Abstract: The present invention relates to a method for preparing high-purity vanadium pentoxide from vanadium-bearing shale by all-wet process. The technical solution is: the “Gradient continuous leaching system of vanadium-bearing shale” is used to wet activate and compound leach vanadium-bearing shale to obtain vanadium-containing acid leachate. The “pH adjusting device of the vanadium-containing acid leachate” is used to adjust the pH of vanadium-containing acid leaching leachate. The post-treatment solution is subjected to hydroxime countercurrent extraction after oxidation, and the raffinate returns to the water using in the wet activation and electrodialysis after neutralization, and the loaded organic phase is regenerated by countercurrent reduction stripping. The regenerated organic phase directly returns to hydroxime countercurrent extraction.

Abstract: The disclosure relates to a method for simulating intraplate volcanism. A technical solution is: mixing 47-60 wt % of calcium oxide powder, 35 wt % of alumina powder and 5-18 wt % of silica powder uniformly to obtain a mixed powder; putting the mixed powder in a corundum crucible, placing the crucible in a high-temperature furnace provided with an observation window outside which an industrial camera with a depression angle of 30-45° is provided, heating to 1,500-1,900° C. at a rate of 1-30° C./min under an air atmosphere at a normal pressure, holding for 0.5-5 h; recording intraplate volcanism formed by upwelling of a melt of the mixed powder along an inner wall of the crucible during the holding with the industrial camera to obtain a simulated process of the intraplate volcanism.

Abstract: The disclosure relates to a method for fabricating a speckle for high temperature deformation measurement of a shaped refractory material. A technical solution includes mixing a hercynite micropowder and a liquid mixing agent in a mass ratio of (3-6):1, and ultrasonically treating to obtain a speckle mixture; polishing a surface of a shaped refractory material to be measured, removing impurities, and spraying the speckle mixture on the surface of the shaped refractory material to be measured with a pneumatic airbrush in a time hood to obtain an uncured speckle; heating the uncured speckle to 60-80° C., keeping for 1-3 h, then heating to 100-120° C., and keeping for 1-3 h to obtain a speckle for high temperature deformation measurement of a shaped refractory material. The fabricated product is suitable for high temperature deformation measurement of a shaped refractory material at 1,600° C.

Abstract: A titanium-containing calcium hexaaluminate material and preparation method thereof is disclosed. The technical solution is: using 60˜80 wt % alumina micro powder, 5˜20 wt % calcium-containing micro powder, 10˜20 wt % titania micro powder and 1˜10 wt % manganese oxide micro powder as raw materials, blending the raw materials evenly in a planetary ball mill to obtain a blend, machine pressing the blend at 100˜200 MPa to obtain a green body, drying the green body at 110˜200° C. for 12˜36 h, and incubating the dried green body at 1500˜1800° C. for 1˜8 h to obtain the titanium-containing calcium hexaaluminate material. The present disclosure has low cost and simple process, and the prepared titanium-containing calcium hexaaluminate material has the characteristics of good chemical stability, high thermal shock resistance and strong melt resistance to titanium-aluminum alloy.

Abstract: A spiral-orifice ceramic filter for metal casting, including spiral channels and two drain openings, where the spiral channels are distributed in a ceramic substrate in a staggered manner. By adoption of the spiral channel structure, molten metal may rotate to generate a centrifugal force while flowing forwards so as to promote separation of inclusions. The spiral-orifice ceramic filter for metal casting includes the following components: 90-95 wt % of MgO, 4-8 wt % of SiO2 and 2-4 wt % of ZrO2. Therefore, the spiral-orifice ceramic filter for metal casting has high strength under normal temperature and optional thermal impact resistance under high temperature, and may tolerate the impact of molten metal at 1700° C. or higher without break. The ceramic substrate and the spiral channel are superficially coated with one layer of functional oxide prepared from CaO.2Al2O3, CaO.6Al2O3, Al2O3, TiO2, or Re2O3.

Abstract: The disclosure provides a method for determining a slope slip plane with a gently-inclined soft interlayer, including: S1, determining a curve formed with a slip arc of a trailing edge tearing plane, a soft interlayer plane and a slip arc of a leading edge shear opening as a slope slip plane; S2, calculating a slip plane stability coefficient; S3, determination of a position of the gently-inclined soft interlayer plane: if the slip plane stability coefficient is less than 1 but close to 1, determining that the position of the slope slip plane is accurate; otherwise, moving the position of the soft interlayer plane and repeating steps S1 and S2, until the slip plane stability coefficient is less than 1 and close to 1. The method is simple, and has a high accuracy for determining a non-circular slip plane with a soft interlayer as a bottom slip plane.

