Abstract: A low friction wear surface with a coefficient of friction in the superlubric regime including graphene and nanoparticles on the wear surface is provided, and methods of producing the low friction wear surface are also provided. A long lifetime wear resistant surface including graphene exposed to hydrogen is provided, including methods of increasing the lifetime of graphene containing wear surfaces by providing hydrogen to the wear surface.
Type:
Grant
Filed:
June 19, 2014
Date of Patent:
February 7, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Anirudha V. Sumant, Diana Berman, Ali Erdemir
Abstract: A lithium-sulfur electrochemical cell includes a cathode including elemental sulfur; an anode including elemental lithium; and an electrolyte including a salt and a non-polar fluorinated ether solvent. Alternatively, a lithium-sulfur electrochemical cell may include an anode; an electrolyte; and a cathode including a polytetrafluoroethylene-coated carbon paper and sulfur.
Abstract: Provided herein are methods and devices to enrich trace quantities of impurities in gaseous mixtures, such as hydrogen fuel. The methods and devices rely on concentration of impurities so as to allow the detection of the impurities using commonly-available detection methods.
Type:
Grant
Filed:
June 20, 2014
Date of Patent:
January 31, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Shabbir Ahmed, Dionissios D. Papadias, Sheldon D. H. Lee, Romesh Kumar
Abstract: A process for forming a surface-treatment layer on an electroactive material includes heating the electroactive material and exposing the electroactive material to a reducing gas to form a surface-treatment layer on the electroactive material, where the surface-treatment layer is a layer of partial reduction of the electroactive material.
Type:
Grant
Filed:
May 25, 2011
Date of Patent:
January 31, 2017
Assignee:
UCHICAGO ARGONNE, LLC
Inventors:
Khalil Amine, Ali Abouimrane, Ilias Belharouak
Abstract: An article of manufacture and method of forming a borided material. An electrochemical cell is used to process a substrate to deposit a plurality of borided layers on the substrate. The plurality of layers are co-deposited such that a refractory metal boride layer is disposed on a substrate and a rare earth metal boride conforming layer is disposed on the refractory metal boride layer.
Type:
Grant
Filed:
January 17, 2014
Date of Patent:
January 31, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Ali Erdemir, Vivekanand Sista, Ozgenur Kahvecioglu, Osman Levent Eryilmaz
Abstract: Methods and compositions to control the stability of proteins with special emphasis on antibodies and proteins with antibody-like structures, e.g., having an “immunoglobulin-like” fold, are described. Controlling the stability facilitates different applications for a protein with the same function, but different stability.
Abstract: A nonreciprocal device is described. It includes a housing, a waveguide layer and at least one layer of magnetic nanofiber composite. The magnetic nanofiber composite layer is made up of a polymer base layer, a dielectric matrix comprising magnetic nanofibers. The nanofibers have a high aspect ratio and wherein said dielectric matrix is embedded in the polymer base layer.
Abstract: A two-dimensional thin film transistor and a method for manufacturing a two-dimensional thin film transistor includes layering a semiconducting channel material on a substrate, providing a first electrode material on top of the semiconducting channel material, patterning a source metal electrode and a drain metal electrode at opposite ends of the semiconducting channel material from the first electrode material, opening a window between the source metal electrode and the drain metal electrode, removing the first electrode material from the window located above the semiconducting channel material providing a gate dielectric above the semiconducting channel material, and providing a top gate above the gate dielectric, the top gate formed from a second electrode material. The semiconducting channel material is made of tungsten diselenide, the first electrode material and the second electrode material are made of graphene, and the gate dielectric is made of hexagonal boron nitride.
