Abstract: In one aspect, an oxygenated hierarchically porous carbon (an “O-HPC”) is provided, the O-HPC comprising: a hierarchically porous carbon (an “UPC”), the HPC comprising a surface, the surface comprising: (A) first order pores having an average diameter of between about 1 ?m and about 10 ?m; and (B) walls separating the first order pores, the walls comprising: (1) second order pores having a peak diameter between about 7 nm and about 130 nm; and (2) third order pores having an average diameter of less than about 4 nm, wherein at least a portion of the HPC surface has been subjected to O2 plasma to oxygenate and induce a negative charge to the surface. In one aspect, the O-HPC further comprises metal nanoparticles dispersed within the first, second, and third order pores. Methods for making and using the metal nanoparticle-impregnated O-HPCs are also provided.

Abstract: In one aspect, an oxygenated hierarchically porous carbon (an “O-HPC”) is provided, the O-HPC comprising: a hierarchically porous carbon (an “HPC”), the HPC comprising a surface, the surface comprising: (A) first order pores having an average diameter of between about 1 ?m and about 10 ?m; and (B) walls separating the first order pores, the walls comprising: (1) second order pores having a peak diameter between about 7 nm and about 130 nm; and (2) third order pores having an average diameter of less than about 4 nm, wherein at least a portion of the HPC surface has been subjected to O2 plasma to oxygenate and induce a negative charge to the surface. In one aspect, the O-HPC further comprises metal nanoparticles dispersed within the first, second, and third order pores. Methods for making and using the metal nanoparticle-impregnated O-HPCs are also provided.

Abstract: In one aspect, an oxygenated hierarchically porous carbon (an “O-HPC”) is provided, the O-HPC comprising: a hierarchically porous carbon (an “HPC”), the HPC comprising a surface, the surface comprising: (A) first order pores having an average diameter of between about 1 ?m and about 10 ?m; and (B) walls separating the first order pores, the walls comprising: (1) second order pores having a peak diameter between about 7 nm and about 130 nm; and (2) third order pores having an average diameter of less than about 4 nm, wherein at least a portion of the HPC surface has been subjected to O2 plasma to oxygenate and induce a negative charge to the surface. In one aspect, the O-HPC further comprises metal nanoparticles dispersed within the first, second, and third order pores. Methods for making and using the metal nanoparticle-impregnated O-HPCs are also provided.

Abstract: A double chamber vacuum resin transfer molding process is provided comprising the initial step of providing a double chamber vacuum resin transfer molding apparatus comprising a first mold portion and a second mold portion. The first mold portion and the second mold portion are configured such that, in an engaged state, the first mold portion and the second mold portion define a mold cavity and a brim cavity. The mold cavity is isolated from the brim cavity by a compressible seal. Either or both of the first mold portion and the second mold portion are further configured to define an injection gate in communication with the mold cavity, a mold cavity vacuum port in communication with the mold cavity, and a brim cavity vacuum port in communication with the brim cavity. The first mold portion, the second mold portion, and the compressible seal are arranged such that a decrease in brim cavity pressure below atmospheric pressure causes a corresponding decrease in mold cavity volume.

Abstract: Two new classes of polysilahydrocarbons: Rn—Si—[CH2CH2—Si—R13](4−n)  (III) C6H(12−m)[CH2CH2SiR13]m  (IV) where R and R1 are alkyl groups having from 1 to 18 carbon atoms, “n” is an integer between 0 and 3, and “m” is an integer between 2 and 6. Lubricant compositions containing the new polysilahydrocarbons are disclosed. Methods of making the new polysilahydrocarbons are also disclosed.

Abstract: A method is provided for forming a highly conductive metal-containing polymer fiber or sheet in which a polymer is immersed in a solution containing a metal precursor selected from organic or inorganic salts of copper, silver, aluminum, gold, iron and nickel. The metal precursor is then reduced by chemical, electrochemical, or thermal means such that conductive metal is incorporated into the polymer.