Abstract: The present disclosure relates to a magnesium-based raw material and a preparation method thereof. According to the technical solution, 40-60 wt % fused magnesia particles, 30-40 wt % fine monoclinic zirconia powder, 5-20 wt % fine zirconium oxychloride powder, 0.5-1.5 wt % calcium hydroxide nanopowder, 0.2-0.5 wt % calcium hydroxide nanopowder, and 0.1-0.3 wt % maleic acid are stirred for 15 min to mix well in a high-speed mixing mill at a constant temperature of 25° C. to obtain a mixed powder; and the mixed powder is mixed through a ball mill at a constant temperature of 25° C. for 3 min, roasted in a high temperature furnace at 250-400° C. for 0.5-3 h, and finally cooled to room temperature.

Abstract: The present invention discloses an optimization method for a screen surface dynamic load of a vibrating screen. The method includes the following steps: step 1. selecting design variables, and establishing an experimental matrix; step 2. performing a response curved surface experiment; step 3. establishing two double-objective optimization models and solving the same to obtain two groups of Pareto solution sets, wherein the solution sets respectively represent screening efficiency optimization paths of the vibrating screen under the conditions of a high screen surface dynamic load and a low screen surface dynamic load; and step 4. calculating an optimization space for a screen surface dynamic load under a high screening efficiency. According to the method of the present invention, the screen surface dynamic load can be directly reduced, and the service life of the screen surface and the whole vibrating screen is prolonged.

Abstract: The present invention discloses an optimization method for a screen surface dynamic load of a vibrating screen. The method includes the following steps: step 1. selecting design variables, and establishing an experimental matrix; step 2. performing a response curved surface experiment; step 3. establishing two double-objective optimization models and solving the same to obtain two groups of Pareto solution sets, wherein the solution sets respectively represent screening efficiency optimization paths of the vibrating screen under the conditions of a high screen surface dynamic load and a low screen surface dynamic load; and step 4. calculating an optimization space for a screen surface dynamic load under a high screening efficiency. According to the method of the present invention, the screen surface dynamic load can be directly reduced, and the service life of the screen surface and the whole vibrating screen is prolonged.

Abstract: The present invention provides a microalloyed steel mechanical property prediction method based on globally additive model, including the following steps: determining some influencing factors of the microalloyed steel mechanical property prediction model; calculating the components and contents of carbonitride precipitation in a microalloyed steel rolling process; expressing the microalloyed steel mechanical property prediction model as an additive form of several submodels according to generalized additive model; estimating the microalloyed steel mechanical property prediction model; and verifying reliability of the submodels. The microalloyed steel property prediction models obtained in the foregoing solution have advantages such as high prediction precision and a wide adaptation range, and may be used for design of new products and steel grade component optimization, so as to reduce the quantity of physical tests, shorten the product research and development cycle, and reduce costs.

Abstract: A nonlinear resonance model-based active filtering crane steel rope resonance elimination control method, including: constructing a two-dimensional dynamic model of a bridge crane according to a Lagrange's equation; constructing a steel wire rope-motor nonlinear resonance model to detect a harmonic; and eliminating the harmonic by means of active filtering. The present disclosure makes in-depth study on positioning of a crane and intelligent control of an anti-swing and resonance elimination control system and uses active filtering to eliminate resonance between a heavy object and the steel wire rope, thereby reducing a swinging angle and achieving the rapid resonance elimination and anti-swing effect. The active filtering technology can quickly and effectively detect a resonance current so as to effectively suppress resonance between the heavy object and the steel wire rope, and further helps a controller quickly and accurately position a trolley to further improve anti-swing performance.

Abstract: A shear box of shear rheology experiment of a soft rock for simulating the coupling of the rainfall seepage and blasting vibration includes an upper shear box, a lower shear box, a normally-loading indenter, a normally-loading cushion block and a test piece joint. The upper shear box is tightly connected to the lower shear box by a vertical roll. The vertical roll passes through the through holes at both sides of the upper shear box and is engaged with the lower shear box through female thread connection holes. The normally-loading indenter passes through a circular through hole and presses against the normally-loading cushion block. The first end of the test piece joint is installed into a water or gas outlet hole, and the second end of the test piece joint is directly mortised into a rock test piece.

Abstract: The present disclosure provides a method for determining free radicals of CaO—Al2O3 series oxide melts. The method includes dividing the CaO—Al2O3 series oxide powder to into two aliquots by mass, putting into two identical corundum crucibles and tamping. The method also includes heating the two aliquots at the same high temperature in furnaces with and without a static magnetic field, respectively. Cylindrical samples with the same diameter and height, and only containing the melt at the bottom of the crucible and the slag reaction interface are drilled out from said two crucibles and ground into powder samples. The free radical relative content of the CaO—Al2O3 series oxide melts can be calculated from a ratio between the difference of the reaction mass contents of CaO in the two powder samples and the total mass content of CaO.

Abstract: The invention provides a method for purifying silicon by means of a phase separation dealloying reaction, including: mixing a silicon raw material containing metallic or non-metallic impurities with magnesium powder first and then fully reacting under an inert atmosphere so as to obtain a first product; placing the first product in a nitrogen-containing atmosphere to undergo a nitriding reaction to form three-dimensional porous silicon and magnesium nitride distributed in pore channels thereof so as to obtain a second product, the impurities further being separated during the precipitation and crystallization of silicon, and being dissolved in the liquid-phase magnesium nitride; treating the second product by using acid-pickling, the magnesium nitride and impurities being dissolved and converted into a solution, and a solid product being high-purity porous silicon.

