Abstract: The present invention is thus directed to an automated system of varying the optical path length in a sample that a light from a spectrophotometer must travel through. Such arrangements allow a user to easily vary the optical path length while also providing the user with an easy way to clean and prepare a transmission cell for optical interrogation. Such path length control can be automatically controlled by a programmable control system to quickly collect and stores data from different path lengths as needed for different spectrographic analysis. Moreover, the system utilizes configured wedge shaped windows to best minimize the reflections of light which cause periodic variation in transmission at different wave lengths (commonly described as “channel spectra”). Such a system, as presented herein, is able to return best-match spectra with far fewer computational steps and greater speed than if all possible combinations of reference spectra are considered.

Abstract: A chromatographic material comprising a zwitterionic ligand covalently bound to a substrate, the ligand preferably has a formula II: wherein R1, R2, R3 are independently selected from an oxygen atom that is configured to connect to a substrate atom in the substrate, an oxygen atom that is configured to connect to a silicon atom of an adjacent ligand, a hydroxyl group, a halogen atom, an alkoxy group, a dialkylamino group, an acyl group, an alkyl group, or an aryl group; L1, L2 and L3 are independently hydrophobic moieties; each containing 2 to 30 carbon atoms, wherein there are at least 10 carbon atoms in the combined chain lengths of L1, L2 and L3; X is an O atom, S atom, amide group or sulfonamide group; n is 0 or 1; R4, R5 are independently selected from a hydrogen atom or a hydrocarbon moiety containing 1 to 20 carbon atoms; and Rf is a negatively charged moiety comprising a sulfonic, carboxylic, or phosphonic functional group.

Abstract: The present invention relates to a drive head for detachable connection of a drive with a rotor of a centrifuge, comprising: a base body which is rotatable about an axis of rotation (R) and at least one coupling element, which is mounted on the base body such that it is movable between a release position (F) and a locking position (V), the coupling element protruding further beyond the outer circumference of the base body in the locking position (V) than in the release position (F). The coupling element is arranged so as to be linearly movable between the release position (F) and the locking position (V) in such a way that a plane (E), along which the coupling element is movable, is inclined relative to a sectional plane (S) extending perpendicularly to the axis of rotation (R), the coupling element having a resting surface in its outer end region, which runs parallel to the sectional plane (S).

Abstract: A rheometer or viscometer has a first measuring part and a second measuring part, between which a sample space for receiving a material sample is formed. By means of a drive device, at least the second measuring part can be rotated and/or can be oscillated, it being possible for the drive movement of the drive device to be transferred to the second measuring device via a transmission element. The drive device is arranged on the side of the first measuring part that is facing away from the second measuring part and the transmission element penetrates through the first measuring part, particularly at a through-bore.

Abstract: The invention relates to an extruder which has an extruder housing. The housing has at least two housing parts and is provided with a delivery channel in order to extrude a medium, at least one screw conveyor being located in said channel. The extruder housing is releasably retained on a frame by means of a first retaining device and a shaft section of the screw conveyor is releasably connected to a drive device. According to the invention the housing parts are fixed relative to one another by means of a second retaining device and the extruder housing is connected to the frame and secured against displacement in the longitudinal direction of the extruder housing by means of a third retaining device. When the first and third retaining device) are released, the housing parts can be removed as a unit from the frame.

Abstract: The present invention is thus directed to an automated system and method of varying the optical path length in a sample that a light from a spectrophotometer must travel through. Such arrangements allow a user to easily vary the optical path length while also providing the user with an easy way to clean and prepare a transmission cell for optical interrogation. Such path length control can be automatically controlled by a programmable control system to quickly collect and stores data from different path lengths as needed for different spectrographic analysis. Such a methodology and system, as presented herein, is able to return best-match spectra with far fewer computational steps and greater speed than if all possible combinations of reference spectra are considered.

Abstract: The invention relates to an extruder which has an extruder housing, in which a delivery channel for a medium to be extruded is formed. At least one screw conveyor is located in the delivery channel and a cooling device is provided for the extruder housing, said device having at least one cooling line in or on the extruder housing, through which line a cooling fluid flows. An electronic device for controlling and/or regulating the operating states of the extruder is accommodated in an electronics housing which can be cooled according to the invention by means of the cooling device for the extruder housing.

Abstract: The present invention is thus directed to an automated system of varying the optical path length in a sample that a light from a spectrophotometer must travel through. Such arrangements allow a user to easily vary the optical path length while also providing the user with an easy way to clean and prepare a transmission cell for optical interrogation. Such path length control can be automatically controlled by a programmable control system to quickly collect and stores data from different path lengths as needed for different spectrographic analysis. Moreover, the system utilizes configured wedge shaped windows to best minimize the reflections of light which cause periodic variation in transmission at different wave lengths (commonly described as “channel spectra”). Such a system, as presented herein, is able to return best-match spectra with far fewer computational steps and greater speed than if all possible combinations of reference spectra are considered.