Abstract: A method for processing thermally intractable rigid-chain polymers into shaped structural articles is provided. The method includes dissolving a rigid-chain polymer in sulfuric acid at a concentration and temperature sufficient to form a nematic liquid crystalline solution which is then formed into a shaped article and cooled to a solid. The solution undergoes a phase transformation upon cooling from a liquid crystalline phase to a solid phase containing crystal solvates. The method allows rigid-chain polymers to be formed into fibers, bulk structural components, fiber reinforced composites and other structural materials without undergoing significant shrinkage or deformation.

Abstract: Solid composite electrolytes are provided for use in lithium batteries which exhibit moderate to high ionic conductivity at ambient temperatures and low activation energies. In one embodiment, a polymer-ceramic composite electrolyte containing poly(ethylene oxide), lithium tetrafluoroborate and titanium dioxide is provided in the form of an annealed film having a room temperature conductivity of from 10−5 S cm−1 to 10−3 S cm−1 and an activation energy of about 0.5 eV.

Abstract: Solid composite electrolytes are provided for use in lithium batteries which exhibit moderate to high ionic conductivity at ambient temperatures and low activation energies. In one embodiment, a ceramic-ceramic composite electrolyte is provided containing lithium nitride and lithium phosphate. The ceramic-ceramic composite is also preferably annealed and exhibits an activation energy of about 0.1 eV.

Abstract: The present invention is directed to an apparatus and method for recovering the group III elemental component of a group III-V material waste material. The method includes heating, under a reduced pressure, solid waste materials which contain group III-V material to cause the group III-V material to separate into a group III element and a group V element vapor; drawing off the group V element vapor; condensing the group V element vapor to produce a condensed group V element solid; and zone refining the group III element to produce a purified group III element. The apparatus is designed to carry out this method in the plant which manufactures the group III-V waste material.

Abstract: A thermal energy transport and storage system is provided which includes an evaporator containing a mixture of a first phase change material and a silica powder, and a condenser containing a second phase change material. The silica powder/PCM mixture absorbs heat energy from a source such as a solar collector such that the phase change material forms a vapor which is transported from the evaporator to the condenser, where the second phase change material melts and stores the heat energy, then releases the energy to an environmental space via a heat exchanger. The vapor is condensed to a liquid which is transported back to the evaporator. The system allows the repeated transfer of thermal energy using the heat of vaporization and condensation of the phase change material.

Abstract: A method and apparatus for producing ordered parts by stereolithography from non-ordered liquid crystal monomers. Liquid crystal monomers contain stiff, rod-like mesogenic segments which can be aligned by an external force such as shear, electric field or magnetic field, causing an anisotropy in properties. When cured in the aligned stated by photopolymerizing the aligned monomers the anisotropic structure is "locked in" resulting in materials with anisotropic physical and mechanical properties. The rigid structure of the mesogenic segments can result in cured networks with high glass transition temperatures if the spacer groups which connect the mesogenic core with the reactive end groups are kept short. Glass transition temperatures of postcured parts ranged from 75 to 148.degree. C. depending on resin and processing conditions. A mechanical anisotropy on the order of two was measured for aligned samples.

Abstract: A thermal energy storage composition is provided which is in the form of a gel. The composition includes a phase change material and silica particles, where the phase change material may comprise a linear alkyl hydrocarbon, water/urea, or water. The thermal energy storage composition has a high thermal conductivity, high thermal energy storage, and may be used in a variety of applications such as in thermal shipping containers and gel packs.

Abstract: A system for actively damping low frequency noise in an enclosure is provided comprising an acoustic wave sensor, and acoustic wave actuator, and an electronic feedback loop. The acoustic wave actuator is substantially collocated with the acoustic wave sensor within an enclosure. The electronic feedback loop is operative to generate a signal at its output by applying a feedback loop transfer function. The feedback loop transfer function comprises a selected second order differential equation including a first variable representing a predetermined damping coefficient and a second variable representing a tuned natural frequency. The transfer function defines a frequency response having a characteristic maximum gain substantially corresponding to the value of the tuned natural frequency and creates a 90 degree phase lead substantially at the tuned natural frequency. The feedback loop output signal represents a rate of change of volume velocity to be produced by the acoustic wave actuator.