Abstract: A nonlinear resonance model-based active filtering crane steel rope resonance elimination control method, including: constructing a two-dimensional dynamic model of a bridge crane according to a Lagrange's equation; constructing a steel wire rope-motor nonlinear resonance model to detect a harmonic; and eliminating the harmonic by means of active filtering. The present disclosure makes in-depth study on positioning of a crane and intelligent control of an anti-swing and resonance elimination control system and uses active filtering to eliminate resonance between a heavy object and the steel wire rope, thereby reducing a swinging angle and achieving the rapid resonance elimination and anti-swing effect. The active filtering technology can quickly and effectively detect a resonance current so as to effectively suppress resonance between the heavy object and the steel wire rope, and further helps a controller quickly and accurately position a trolley to further improve anti-swing performance.

Abstract: The present disclosure relates to a magnesium-based raw material with low thermal conductivity and low thermal expansion and a preparation method thereof. According to the technical solution, 40-60 wt % fused magnesia particles, 30-40 wt % fine monoclinic zirconia powder, 5-20 wt % fine zirconium oxychloride powder, 0.5-1.5 wt % calcium hydroxide nanopowder, 0.2-0.5 wt % calcium hydroxide nanopowder, and 0.1-0.3 wt % maleic acid are stirred for 15 min to mix well in a high-speed mixing mill at a constant temperature of 25° C. to obtain a mixed powder; and the mixed powder is mixed through a ball mill at a constant temperature of 25° C. for 3 min, roasted in a high temperature furnace at 250-400° C. for 0.5-3 h, and finally cooled to room temperature. The magnesium-based refractory material prepared has the advantages of relatively low thermal conductivity, low thermal expansion coefficient, excellent dispersibility, and strong resistance to slag penetration and erosion.

Abstract: A preparation method of an ant nest like porous silicon for a lithium-ion battery comprises: (1) enabling a magnesium silicide raw material to react for 2-24 h in an ammonia gas or an atmosphere containing an ammonia gas at 600-900° C. to obtain a crude product containing porous silicon; and (2) subjecting the crude product containing porous silicon to an acid pickling treatment to obtain the ant nest like porous silicon. The preparation method has the advantages of simplicity and easiness. A large amount of porous silicon can be obtained by directly heating the magnesium silicide raw material in the ammonia gas or a mixed gas of the ammonia gas and an inert gas with a high yield.

Abstract: The disclosure relates to a phase change thermal storage ceramic having high service temperature and improved utilization rate and utilization efficiency of heat. It is prepared at a low cost with a simple, easy-to-industrially-realized method. A mixture is obtained by mixing and stirring evenly 50-85 wt % of fused mullite powder, 10-45 wt % of pretreated aluminum-silicon alloy powder, and 3-8 wt % of ball clay. A ceramic body is formed by press molding the mixture at 80-150 MPa. The ceramic body is cured at 25-28° C. and a relative humidity of 70-75 RH for 24-36 h, dried at 80-120° C. for 24-36 h, and held at 1,100-1,300° C. for 3-5 h to prepare the phase change thermal storage ceramic. The pretreated aluminum-silicon alloy powder is prepared by holding aluminum-silicon alloy powder in water vapor at 0.02-0.20 MPa for 0.5-3 h to impregnate in an alkaline silica sol and drying the impregnated powder.

Abstract: A multi-police-officer collaborative round-up task allocation and path planning method under the constraint of a road network, including: acquiring a road topological map G of the road network; acquiring police officer distribution information and information of a task target location in the G of the road network; according to the position where the task target appears, a set of nodes that the task target is next likely to reach are determined; acquiring the movement speed of police officers and the task target; confirming a set of police officers to be assigned according to an interception point set and the movement speed of the police officers and the task target; calculating the congestion degree of each intersection in the interception point set; building a multi-police-officer collaborative round-up task allocation and path planning optimization model; solving the optimization model to obtain a multi-police-officer collaborative round-up task allocation and path planning scheme.

Abstract: A titanium-containing calcium hexaaluminate material and preparation method thereof is disclosed. The technical solution is: using 60˜80 wt % alumina micro powder, 5˜20 wt % calcium-containing micro powder, 10˜20 wt % titania micro powder and 1˜10 wt % manganese oxide micro powder as raw materials, blending the raw materials evenly in a planetary ball mill to obtain a blend, machine pressing the blend at 100˜200 MPa to obtain a green body, drying the green body at 110˜200° C. for 12˜36 h, and incubating the dried green body at 1500˜1800° C. for 1˜8 h to obtain the titanium-containing calcium hexaaluminate material. The present disclosure has low cost and simple process, and the prepared titanium-containing calcium hexaaluminate material has the characteristics of good chemical stability, high thermal shock resistance and strong melt resistance to titanium-aluminum alloy.