Patents Assigned to Vitaworks IP, LLC
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Patent number: 11851395Abstract: There is disclosed a process for producing taurine in a molar yield of at least 80% from alkali isethionate, alkali ditaurinate, or alkali tritaurinate by adding excess ammonia and at least of equal molar amount of an alkali hydroxide to a solution comprised of alkali ditaurinate, alkali tritaurinate, or their mixture and subjecting the solution to an ammonolysis to yield a solution comprised of alkali taurinate.Type: GrantFiled: February 17, 2023Date of Patent: December 26, 2023Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 11845714Abstract: There is disclosed a process for producing taurine in a molar yield of at least 80% from alkali isethionate, alkali ditaurinate, or alkali tritaurinate by adding excess ammonia and at least of equal molar amount of an alkali hydroxide to a solution comprised of alkali ditaurinate, alkali tritaurinate, or their mixture and subjecting the solution to an ammonolysis to yield a solution comprised of alkali taurinate.Type: GrantFiled: February 16, 2023Date of Patent: December 19, 2023Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 11623914Abstract: There is disclosed a cyclic process for producing taurine from monoethanolamine comprising the steps of: (a) recovering monoethanolamine sulfate from an aqueous mother liquor solution; (b) reacting the monoethanolamine sulfate with sulfuric acid to form an aqueous solution comprised of monoethanolamine bisulfate; (c) heating the aqueous solution comprised of the monoethanolamine sulfate and optionally added monoethanolamine sulfate to yield 2-aminoethyl hydrogen sulfate ester; and (d) reacting the ester with ammonium sulfite or an alkali sulfite to yield taurine.Type: GrantFiled: January 14, 2022Date of Patent: April 11, 2023Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 11578036Abstract: There is disclosed a process for recovering monoethanolamine from an aqueous mother liquor solution comprising the steps of: (a) adding excess ammonia or alkali hydroxide and a solvent to the aqueous solution comprised of monoethanolamine sulfate and at least one component selected from the group of inorganic salts consisting of ammonium sulfate, ammonium sulfite, alkali sulfite, and alkali sulfate, to precipitate the inorganic salts, wherein the alkali is lithium, sodium, or potassium; (b) separating the inorganic salts by means of a solid-liquid separation to yield an aqueous solution comprised of the monoethanolamine; and (c) distilling the solvent to yield an aqueous solution comprised of the monoethanolamine and optionally purifying the MEA by distillation. The recovered MEA is recycled to produce taurine.Type: GrantFiled: September 9, 2020Date of Patent: February 14, 2023Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 11384050Abstract: There is disclosed a method for preparing levetiracetam and intermediates from a compound of the formula: wherein CR is selected from the group consisting of cyano, carboxylic acid, carboxamide, alkali carboxylate, alkaline earth metal carboxylate, alkyl carboxylate, and a mixture thereof.Type: GrantFiled: February 3, 2021Date of Patent: July 12, 2022Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 11254639Abstract: There is disclosed a cyclic process for producing taurine from monoethanolamine comprising the steps of: (a) recovering monoethanolamine sulfate from an aqueous mother liquor solution; (b) reacting the monoethanolamine sulfate with sulfuric acid to form an aqueous solution comprised of monoethanolamine bisulfate; (c) heating the aqueous solution comprised of the monoethanolamine sulfate and optionally added monoethanolamine sulfate to yield 2-aminoethyl hydrogen sulfate ester; (d) reacting the ester with ammonium sulfite or an alkali sulfite to yield taurine and ammonium or alkali sulfate; (e) separating taurine and ammonium or alkali sulfate to give an aqueous mother liquor solution; and (f) recovering the monoethanolamine sulfate from the aqueous mother liquor solution and recycling to the monoethanolamine sulfate to step (b).Type: GrantFiled: September 9, 2020Date of Patent: February 22, 2022Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 11161808Abstract: There is disclosed a cyclic process for producing taurine from monoethanolamine comprising the steps of: (a) reacting monoethanolamine with ammonium sulfate in the