Type:
Grant
Filed:
April 21, 2015
Date of Patent:
January 17, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Saptarshi Das, Anirudha V. Sumant, Andreas Roelofs
Abstract: A nanopositioning system for producing a coupling interaction between a first nanoparticle and a second nanoparticle. A first MEMS positioning assembly includes an electrostatic comb drive actuator configured to selectively displace a first nanoparticle in a first dimension and an electrode configured to selectively displace the first nanoparticle in a second dimensions. Accordingly, the first nanoparticle may be selectively positioned in two dimensions to modulate the distance between the first nanoparticle and a second nanoparticle that may be coupled to a second MEMS positioning assembly. Modulating the distance between the first and second nanoparticles obtains a coupling interaction between the nanoparticles that alters at least one material property of the nanoparticles applicable to a variety of sensing and control applications.
Type:
Grant
Filed:
December 10, 2014
Date of Patent:
January 17, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Daniel Lopez, Gary Wiederrecht, David J. Gosztola, Derrick C. Mancini
Abstract: A method for coating a substrate comprises producing a plasma ball using a microwave plasma source in the presence of a mixture of gases. The plasma ball has a diameter. The plasma ball is disposed at a first distance from the substrate and the substrate is maintained at a first temperature. The plasma ball is maintained at the first distance from the substrate, and a diamond coating is deposited on the substrate. The diamond coating has a thickness. Furthermore, the diamond coating has an optical transparency of greater than about 80%. The diamond coating can include nanocrystalline diamond. The microwave plasma source can have a frequency of about 915 MHz.
Abstract: A method comprising irradiating a polycrystalline rare earth metal-alkaline earth metal-transition metal-oxide superconductor layer with protons having an energy of 1 to 6 MeV. The irradiating process produces an irradiated layer that comprises randomly dispersed defects with an average diameter in the range of 1-10 nm.
Type:
Grant
Filed:
March 17, 2014
Date of Patent:
January 10, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Ulrich Welp, Dean J. Miller, Wai-Kwong Kwok, Martin W. Rupich, Steven Fleshler, Alexis P. Malozemoff
Abstract: Briefly, the invention provides a method for magnetically assisting demulsification of extraction phases, the method having the steps of contacting a first solution of a first solvent and a solvated paramagnetic metal ion with a second solvent, where the second solvent is immiscible with the first solvent; mixing the first and second solutions to create an emulsion having a first phase of the first solvent and second phase comprising the second solvent where the phases of the emulsion contain different concentrations of the paramagnetic metal ion; and applying a magnetic field gradient to the first and second phases of the emulsion to accelerate separation of the first phase from the second phase. Also provided is a system for demulsifying phases used in the extraction of paramagnetic moieties from solution having a lumen with an interior region, an interior surface, and exterior surface; and a magnetic field gradient present within the interior region.
Abstract: A process for preparing intermetallic nanoparticles of two or more metals is provided. In particular, the process includes the steps: a) dispersing nanoparticles of a first metal in a solvent to prepare a first metal solution, b) forming a reaction mixture with the first metal solution and a reducing agent, c) heating the reaction mixture to a reaction temperature; and d) adding a second metal solution containing a salt of a second metal to the reaction mixture. During this process, intermetallic nanoparticles, which contain a compound with the first and second metals are formed. The intermetallic nanoparticles with uniform size and a narrow size distribution is also provided. An electrochemical device such as a battery with the intermetallic nanoparticles is also provided.
Type:
Grant
Filed:
November 3, 2015
Date of Patent:
January 3, 2017
Assignee:
UChicago Argonne, LLC
Inventors:
Dileep Singh, Yusuf Yusufoglu, Elena Timofeeva, Jules L. Routbort
Abstract: The invention provides a process for forming crack-free dielectric films on a substrate. The process comprises the application of a dielectric precursor layer of a thickness from about 0.3 ?m to about 1.0 ?m to a substrate. The deposition is followed by low temperature heat pretreatment, prepyrolysis, pyrolysis and crystallization step for each layer. The deposition, heat pretreatment, prepyrolysis, pyrolysis and crystallization are repeated until the dielectric film forms an overall thickness of from about 1.5 ?m to about 20.0 ?m and providing a final crystallization treatment to form a thick dielectric film. The process provides a thick crack-free dielectric film on a substrate, the dielectric forming a dense thick crack-free dielectric having an overall dielectric thickness of from about 1.5 ?m to about 20.0 ?m.
