Abstract: A process for recovering residual uranium from emptied uranium hexafluoride shipping cylinder during cleaning, including rinsing a uranium hexafluoride shipping cylinder with hydrofluoric acid to dissolve a heel of uranium hexafluoride therein to form a mixture of sediment, precipitates and a uranium solution; separating the uranium solution from the sediment and precipitates; mixing sodium hydroxide with the uranium solution to precipitate sodium diuranate; separating the solid sodium diuranate from the sodium fluoride solution formed; re-dissolving the sodium diuranate in sodium carbonate solution to form uranyl carbonate complex solution; and adjusting the pH of uranyl carbonate complex solution further to precipitate uranyl peroxide with the addition of hydrogen peroxide. Sodium fluoride solution produced is further treated to remove fluoride by percolating it through a calcite limestone bed to form calcium fluoride solid.

Abstract: A tilt roll table for use with uranium hexafluoride cylindrical containers securely holds the container, supported from its domed ends by spindles mounted to brackets as the container is tilted and rolled. The spindles have greater surface area over which to distribute the weight and are shaped to complement the domed container ends. The brackets supporting the spindles, stiffened by vertical and horizontal braces, can be adjusted vertically and moved axially toward and away from the domed ends of the containers by a gear drive to accommodate different sizes of cylindrical containers. In addition, bands encircle the containers to hold them onto the frame during tilting and rolling.