recycling mother liquor to yield monoethanolamine sulfate; (b) reacting the monoethanolamine sulfate with sulfuric acid to form 2-aminoethyl hydrogen sulfate ester; (c) subjecting the 2-aminoethyl hydrogen sulfate ester to a sulfonation reaction with ammonium sulfite to yield taurine and ammonium sulfate; (d) separating the taurine and the ammonium sulfate by means of solid-liquid separation; (e) removing the excess ammonium sulfite from the mother liquor to obtain an aqueous solution comprised of ammonium sulfate and (f) returning the aqueous solution to step (a) to complete the cyclic process.Type: GrantFiled: September 9, 2020Date of Patent: November 2, 2021Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 10961183Abstract: There is disclosed a process for producing alkali taurinate by the ammonolysis of alkali ditaurinate, alkali tritaurinate, or a solution of alkali ditaurinate and alkali tritaurinate in the presence of one or more catalysts. The ammonolysis reaction is catalyzed by alkali salts of hydroxide, sulfate, sulfite, phosphate, or carbonate.Type: GrantFiled: July 9, 2018Date of Patent: March 30, 2021Assignee: VITAWORKS IP, LLCInventor: Songzhou Hu
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Patent number: 10899700Abstract: There is disclosed a process for the separation of long chain amino acid and long chain dibasic acid, comprising: (1) adding an ammonium salt to the mixture of alkali salts of long chain amino acid and long chain dibasic acid; (2) heating to remove ammonia; and (3) separating long chain amino acid by solid-liquid separation; and (4) acidifying the salt of long chain dibasic acid with an acid to separate long chain dibasic acid.Type: GrantFiled: December 17, 2019Date of Patent: January 26, 2021Assignee: Vitaworks IP, LLCInventors: Songzhou Hu, Zhen Song
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Patent number: 10822300Abstract: There is disclosed a process for the production of dodecanedioic acid and 11-aminoundecanoic acid, comprising: (1) reacting castor oil with a primary or secondary amine to form a amide; (2) isomerizing the amide in the presence of a catalyst to form ketoamide; (3) reacting the ketoamide with hydroxylamine to form the oximeamide; (4) subjecting the oximeamide to Beckmann rearrangement to yield a mixture of two diamides; and (5) hydrolyzing the mixed diamides to produce dodecanedioic acid, 11-aminoundecanoic acid, hexylamine and heptanoic acid.Type: GrantFiled: June 10, 2019Date of Patent: November 3, 2020Assignee: VITAWORKS IP, LLCInventors: Songzhou Hu, Zhen Song
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Patent number: 10793517Abstract: There is disclosed a process for producing taurine by subjecting an ammonia solution ammonium isethionate in the presence of a hydrogenation catalyst and hydrogen to an ammonolysis reaction to form ammonium taurinate. Taurine is obtained by decomposing ammonium taurinate to taurine and ammonia and recovered by solid-liquid separation.Type: GrantFiled: January 8, 2020Date of Patent: October 6, 2020Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: 10683264Abstract: There is disclosed a process for producing taurine by reacting 2-oxazolidinone with ammonium sulfite, or ammonium bisulfite, or a mixture of ammonium sulfite and ammonium bisulfite in an aqueous solution to form ammonium taurinate and ammonium bicarbonate. Taurine is obtained by decomposing ammonium taurinate to taurine and ammonia and recovered by solid-liquid separation.Type: GrantFiled: November 27, 2018Date of Patent: June 16, 2020Assignee: VITAWORKS IP, LLCInventor: Songzhou Hu
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Publication number: 20200181070Abstract: There is disclosed a process for producing taurine by subjecting an ammonia solution ammonium isethionate in the presence of a hydrogenation catalyst and hydrogen to an ammonolysis reaction to form ammonium taurinate. Taurine is obtained by decomposing ammonium taurinate to taurine and ammonia and recovered by solid-liquid separation.Type: ApplicationFiled: January 8, 2020Publication date: June 11, 2020Applicant: Vitaworks IP, LLCInventor: Songzhou Hu
