Abstract: A large capacity centrifugal vacuum concentrator includes a rotor assembly mounting a plurality of vertical spaced rotors mounted on a drive shaft and intervened with spacers between each lower rotor and a rotor next above, the rotors and spacers having interengaging drive transmission means for transmitting drive to the rotors and spacers when the drive shaft is driven. The rotor assembly is enclosed by a, e.g., cylindrical stainless steel cover which sits on a base and with the base defines a vacuum chamber. When the cover is elevated to open position, four quadrant access is available for loading and unloading of samples on the rotors. The rotor assembly is made up of interchangeable rotors, spacers and vessel holder frames which are selected from families of such dependent on particular vessel capacity and holder frame requirements.

Abstract: A condenser cold trap unit for recovering as separate primary and secondary condensate fractions solvents contained in an effluent drawn from products being dried in a vacuum chamber includes inner and outer shell vessels, the inner shell vessel be disposed coaxially with the outer shell vessel inside said outer shell vessel with a space being present in the outer shell vessel under the bottom of the inner shell vessel and in a course surrounding the exterior of the inner shell vessel. A cover closes off the open tops of the two shell vessels and the interior space of the outer shell vessel is sealed from communication with outside atmosphere, and the interior space of the inner shell vessel is sealed from any communication with the interior space of the outer shell vessel. A common refrigeration coil encircles the exterior of the inner shell vessel and extends down therefrom to effect solvents condensing temperature levels cooling in both shell vessels.