Patents Assigned to Zeochem
  • Patent number: 10099201
    Abstract: A molecular sieve blend containing a zeolite, particularly a zeolite X or A, blended with a halloysite clay binder, wherein the binder contains at least 90% by weight halloysite clay, with a particle length less than about 1 ?m and processes for the production and use of this blend, particularly for adsorption of water from a feedstream and for the production of oxygen.
    Type: Grant
    Filed: February 5, 2016
    Date of Patent: October 16, 2018
    Assignee: ZEOCHEM LLC
    Inventors: Kerry Weston, Jim Palmore, Dave Jaussaud
  • Patent number: 9925522
    Abstract: A material for reverse phase chromatography comprises surface modifying apolar and charged groups bound to a solid support, said charged groups being present in amounts of about 0.25 to about 22% of the surface modifying groups, or in amounts of about 0.01 ?mol/m2 to 0.8 ?mol/m2 referred to the surface of the solid support for a material with a total amount of surface modifying groups of 3.6 ?mol/m2. Such material and suitable purification conditions for active pharmaceutical ingredients (APIs) like peptides can be evaluated by (a) determining the isoelectric point (pI) of the API of interest, (b) choosing a pH in a range where the solid phase material is stable, (c) determining the difference pI?pH and (d) if the difference pI?pH is positive, choosing an anion exchange (AIEX) material, or if the difference pI?pH is negative, choosing an cation exchange (CIEX) material.
    Type: Grant
    Filed: March 21, 2013
    Date of Patent: March 27, 2018
    Assignee: ZEOCHEM AG
    Inventors: Nicola Forrer, Mandy Erdmann, David Gétaz, Massimo Morbidelle, Susanna Bernardi, Rushd Khalaf
  • Patent number: 9555401
    Abstract: A molecular sieve blend with improved performance characteristics produced by preparing or obtaining a hydrophilic zeolite, particularly a hydrophilic zeolite A with a low SiO2:Al2O3 ratio, preparing or obtaining a hydrophobic silicon based binder, particularly a hydrophobic colloidal silica or a hydrophobic siloxane based material, mixing the zeolite with the silicon based binder and, in one embodiment, a seed containing small quantities of a clay binding agent and the zeolite, to form a mixture, and forming the mixture into the molecular sieve blend.
    Type: Grant
    Filed: March 24, 2014
    Date of Patent: January 31, 2017
    Assignee: ZEOCHEM LLC
    Inventors: Kerry Weston, Patrick Purcell
  • Publication number: 20150087816
    Abstract: A material for reverse phase chromatography comprises surface modifying apolar and charged groups bound to a solid support, said charged groups being present in amounts of about 0.25 to about 22% of the surface modifying groups, or in amounts of about 0.01 ?mol/m2 to 0.8 ?mol/m2 referred to the surface of the solid support for a material with a total amount of surface modifying groups of 3.6 ?mol/m2. Such material and suitable purification conditions for active pharmaceutical ingredients (APIs) like peptides can be evaluated by (a) determining the isoelectric point (pI) of the API of interest, (b) choosing a pH in a range where the solid phase material is stable, (c) determining the difference pI-pH and (d) if the difference pI-pH is positive, choosing an anion exchange (AIEX) material, or if the difference pI-pH is negative, choosing an cation exchange (CIEX) material.
    Type: Application
    Filed: March 21, 2013
    Publication date: March 26, 2015
    Applicant: ZEOCHEM AG
    Inventors: Nicola Forrer, Mandy Erdmann, David Gétaz, Massimo Morbidelle, Susanna Bernardi, Rushd Khalaf
  • Patent number: 8969633
    Abstract: A process for the production of a molecular sieve blend with improved performance characteristics produced by preparing or obtaining a hydrophilic zeolite, particularly a hydrophilic zeolite A with a low SiO2:Al2O3 ratio, preparing or obtaining a hydrophobic silicon based binder, particularly a hydrophobic colloidal silica or a hydrophobic siloxane based material, mixing the zeolite with the silicon based binder and, in one embodiment, a seed containing small quantities of a clay binding agent and the zeolite, to form a mixture, and forming the mixture into the molecular sieve blend.
    Type: Grant
    Filed: March 24, 2014
    Date of Patent: March 3, 2015
    Assignee: Zeochem LLC
    Inventors: Kerry Weston, Patrick Purcell
  • Publication number: 20140221702
    Abstract: A process for the production of a molecular sieve blend with improved performance characteristics produced by preparing or obtaining a hydrophilic zeolite, particularly a hydrophilic zeolite A with a low SiO2:Al2O3 ratio, preparing or obtaining a hydrophobic silicon based binder, particularly a hydrophobic colloidal silica or a hydrophobic siloxane based material, mixing the zeolite with the silicon based binder and, in one embodiment, a seed containing small quantities of a clay binding agent and the zeolite, to form a mixture, and forming the mixture into the molecular sieve blend.