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Publication number: 20200157041Abstract: There is disclosed a process for the separation of long chain amino acid and long chain dibasic acid, comprising: (1) adding an ammonium salt to the mixture of alkali salts of long chain amino acid and long chain dibasic acid; (2) heating to remove ammonia; and (3) separating long chain amino acid by solid-liquid separation; and (4) acidifying the salt of long chain dibasic acid with an acid to separate long chain dibasic acid.Type: ApplicationFiled: December 17, 2019Publication date: May 21, 2020Applicant: Vitaworks IP, LLCInventors: Songzhou Hu, Zhen Song
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Patent number: RE48238Abstract: A process for producing taurine from alkali ditaurinate or alkali tritaurinate, or their mixture, comprising the conversion of alkali ditaurinate to dialkali ditaurinate or alkali tritaurinate to trialkali tritaurinate, or their mixture, the ammonolysis reaction of ammonia added to a solution of dialkali ditaurinate or trialkali tritaurinate, or their mixture, to yield alkali taurinate, removing excess ammonia from the foregoing and neutralizing alkali taurinates with an acid to form a crystalline suspension of taurine, and recovering taurine by means of solid-liquid separation.Type: GrantFiled: April 8, 2020Date of Patent: October 6, 2020Assignee: VITAWORKS IP, LLCInventor: Songzhou Hu
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Patent number: RE48333Abstract: A process for producing taurine from alkali ditaurinate or alkali tritaurinate, or their mixture, comprising the conversion of alkali ditaurinate to dialkali ditaurinate or alkali tritaurinate to trialkali tritaurinate, or their mixture, the ammonolysis reaction of ammonia added to a solution of dialkali ditaurinate or trialkali tritaurinate, or their mixture, to yield alkali taurinate, removing excess ammonia from the foregoing and neutralizing alkali taurinates with an acid to form a crystalline suspension of taurine, and recovering taurine by means of solid-liquid separation.Type: GrantFiled: April 21, 2020Date of Patent: December 1, 2020Assignee: VITAWORKS IP, LLCInventor: Songzhou Hu
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Patent number: RE48354Abstract: A process for producing taurine from alkali ditaurinate or alkali tritaurinate, or their mixture, comprising the conversion of alkali ditaurinate to dialkali ditaurinate or alkali tritaurinate to trialkali tritaurinate, or their mixture, the ammonolysis reaction of ammonia added to a solution of dialkali ditaurinate or trialkali tritaurinate, or their mixture, to yield alkali taurinate, removing excess ammonia from the foregoing and neutralizing alkali taurinates with an acid to form a crystalline suspension of taurine, and recovering taurine by means of solid-liquid separation.Type: GrantFiled: April 21, 2020Date of Patent: December 15, 2020Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: RE48369Abstract: There is disclosed a process for producing taurine by the ammonolysis of alkali isethionate in the presence of alkali ditaurinate or alkali tritaurinate, or their mixture, to inhibit the formation of byproducts and to continuously convert the byproducts of the ammonolysis reaction to alkali taurinate. The production yield is increased to from 90% to nearly quantitative. The ammonolysis reaction is catalyzed by alkali salts of hydroxide, sulfate, sulfite, phosphate, or carbonate.Type: GrantFiled: April 7, 2020Date of Patent: December 29, 2020Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: RE48392Abstract: A cyclic process is disclosed for the production of taurine from alkali isethionate in a high overall yield by continuously converting the byproducts of the ammonolysis reaction, sodium ditaurinate and sodium tritaurinate, to sodium taurinate. Sodium sulfate and residual taurine in the crystallization mother liquor are efficiently separated by converting taurine into a highly soluble form of sodium taurinate or ammonium taurinate while selectively crystallizing sodium sulfate.Type: GrantFiled: April 30, 2020Date of Patent: January 12, 2021Assignee: Vitaworks IP, LLCInventor: Songzhou Hu
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Patent number: RE49370Abstract: A method is disclosed for the production of taurine in high yield by a cyclic process of reacting monoethanolamine, sulfuric acid, and ammonium sulfite in the presence of additives to inhibit the hydrolysis of 2-aminoethyl hydrogen sulfate intermediate. The cyclic process is economical and little waste is generated.Type: GrantFiled: June 8, 2020Date of Patent: January 17, 2023Assignee: Vitaworks IP, LLCInventor: Songzhou Hu