Abstract: A process to manufacture substituted tetracyano-hexaazatricyclics with the substitutions occurring at the 9 and 10 hydrogens. The process begins with 2,3-dichloro-5,6-dicyanopyrazine, which is reacted to form the desired tetracyano-hexaazatricyclic. Different process embodiments enable different reaction paths to the desired tetracyano-hexaazatricyclic. Different tetracyano-hexaazatricyclic embodiments include bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene and bis(2-methoxyethoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene.
Type:
Grant
Filed:
December 2, 2012
Date of Patent:
June 3, 2014
Assignee:
Vinazene, Inc.
Inventors:
Paul George Rasmussen, Richard Graham Lawton
Abstract: An electrical storage device utilizing a pyrazine-based cyanoazacarbon or pyrazine-based cyanoazacarbon polymer as a redox active material which can undergo both oxidation and reduction. The device has an ion selective barrier with a cathode side and an anode side; a cathode compartment which is functionally attached to the cathode side of the ion selective barrier and contains a mixture of pyrazine-based cyanoazacarbons, solvent, and positive ions of pyrazine-based cyanoazacarbons; an anode compartment which is functionally attached to the anode side of the ion selective barrier and contains a mixture of pyrazine-based cyanoazacarbons, solvent, and negative ions of pyrazine-based cyanoazacarbons; a cathode which is electrically connected to the cathode compartment; and an anode which is electrically connected to the anode compartment.