Patents Assigned to The United States of America as represented by the Secretary of Interior
  • Patent number: 5429887
    Abstract: A process for treating an AB.sub.5 Ni--MH battery to recover purified positive and negative electrode components of the battery is disclosed. An AB.sub.5 Ni--MH battery is placed in a mineral acid leach solution to cause the positive and negative electrode components of the battery to separate. The positive and negative electrode components are maintained in the leach solution until the negative electrode component breaks down into its dissolved rare earth metal constituents and metallic solids. The metallic solids remaining from the negative electrode component and the positive electrode components are separated from the mineral acid leach solution and subjected to an elutriation process and thereafter to ball milling to obtain Ni rich powder and Fe. The mineral acid leach solution containing the completely dissolved rare earth metals is subjected to a phosphate precipitation process to recover La and Ce in precipitate, and then subjected to a second precipitation process to recover Ni, Co, Mn and Al.
    Type: Grant
    Filed: May 16, 1994
    Date of Patent: July 4, 1995
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Jane W. Lyman, Glenn R. Palmer
  • Patent number: 5407253
    Abstract: The invention relates to a water spray ventilator system mounted on a continuous mining machine to streamline airflow and provide effective face ventilation of both respirable dust and methane in underground coal mines. This system has two side spray nozzles mounted one on each side of the mining machine and six spray nozzles disposed on a manifold mounted to the underside of the machine boom. The six spray nozzles are angularly and laterally oriented on the manifold so as to provide non-overlapping spray patterns along the length of the cutter drum.
    Type: Grant
    Filed: July 6, 1994
    Date of Patent: April 18, 1995
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Steven J. Page, Thomas Mal
  • Patent number: 5404834
    Abstract: An indicator device indicates that the temperature in a location in which the device is placed has exceeded a predetermined maximum temperature value. The he device includes a liquid receptacle comprising frangible bulb portion and an integral capillary portion and an absorbent card to which said receptacle is secured. The bulb portion contains a first liquid and the capillary portion contains a second liquid which is insoluble in said first liquid. The second liquid has a freezing point higher then that of the first liquid and close to but greater than the predetermined temperature value so that when the device is placed in a location which has temperature lower than the predetermined value and in which the predetermined value is to be maintained, the second liquid freezes in the capillary tube and prevents the first liquid from expanding.
    Type: Grant
    Filed: March 15, 1993
    Date of Patent: April 11, 1995
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventor: Andrew P. Murphy
  • Patent number: 5404946
    Abstract: A borehole probe containing one or more inflatable packers, usually, although not necessarily, in connection with geophysical sensors, is hung from a geophysical logging cable. The packers are inflated or deflated with liquid at ambient borehole pressure, advantageously, the liquid resident in the borehole, using a submersible, reversible electric pump which is part of the borehole packer assembly. The electric pump is powered and controlled from the surface through the interconnecting logging cable. A differential pressure actuated valve located between the pump and packer controls the flow of pumped fluid into and out of the packers. The packers may be used to control the movement of borehole fluid at any desired depth within a borehole, constrained only by the length of the interconnecting logging cable.
    Type: Grant
    Filed: August 2, 1993
    Date of Patent: April 11, 1995
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventor: Alfred E. Hess
  • Patent number: 5395426
    Abstract: A device and method for removing, concentrating and analyzing airborne organic compounds. The device includes a nonporous membrane which contains a collection media. The liquid collection media typically includes a component which has a molecular weight that is too large to pass through transport corridors in the nonporous membrane and a component which has a molecular weight which is sufficiently small enough to pass through the transport corridors in the nonporous membrane and thereby forming a thin film on the exterior surface of the device. The collection media can consist of only components too large to pass through the membrane transport corridors. Organic contaminants are trapped in the thin film on the exterior surface of the device or the membrane and transported by concentration gradient diffusion forces into the bulk of the collection media within the nonporous membrane.
    Type: Grant
    Filed: July 8, 1993
    Date of Patent: March 7, 1995
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: James N. Huckins, Jimmie D. Petty, James A. Zajicek, Virginia L. Gibson
  • Patent number: 5387273
    Abstract: A process for removing copper in a recoverable form from a copper/solid ferrous scrap metal mix is disclosed. The process begins by placing a copper/solid ferrous scrap metal mix into a reactor vessel. The atmosphere within the reactor vessel is purged with an inert gas or oxidizing while the reactor vessel is heated in the area of the copper/solid ferrous scrap metal mix to raise the temperature within the reactor vessel to a selected elevated temperature. Air is introduced into the reactor vessel and thereafter hydrogen chloride is introduced into the reactor vessel to obtain a desired air-hydrogen chloride mix. The air-hydrogen chloride mix is operable to form an oxidizing and chloridizing atmosphere which provides a protective oxide coating on the surface of the solid ferrous scrap metal in the mix and simultaneously oxidizes/chloridizes the copper in the mix to convert the copper to a copper monochloride gas for transport away from the solid ferrous scrap metal.