    Type: Application
    Filed: March 24, 2014
    Publication date: August 7, 2014
    Applicant: ZEOCHEM LLC
    Inventors: Kerry Weston, Patrick Purcell
  • Publication number: 20140217324
    Abstract: A molecular sieve blend with improved performance characteristics produced by preparing or obtaining a hydrophilic zeolite, particularly a hydrophilic zeolite A with a low SiO2:Al2O3 ratio, preparing or obtaining a hydrophobic silicon based binder, particularly a hydrophobic colloidal silica or a hydrophobic siloxane based material, mixing the zeolite with the silicon based binder and, in one embodiment, a seed containing small quantities of a clay binding agent and the zeolite, to form a mixture, and forming the mixture into the molecular sieve blend.
    Type: Application
    Filed: March 24, 2014
    Publication date: August 7, 2014
    Applicant: ZEOCHEM LLC
    Inventors: Kerry Weston, Patrick Purcell
  • Patent number: 8680344
    Abstract: A process for the production and use of a molecular sieve blend with improved performance characteristics produced by preparing or obtaining a hydrophilic zeolite, particularly a hydrophilic zeolite 3A with a low SiO2:Al2O3 ratio, preparing or obtaining a hydrophobic silica binder, particularly a hydrophobic colloidal silica, mixing the zeolite with the silica binder to form a mixture, and forming the mixture into the molecular sieve blend.
    Type: Grant
    Filed: January 25, 2011
    Date of Patent: March 25, 2014
    Assignee: Zeochem LLC
    Inventors: Kerry C. Weston, Patrick Purcell
  • Publication number: 20120190900
    Abstract: A process for the production and use of a molecular sieve blend with improved performance characteristics produced by preparing or obtaining a hydrophilic zeolite, particularly a hydrophilic zeolite 3A with a low SiO2:Al2O3 ratio, preparing or obtaining a hydrophobic silica binder, particularly a hydrophobic colloidal silica, mixing the zeolite with the silica binder to form a mixture, and forming the mixture into the molecular sieve blend.
    Type: Application
    Filed: January 25, 2011
    Publication date: July 26, 2012
    Applicant: ZEOCHEM LLC
    Inventors: Kerry C. Weston, Patrick Purcell
  • Patent number: 7651550
    Abstract: A desorption process and a process for producing a catalytically deactivated formed zeolitic adsorbent, whereby both processes are suitable to improve the lifetime of a formed zeolitic adsorbent in the removal of sulfur compounds from sulfur contaminated gas and liquid feed streams. The adsorbent is in particular a synthetic 13X or LSX faujasite with a silica to alumina ratio from 1.9:1.0 to about 3.0:1.0. The cations of the faujasite include alkali and alkaline earth metals. The formed zeolite mixture is preferably catalytically deactivated due to a phosphate treatment. The desorption is carried out thermally, wherein the heat treatment is done at different temperature stages to avoid decomposition of the organic sulfur compounds.
    Type: Grant
    Filed: June 6, 2003
    Date of Patent: January 26, 2010
    Assignee: Zeochem AG
    Inventors: Peter Hawes, Andreas Scheuble, Beat Kleeb, Armin Pfenninger
  • Patent number: 7300899
    Abstract: A lithium exchanged zeolite X adsorbent blend with improved performance characteristics produced by preparing a zeolite X, preparing a binder which includes highly dispersed attapulgite fibers wherein the tapped bulk density of the highly dispersed attapulgite fibers measured according to DIN/ISO 787 is more than about 550 g/ml, mixing the zeolite X with the binder to form a mixture, forming the mixture into a shaped material, ion exchanging the zeolite X at least 75% with lithium ions, and calcining the shaped material.
    Type: Grant
    Filed: July 8, 2005
    Date of Patent: November 27, 2007
    Assignee: Zeochem, LLC
    Inventors: Kerry Weston, Dave Jaussaud, Robert L. Chiang
  • Publication number: 20070193939
    Abstract: Abstract Described is a desorption process and a process for producing a catalytically deactivated formed zeolitic adsorbent, whereby both processes are suitable to improve the lifetime of a formed zeolithic adsorbant in the removal of sulfur compounds from sulfur contaminated gas and liquid feed streams. The adsorbent is in particular a synthetic 13X or LSX faujasite with a silica to alumina ratio from 1.9:1.0 to about 3.0:1.0. The cations of the faujasite include alkali and alkaline earth metals. The formed zeolite mixture is preferably catalytically deactivated due to a phosphate treatment. The desorption is carried out thermally, wherein the heat treatment is done at different temperature stages to avoid decomposition of the organic sulfur compounds.