Abstract: The present invention is directed to a method for separating the group III element component of a group III-V material from an aqueous waste containing a group III-V material to allow for their recovery and beneficial use. The method includes adjusting the pH of an aqueous waste containing a group III-V material to a pH from about 9.5 to about 12.5 by adding an alkali metal hydroxide base to the aqueous waste; precipitating a group V element oxyanion by adding a soluble alkaline metal salt to the aqueous waste; separating the group V element oxyanion from the aqueous waste; adjusting the pH of the aqueous waste to form a group III element hydroxide precipitate by adding a mineral acid to the aqueous waste; separating the group III element hydroxide precipitate from the aqueous waste; and recovering the group III element from the group III element hydroxide precipitate.

Abstract: A method and apparatus are disclosed for the analysis of a fluid to determine the remaining useful life of the fluid and whether the fluid has become contaminated. The method can be performed either on-line or off-line, however, the on-line method is preferred. In the method, a sample of the fluid is contacted by a single electrode which is connected to the ground potential by means of the equipment in which the fluid is used. A current is applied to the sample through the electrode and the conductivity of the sample is measured. The conductivity measurement can then compared to known values for the fluid to determine the remaining useful life of the fluid and whether the fluid has become contaminated.

Abstract: The present invention relates to a method and apparatus which can be used to detect the abnormal operating condition of equipment, such as engines and machinery, the usefulness of the fluid, and the content of wear metals and elemental constituents in the fluid. The method comprises the steps of bringing at least two electrodes into contact with a sample of a fluid to be analyzed; applying a square voltage wave form to the electrodes at a predetermined scan range and scan rate to cause a current to flow between the electrodes; monitoring the current at the electrodes to determine a current output signal; using the current output signal to measure the conductivity of the fluid; and analyzing the sample to determine a content of wear metals and elemental constituents in the sample.

Abstract: The present invention is directed to a fiber composition comprising a fiber forming polymer and a phase change material integrally incorporated throughout the fiber forming polymer which is either a polyalkylene oxide, polyalkylene ether or mixture of various polyolefins. The phase change material has a melting temperature between about 15.degree. C. and about 65.degree. C. The fiber composition can be used as a loose fill insulating material for use in clothing or bedding articles or can be formed into a fabric for the same uses.

Abstract: An ultrasonic transducer is provided comprising a transducer housing, a piezoelectric assembly, and a seating assembly. The transducer housing includes a front end, a rear end opposite the front end, and an ultrasonic window positioned at the front end. The piezoelectric assembly is positioned within the transducer housing and comprises a piezoelectric assembly substrate and a piezoelectric laminate formed over a front surface of the assembly substrate. The seating assembly is arranged to secure the piezoelectric assembly within the transducer housing such that at least a portion of the piezoelectric laminate is aligned with the ultrasonic window. The transducer housing, the assembly substrate, and the seating assembly are preferably constructed of high temperature and high pressure materials characterized by substantially equivalent coefficients of thermal expansion.

Abstract: A magnetostrictive actuator is provided comprising an actuator base, a magnetostrictive assembly, an actuator frame, and a flexible disk. The magnetostrictive assembly includes a magnetostrictive element. A first end of the magnetostrictive element is mechanically coupled to the actuator base. A first portion of the actuator frame is mechanically coupled to the actuator base. The flexible disk includes a perimetrical disk portion and a bearing surface portion. The perimetrical disk portion is mechanically coupled to the second frame portion and the bearing surface portion is mechanically coupled to the second magnetostrictive element end portion. The magnetostrictive actuator comprises a magnetostrictive material portion and a plurality of cooling fluid bores formed within the magnetostrictive material portion.