    Type: Grant
    Filed: December 28, 1993
    Date of Patent: February 7, 1995
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Alan D. Hartman, Laurance L. Oden, Jack C. White
  • Patent number: 5372195
    Abstract: A method for directional hydraulic fracturing using borehole seals to confine pressurized fluid in planar permeable regions, comprising: placing a sealant in the hole of a structure selected from geologic or cemented formations to fill the space between a permeable planar component and the geologic or cemented formation in the vicinity of the permeable planar component; making a hydraulic connection between the permeable planar component and a pump; permitting the sealant to cure and thereby provide both mechanical and hydraulic confinement to the permeable planar component; and pumping a fluid from the pump into the permeable planar component to internally pressurize the permeable planar component to initiate a fracture in the formation, the fracture being disposed in the same orientation as the permeable planar component.
    Type: Grant
    Filed: September 13, 1993
    Date of Patent: December 13, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: David E. Swanson, Daniel W. Daly
  • Patent number: 5368105
    Abstract: A cryogenic slurry comprising a mixture of solid carbon dioxide particles suspended in liquid nitrogen is provided which is useful in extinguishing underground fires.
    Type: Grant
    Filed: December 11, 1991
    Date of Patent: November 29, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Robert F. Chaiken, Ann G. Kim, Andrew M. Kociban, Joseph P. Slivon, Jr.
  • Patent number: 5366817
    Abstract: A corrosion resistant electrically conductive coating on steel anode studs used in the production of aluminum by electrolysis.
    Type: Grant
    Filed: April 27, 1992
    Date of Patent: November 22, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Laurance L. Oden, Jack C. White, James A. Ramsey
  • Patent number: 5366571
    Abstract: An improved emulsion explosive composition including hollow microspheres/bulking agents having high density and high strength. The hollow microspheres/bulking agents have true particle densities of about 0.2 grams per cubic centimeter or greater and include glass, siliceous, ceramic and synthetic resin microspheres, expanded minerals, and mixtures thereof. The preferred weight percentage of hollow microspheres/bulking agents in the composition ranges from 3.0 to 10.0 A chlorinated paraffin oil, also present in the improved emulsion explosive composition, imparts a higher film strength to the oil phase in the emulsion. The emulsion is rendered nonincendive by the production of sodium chloride in situ via the decomposition of sodium nitrate, a chlorinated paraffin oil, and sodium perchlorate. The air-gap sensitivity is improved by the in situ formation of monomethylamine perchlorate from dissolved monomethylamine nitrate and sodium perchlorate.
    Type: Grant
    Filed: January 15, 1993
    Date of Patent: November 22, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Thomas C. Ruhe, Pilaka P. Rao
  • Patent number: 5335977
    Abstract: A double acting bit holder that permits bits held in it to be resharpened during cutting action to increase energy efficiency by reducing the amount of small chips produced.
    Type: Grant
    Filed: May 26, 1993
    Date of Patent: August 9, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Roger J. Morrell, David A. Larson, Peter L. Ruzzi
  • Patent number: 5332509
    Abstract: A chemical process for selectively removing organometallic compounds from water supplies. The process utilizes a combination of a transition metal selected from the group consisting of nickel, copper, iron and zinc, and an electropositive metal selected from the group consisting of magnesium and aluminum to effectively remove organometallic compounds from water whether present in ionic or non-ionic form.
    Type: Grant
    Filed: February 24, 1993
    Date of Patent: July 26, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventor: Andrew P. Murphy
  • Patent number: 5324491
    Abstract: A method for removing uranium from uranium contaminated water involves adding uranium reducing microorganisms and an electron donor to uranium contaminated water to reduce U(VI) in the uranium contaminated water to U(IV) which in turn forms a UO.sub.2 precipitate The UO.sub.2 precipitate is then separated from the contaminated water.
    Type: Grant
    Filed: April 3, 1992
    Date of Patent: June 28, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventor: Derek R. Lovley
  • Patent number: 5324394
    Abstract: A method of producing lithium of high purity from lithium aluminum alloys using an engineered scavenger compound, comprising:I) preparing an engineered scavenger compound by: a) mixing and heating compounds of TiO2 and Li2CO3 at a temperature sufficient to dry the compounds and convert Li.sub.2 CO.sub.3 to Li.sub.2 O; and b) mixing and heating the compounds at a temperature sufficient to produce a scavenger Li.sub.2 O.3TiO.sub.