Abstract: A novel emission and transmission optical spectrometer is introduced herein, which is capable of optically interrogating solid or liquid samples of organic, inorganic or polymeric chemistry, for pharmaceutical research, forensic and liquid analyses, used for identification, purity check, and/or structural study of chemicals. The beneficial aspects of the system are a single sample compartment as confined within the walls of the spectrometer housing, a more compact accessory, and the capability of making both emission (e.g., Raman and Fluorescence) and Infrared (IR, NIR) transmission measurements at designed sample points.

Abstract: A particulate material for chromatographic use comprising silica particles is provided having a skeleton structure containing silsesquioxane cage moieties. The material is useful as a chromatographic material, for example in HPLC. The silica particles may be hybrid organo-silica particles wherein the silsesquioxane moieties comprise a cage structure having silicon atoms positioned at corners of the cage wherein one or more silicon atoms positioned at the corners of the cage carry an organic group. A preferred method of preparing the particulate material comprises hydrolysing a silsesquioxane as a co-component of a hydrolysis mixture, especially in a Stöber or modified Stöber process.

Abstract: An all-graphite interferometer bearing assembly is introduced that allows the movement of a movable mirror in a Michelson interferometer without degradation during use. The assembly includes a stationary hollow graphite tube and a movable assembly which includes a mirror and a monolithic graphite member slidably disposed within the bore of the graphite tube that is composed of the same grade of graphite material as the monolithic graphite member. The result is a robust novel moving mirror arrangement in a Michelson interferometer that enables precise mirror alignment control, a long stroke length, excellent vibration damping and reduced sensitivity to external vibrations.

Abstract: A novel means of provided velocity control of an interferometer wherein one of the moving components includes the beamsplitter element is introduced herein. Using a moving beamsplitter and coupled flexure mounting allows improved velocity control because the low mass of the beamsplitter enables the systems disclosed herein to respond faster than conventional mirror velocity controlled interferometer instruments with a resultant lower velocity error so as to provide a more stable and lower noise spectra from the analytical instrument. The control of the velocity of the beamsplitter and if desired, one or both of the configured mirrors, reduces the time wasted changing velocity at the ends of each scan. The result is an increase in data collection available in any given experiment time frame. Such desirable arrangements of the present invention thus allow scans to be collected at higher rates, which beneficially increase the ability to monitor rapidly changing systems.

Abstract: An infrared (IR) source apparatus that includes a desired infrared source element coupled to an insulating housing so to minimize overall source inefficiency at desired optical bandwidths is introduced. The insulation itself is machined or configured in a way so that the infrared source element is in contact with a designed cavity in the insulation so that the IR source image becomes the average of the insulation material and the infrared element. Such an arrangement of the present invention increases the emissivity of the IR source below about 1500 wave numbers, more often, below about 1100 wave numbers, and even more particularly, at about 1079 wave numbers. Accordingly, the combined emissivity of the infrared source and the insulation substantially enhances spectral emission and eliminates or reduces spectral artifacts from the formation of oxides on the infrared source surfaces.

Abstract: The present invention is thus directed to an automated system of varying the optical path length in a sample that a light from a spectrophotometer must travel through. Such arrangements allow a user to easily vary the optical path length while also providing the user with an easy way to clean and prepare a transmission cell for optical interrogation. Such path length control can be automatically controlled by a programmable control system to quickly collect and stores data from different path lengths as needed for different spectrographic analysis. Moreover, the system utilizes configured wedge shaped windows to best minimize the reflections of light which cause periodic variation in transmission at different wave lengths (commonly described as “channel spectra”). Such a system, as presented herein, is able to return best-match spectra with far fewer computational steps and greater speed than if all possible combinations of reference spectra are considered.

Abstract: A novel means of provided a hybrid flexure mounted moving mirror component in an interferometer is introduced herein. In particular, a linear bearing in combination with a novel flexure mounting having novel tilt and velocity control of the moving optical component is provided. Such an arrangement enables correction of the errors at the mirror itself while also solving the problem of isolating vibration and noise caused by the imperfections in the bearing surfaces used in many conventional interferometers. Using such a coupled flexure mounting of the present invention, in addition to the above benefits, also enhances velocity control because the resultant low mass of the moving mirror assembly enables the systems disclosed herein to respond faster than conventional mirror velocity controlled interferometer instruments and with a lower velocity error so as to provide a more stable and lower noise spectra from the analytical instrument.

Abstract: The present invention relates to a laboratory centrifuge having a cooling device which comprises a compressor enclosed by a compressor housing, with the compressor housing, in the region of the compressor head, being at least regionally provided with a damping material which is capable of absorbing vibrations in the range from 20 Hz to 100 Hz.

Abstract: A novel soft beamsplitter mounting system as part of an interferometer to protect the beamsplitter substrate from external stresses and thus preserve optical flatness is introduced. The soft mounting system enables such protection by being more flexible that the beamsplitter substrate so external forces deforms the mount rather than the beamsplitter. Although the soft beamsplitter mounting configurations disclosed herein protects the beamsplitter, the interferometer itself is less stable because the mounts of the present invention allows the beamsplitter to tilt more easily than other components held in the interferometer. The improved tilt control embodiments of the present invention turns this seemingly deleterious effect into a cost saving benefit by using the inexpensive soft mounting system as a flexure to allow an improved active control system to maintain tilt alignment in a system that is more rugged than conventional interferometers.