an SHS or intense heat producing process. Said composite essentially comprises either (1) one or more skeletal structures of three dimensionally joined pieces of at least one ceramic material selected from carbide, boride, nitride and silicide of titanium, zirconium, tantalum, niobium, silicon, chromium, tungsten, and molybdenum, and metallic material of alloy and/or intermetallic compound which fills the gaps within each and between adjacent skeletal structures, or (2) a matrix consisting of SHS products of metallic and/or ceramic substances, and particles of superabrasive selected from diamond and high pressure polymorphism of boron nitride, which are held and distributed in the matrix in the whole, in the surface or surface area comprising the portion corresponding to the end working face.
    Type: Grant
    Filed: September 18, 2000
    Date of Patent: December 31, 2002
    Assignees: Ishizuka Research Institute, Ltd., Moscow Steel & Alloys Institute SHS-Center
    Inventors: Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi, Evgeny A. Levashov, Alexander V. Trotsue, Inna P. Borovinskaya
  • Patent number: 6451249
    Abstract: This invention provides a composite product and an effective method for producing the same, based on an SHS or intense heat producing process. Said composite essentially comprises either (1) one or more skeletal structures of three dimensionally joined pieces of at least one ceramic material selected from carbide, boride, nitride and silicide of titanium, zirconium, tantalum, niobium, silicon, chromium, tungsten, and molybdenum, and metallic material of alloy and/or intermetallic compound which fills the gaps within each and between adjacent skeletal structures, or (2) a matrix consisting of SHS products of metallic and/or ceramic substances, and particles of superabrasive selected from diamond and high pressure polymorphism of boron nitride, which are held and distributed in the matrix in the whole, in the surface or surface area comprising the portion corresponding to the end working face.
    Type: Grant
    Filed: September 18, 2000
    Date of Patent: September 17, 2002
    Assignees: Ishizuka Research Institute, Ltd., Mitsue Koizumi, Manshi Ohyanagi, Moscow Steel & Alloys Institute SHS-Center
    Inventors: Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi, Evgeny A. Levashov, Alexander V. Trotsue, Inna P. Borovinskaya
  • Patent number: 6432150
    Abstract: A superabrasive containing layered composite is provided which comprises a substrate block consisting of either ceramic material and metallic or several metallic materials, and a superabrasive containing body adjacent said substrate block. The superabrasive contains superabrasive particles, and a metallic ingredient which is distributed in the superabrasive containing layer, including a working surface. The superabrasive material may be formed using a compression cell wherein the compression cell comprises a die defined by a vertical wall and a flat closed bottom. Placed in the die, in order from bottom upward, comprises a formed pallet of single body or layers of mixed powder forming a refractory compound, a material mass of a working layer containing diamond particles, a mass of ignition material comprising an SHS composition, and an electrical heating element.
    Type: Grant
    Filed: May 12, 2000
    Date of Patent: August 13, 2002
    Assignees: The Ishizuka Research Institute, Ltd., Moscow Steel and Alloys Institute, SHS-Center
    Inventors: Evgeny Alexandrovich Levashov, Alexander Sergeevich Rogatchov, Boris Vladmirovich Spitsin, Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi
  • Patent number: 6337060
    Abstract: The principal objects of the invention is to provide diamond fine particles with a surface nature so improved as to form a stable, uniform suspension or dispersion in a common medium such as water and alcohol. Another object is to provide an effective technique for producing hydrophilic diamond fine particles by chemically modifying the particle surface nature, while removing at the same time contaminants and foreign materials which coexist with the diamond. In the invention, diamond particles are treated by boiling in the treatment fluid of sulfuric acid solution, which is in particular of concentrated or fuming nature, at a temperature more than 200° C., which is preferably 250° C. or more.
    Type: Grant
    Filed: June 12, 1996
    Date of Patent: January 8, 2002
    Assignees: The Ishizuka Research Institute, Ltd.
    Inventors: Akio Hiraki, Toshimichi Ito, Akimitsu Hatta, Hiroshi Makita, Kazuhito Nishimura, Hiroshi Ishizuka, Satoru Hosomi
  • Patent number: 6336950
    Abstract: An aspect of this invention is an electrode rod for spark alloying, comprising a compact of a first powder of a first component which comprises a metal selected from a group of Fe, Co, Ni, metals of 4a, 5a and 6a of the periodic table and Si, and a second powder of a second component which is capable of self-propagating high temperature synthesis to form with said first component carbide, nitride, boride, silicide or intermetallic compound, said first and second powders being mixed intimately with each other and formed into an axial rod.
    Type: Grant
    Filed: May 5, 2000
    Date of Patent: January 8, 2002
    Assignees: The Ishizuka Research Institute Ltd., Moscow Steel and Alloys Institute, SHS-Center
    Inventors: Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi, Evgeny Alexandrovich Levashov, Alexander Gennadievich Nikolaev, Alexander Evgenievich Kudryashov
  • Patent number: 6203897
    Abstract: This invention provides a composite product and an effective method for producing the same, based on an SHS or intense heat producing process. Said composite essentially comprises either (1) one or more skeletal structures of three dimensionally joined pieces of at least one ceramic material selected from carbide, boride, nitride and silicide of titanium, zirconium, tantalum, niobium, silicon, chromium, tungsten, and molybdenum, and metallic material of alloy and/or intermetallic compound which fills the gaps within each and between adjacent skeletal structures, or (2) a matrix consisting of SHS products of metallic and/or ceramic substances, and particles of superabrasive selected from diamond and high pressure polymorphism of boron nitride, which are held and distributed in the matrix in the whole, in the surface or surface area comprising the portion corresponding to the end working face.