    Type: Grant
    Filed: October 5, 1992
    Date of Patent: June 28, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: W. D. Riley, B. W. Jong, Collins, W. K., S. J. Gerdemann
  • Patent number: 5322800
    Abstract: This invention concerns a method and apparatus for collecting and preserving field water samples on site in which a salt solution, contained in a syringe by a rupturable thin film membrane, is injected through a strong acid or base ion exchange filter to produce a required amount of either nitric acid, sulfuric acid or sodium hydroxide for sample collection and preservation.
    Type: Grant
    Filed: August 13, 1993
    Date of Patent: June 21, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventor: Andrew P. Murphy
  • Patent number: 5279745
    Abstract: Polymer beads are prepared containing an immobilized extractant for sorbing metal contaminants at concentrations of less than 1 mg/L in dilute aqueous solutions. A preferred polymer is polysulfone and the extractant can be a biomass material or a synthetic chemical compound sorbed into activated carbon. The polymer beads are prepared by dissolving the polymer in an organic solvent to form a solution, adding the extractant to the solution to form a mixture and injecting the mixture through a nozzle into water to form the beads.
    Type: Grant
    Filed: December 26, 1991
    Date of Patent: January 18, 1994
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Thomas H. Jeffers, Don C. Seidel
  • Patent number: 5271831
    Abstract: A method and apparatus for removing selenate from waste water through the use of selenate respiring microorganisms under substantially anoxic conditions is described. The method includes a first zone for removing nitrate by assimilation into biomass. The first zone is maintained under aerobic conditions and is separated from a second zone where selenate is respired to elemental selenium by selenate respiring microorganisms under anoxic conditions. Biomass produced in the first zone may be processed to provide nutrients and electron acceptors for the maintenance of selenate respiring microorganisms when selenate becomes growth limiting. An optional sulfate reduction zone is provided in the method and apparatus where hydrogen sulfide is produced. The hydrogen sulfide so produced is circulated to the second zone and may be used to reduce residual selenite to elemental selenium.
    Type: Grant
    Filed: December 14, 1990
    Date of Patent: December 21, 1993
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventor: Ronald S. Oremland
  • Patent number: 5265664
    Abstract: A method of casting metal using evaporative pattern casting process patterns in combination with a fixture for creating and maintaining a desired configuration in flexible patterns. A pattern is constructed and gently bent to the curvature of a suitable fixture. String or thin wire, which burns off during casting, is used to tie the pattern to the fixture. The fixture with pattern is dipped in a commercially available refractory wash to prevent metal adherence and sticking to the fixture. When the refractory wash is dry, the fixture and pattern are placed in a flask, and sand is added and compacted by vibration. The pattern remains in position, restrained by the fixture. Metal that is poured directly into the pattern replaces the pattern exactly but does not contact or weld to the fixture due to the protective refractory layer. When solid, the casting is easily separated from the fixture. The fixture can be cleaned for reuse in conventional casting cleaning equipment.
    Type: Grant
    Filed: December 27, 1991
    Date of Patent: November 30, 1993
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Paul C. Turner, Ronald R. Jordan, Jeffrey S. Hansen
  • Patent number: 5259862
    Abstract: A continuous process for producing a granular metal selected from the group consisting of Ti, Zr or Hf under conditions that provide orderly growth of the metal free of halide inclusions comprising:a) dissolving a reducing metal selected from the group consisting of Na, Mg, Li or K in their respective halide salts to produce a reducing molten salt stream;b) preparing a second molten salt stream containing the halide salt of Ti, Zr or Hf;c) mixing and reacting the two molten streams of steps a) and b) in a continuous stirred tank reactor;d) wherein steps a) through c) are conducted at a temperature range of from about 800.degree. C. to about 1100.degree. C. so that a weight percent of equilibrium solubility of the reducing metal in its respective halide salt varies from about 1.6 weight percent at about 900.degree. C. to about 14.4 weight percent at about 1062.degree. C.
    Type: Grant
    Filed: October 5, 1992
    Date of Patent: November 9, 1993
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Jack C. White, Laurance L. Oden
  • Patent number: 5256368
    Abstract: A pressure-reaction synthesis process for producing increased stiffness and improved strength-to-weight ratio titanium metal matrix composite materials comprising exothermically reacting a titanium powder or titanium powder alloys with non-metal powders or gas selected from the group consisting of C, B, N, BN, B.sub.4 C, SiC and Si.sub.3 N.sub.4 at temperatures from about 900.degree. to about 1300.degree. C., for about 5 to about 30 minutes in a forming die under pressures of from about 1000 to 5000 psi.
    Type: Grant
    Filed: July 31, 1992
    Date of Patent: October 26, 1993
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Laurance L. Oden, Thomas L. Ochs, Paul C. Turner