Abstract: An X-ray article and method for analyzing hard X-rays which have interacted with a test system. The X-ray article is operative to diffract or otherwise process X-rays from an input X-ray beam which have interacted with the test system and at the same time provide an electrical circuit adapted to collect photoelectrons emitted from an X-ray optical element of the X-ray article to analyze features of the test system.
Type:
Grant
Filed:
September 30, 2013
Date of Patent:
December 27, 2016
Assignee:
UChicago Argonne, LLC
Inventors:
Stanislav Stoupin, Yury Shvydko, John Katsoudas, Vladimir D. Blank, Sergey A. Terentyev
Abstract: Nickel-containing carbon nanofiber (NiCNF) materials and lubricants comprising the nanofiber materials are described herein. The NiCNF materials comprise a plurality of elongate nickel-containing carbon nanofibers. Each NiCNF comprises a carbon nanofiber shaft that is capped at one end by a nickel nanoparticle encapsulated in multiple layers of graphitic carbon. The nanofibers typically have a generally circular cross-section (i.e., in the direction perpendicular to the length-axis of the fibers). The NiCNF materials as useful, e.g., in lubricant compositions, which also are described herein.
Type:
Application
Filed:
August 29, 2016
Publication date:
December 22, 2016
Applicant:
UCHICAGO ARGONNE, LLC
Inventors:
Ali ERDEMIR, Vilas G. POL, Michael M. THACKERAY, Kuldeep MISTRY, Qiuying CHANG
Abstract: A microcalorimeter for radiation detection that uses superconducting kinetic inductance resonators as the thermometers. The detector is frequency-multiplexed which enables detector systems with a large number of pixels.
Type:
Grant
Filed:
April 10, 2014
Date of Patent:
December 20, 2016
Assignee:
UChicago Argonne, LLC
Inventors:
Thomas Cecil, Lisa Gades, Antonio Miceli, Orlando Quaranta
Abstract: A method, apparatus, and system are provided for monitoring environment parameters of critical facilities. A Remote Area Modular Monitoring (RAMM) apparatus is provided for monitoring environment parameters of critical facilities. The RAMM apparatus includes a battery power supply and a central processor. The RAMM apparatus includes a plurality of sensors monitoring the associated environment parameters and at least one communication module for transmitting one or more monitored environment parameters. The RAMM apparatus is powered by the battery power supply, controlled by the central processor operating a wireless sensor network (WSN) platform when the facility condition is disrupted. The RAMM apparatus includes a housing prepositioned at a strategic location, for example, where a dangerous build-up of contamination and radiation may preclude subsequent manned entrance and surveillance.
Type:
Grant
Filed:
June 16, 2014
Date of Patent:
December 13, 2016
Assignee:
UChicago Argonne, LLC
Inventors:
Hanchung Tsai, John T. Anderson, Yung Y. Liu
Abstract: A system for monitoring a plurality radio frequency identification tags is described. The system uses at least one set of radio frequency identification tags. Each tag is attached to a container and includes several sensors for detecting physical conditions of said container. The system includes at least one autonomous intermediate reader in wireless communication with the frequency identification tags. The intermediate reader includes external wireless communication system, intermediate reader logic controller, and a self-contained rechargeable power supply. The system uses a central status reporting system in communication the intermediate reader.
Type:
Grant
Filed:
August 4, 2014
Date of Patent:
December 6, 2016
Assignee:
UChicago Argonne, LLC
Inventors:
Han-Chung Tsai, Yung Y. Liu, Hok L. Lee, Brian Craig, Kevin Byrne, Ketan Mittal, Justin C. Scherer