    Type: Grant
    Filed: August 12, 1996
    Date of Patent: March 20, 2001
    Assignees: The Ishizuka Research Institute, Ltd., Moscow Steel and Alloys Institute, SHS-Center
    Inventors: Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi, Evgeny A. Levashov, Alexander V. Trotsue, Inna P. Borovinskaya
  • Patent number: 6171709
    Abstract: The invention provides a superabrasive containing composite product, comprising and/or prepared on the intense heating of an SHS process, self-propagating high-temperature synthesis. An effective method of such product is also provided. Said composite comprises a substrate of shaped metallic block and a functional layer of ceramic materials containing superabrasive particles, which is joined on a surface of the former, by means of and intermediated by molten metal which occurred during the SHS process.
    Type: Grant
    Filed: May 11, 1998
    Date of Patent: January 9, 2001
    Assignees: The Ishizuka Research Institute, Ltd., Mitsue Koizumi, Manshi Ohyanagi, Moscow Steel and Alloys Institute, SHS-Center
    Inventors: Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi, Evgeny A. Levashov, Alexander V. Trotsue, Inna P. Borovinskaya
  • Patent number: 5882740
    Abstract: A method is provided for efficiently producing an entirely quality-controlled CVD diamond. A CVD process is interrupted at an early stage and the deposit is taken out of the reaction chamber, before a significant mass is accumulated, and is inspected by means of cathodoluminescence. The spectrum are compared with a given reference in terms of peak position, half width and 20%-value width in coordination. The observed deviation allows to determine whether to maintain or alter the settings.A diamond substance of acceptable quality which is properly specified in terms of the CL parameters is also provided.
    Type: Grant
    Filed: April 1, 1996
    Date of Patent: March 16, 1999
    Assignees: Ishizuka Research Institute Ltd., Ensei Ko, Osaka Diamond Industrial Co., Ltd
    Inventors: Chia-Fu Chen, Kazuhito Nishimura, Ensei Ko, Hiroshi Ishizuka, Satoru Hosomi
  • Patent number: 5510157
    Abstract: Making a diamond substance exhibiting a cathodoluminescence spectrum with the peak at a photon energy greater than 2.8 eV (electron volt), the half-value and 20%-value width not exceeding 0.5 eV and 0.8 eV, respectively, comprising: providing a substrate in a closed chamber, introducing a matrix gas comprising H.sub.2 and one selected from hydrocarbon and CO to said chamber, exciting the gas to create a plasma while heating said substrate to a temperature of at least 700.degree. C. and, thus, causing deposition and growth of diamond substance which is crystallographically diamond, controlling parameters of the deposition by means of the cathodoluminescence record and recovering the diamond substance from the chamber.
    Type: Grant
    Filed: November 6, 1991
    Date of Patent: April 23, 1996
    Assignees: Ishizuka Research Institute, Ltd., Ensei Ko, Osaka Diamond Industrial Co., Ltd.
    Inventors: Chia-Fu Chen, Kazuhito Nishimura, Ensei Ko, Hiroshi Ishizuka, Satoru Hosomi
  • Patent number: 5061292
    Abstract: Diamond abrasive comprising a mass of idiomorphic crystal grits which each have an irregular shaped core of diamond formed under pressure where diamond is thermodynamically favored phase, and a growth layer of diamond and/or diamond-like carbon formed over said core by chemical vapor deposition.
    Type: Grant
    Filed: July 13, 1989
    Date of Patent: October 29, 1991
    Assignees: The Ishizuka Research Institute, Ltd., Ensei Ko
    Inventors: Chia-Fu Chen, Ensei Ko, Hiroshi Ishizuka, Satoru Hosomi
  • Patent number: 4844988
    Abstract: A diamond composite combined with a cobalt-containing substrate, comprising: a sintered mass of diamond, in which practically all the diamond particles are joined immediately with adjacent particles, a mass of cobalt-containing carbide, said latter mass being larger than the former and said first and latter masses being of a same cross section at the opposed ends, and an intermediate layer of a solid material which consists of Mo, Co and C with a minor proportion of inevitable impurities and which comprises a molybdenum carbide exhibiting a melting point within 200 degrees C. of that of the first said carbide material, said layer intervening between the masses and having a total radial cross sectional area of at least 80% but not greater than 97% of that of the diamond mass and carbide masses at the joint and a thickness of, at least, 25 microns over the whole cross sectional area and method for producing the same.
    Type: Grant
    Filed: December 22, 1987
    Date of Patent: July 4, 1989
    Assignee: The Ishizuka Research Institute, Ltd.
    Inventors: Hiroshi Ishizuka, Satoshi Hayakawa
  • Patent number: 4596693
    Abstract: A method of producing a composite compact of cBN and WC-Co, comprising: mixing fine particles of cBN with a minor part of titanium carbide, the former being in an amount of 60-80% and the latter 40-20%, correspondingly, of the combined volume, putting the mixture in an intimate contact with a composite of WC-Co, heating the whole to a temperature high enough to cause an outflow of a liquid phase from said composite and infiltration thereof into said mixture under a pressure-temperature condition where cubic boron nitride is crystallographically stable, interjoining adjacent particles of cBN and titanium carbide, and as a whole to the composite of WC-Co, and recovering the integrated product of cBN, titanium carbide and WC-Co.
    Type: Grant
    Filed: September 16, 1985
    Date of Patent: June 24, 1986
    Assignee: The Ishizuka Research Institute Ltd.
    Inventors: Hiroshi Ishizuka, Shuhei Kuge