    Type: Application
    Filed: June 6, 2003
    Publication date: August 23, 2007
    Applicant: ZEOCHEM AG
    Inventors: Peter Hawes, Andreas Scheuble, Beat Kleeb, Armin Pfenninger
  • Publication number: 20070062369
    Abstract: Disclosed is a synthetic zeolite by means of which gas streams containing steam and carbon dioxide as impurities can be purified. The zeolitic adsorbing agent is a 13X type or LSX type faujasite or a mixture of both types that are deformed with a binder, at least some parts of which are highly dispersed. Said novel adsorption system allows extraordinarily high adsorption capacities to be obtained while keeping the mass transfer zones short resulting in a longer service life of the adsorption systems before carbon dioxide is able to break through.
    Type: Application
    Filed: April 7, 2004
    Publication date: March 22, 2007
    Applicant: ZEOCHEM AG
    Inventors: Armin Pfenninger, Sonja Odolo-Hitz
  • Publication number: 20060043001
    Abstract: A method for producing a substantially desulfurized hydrocarbon fuel stream at temperatures less than 100° C. including providing a nondesulfurized fuel cell hydrocarbon fuel stream and passing the fuel stream through a sequential sulfur adsorbent bed system containing at least one selective sulfur adsorbent and a calcium exchanged zeolite to produce a substantially desulfurized hydrocarbon fuel stream.
    Type: Application
    Filed: August 18, 2005
    Publication date: March 2, 2006
    Applicants: Sud-Chemie Inc., Zeochem, LLC.
    Inventors: Eric Weston, R. Spivey, Kerry Weston
  • Publication number: 20050272594
    Abstract: A lithium exchanged zeolite X adsorbent blend with improved performance characteristics produced by preparing a zeolite X, preparing a binder which includes highly dispersed attapulgite fibers wherein the tapped bulk density of the highly dispersed attapulgite fibers measured according to DIN/ISO 787 is more than about 550 g/ml, mixing the zeolite X with the binder to form a mixture, forming the mixture into a shaped material, ion exchanging the zeolite X at least 75% with lithium ions, and calcining the shaped material.
    Type: Application
    Filed: July 8, 2005
    Publication date: December 8, 2005
    Applicant: Zeochem, LLC
    Inventors: Kerry Weston, Dave Jaussaud, Robert Chiang
  • Patent number: 6918948
    Abstract: A Process for the production and uses of a molecular sieve adsorbent blend product with improved performance characteristics produced by preparing a zeolite powder, preparing a highly dispersed attapulgite fiber binder, mixing the zeolite powder with the highly dispersed attapulgite binder to form a mixture, forming molecular sieve adsorbent products into a shaped material and calcining the shaped material, wherein the tapped bulk density of the highly dispersed attapulgite fibers measured according to DIN/ISO 787 is more than about 550 g/ml.
    Type: Grant
    Filed: January 26, 2004
    Date of Patent: July 19, 2005
    Assignee: Zeochem LLC
    Inventors: Dave Jaussaud, Kerry Weston, Armin Pfenninger, Beat Kleeb
  • Publication number: 20050119112
    Abstract: A process for the production of a molecular sieve adsorbent blend with improved performance characteristics produced by preparing a zeolite material, which may include zeolite 13X, zeolite LSX or mixtures thereof, preparing a binder which includes highly dispersed attapulgite fibers alone or blended with a non-highly dispersed attapulgite clay, mixing the zeolite material with the binder to form a mixture, forming molecular sieve adsorbent blends into a shaped material and treating the shaped material, wherein the tapped bulk density of the highly dispersed attapulgite fibers measured according to DIN/ISO 787 is more than about 550 g/ml.
    Type: Application
    Filed: September 13, 2004
    Publication date: June 2, 2005
    Applicant: Zeochem, LLC
    Inventors: Armin Pfenninger, Sonja Odolo-Hitz, Kerry Weston, Beat Kleeb, Dave Jaussaud
  • Patent number: 6743745
    Abstract: A process for the production of a molecular sieve adsorbent blend product with improved performance characteristics produced by preparing a zeolite powder, preparing a highly dispersed attapulgite fiber binder, mixing the zeolite powder with the highly dispersed attapulgite binder to form a mixture, forming molecular sieve adsorbent products into a shaped material and calcining the shaped material, wherein the tapped bulk density of the highly dispersed attapulgite fibers measured according to DIN/ISO 787 is more than about 550 g/ml.
    Type: Grant
    Filed: January 22, 2002
    Date of Patent: June 1, 2004
    Assignee: Zeochem
    Inventors: Dave Jaussaud, Kerry Weston, Armin Pfenninger, Beat Kleeb
  • Publication number: 20030171205
    Abstract: A process for the production of a molecular sieve adsorbent blend product with improved performance characteristics produced by preparing a zeolite powder, preparing a highly dispersed attapulgite fiber binder, mixing the zeolite powder with the highly dispersed attapulgite binder to form a mixture, forming molecular sieve adsorbent products into a shaped material and calcining the shaped material, wherein the tapped bulk density of the highly dispersed attapulgite fibers measured according to DIN/ISO 787 is more than about 550 g/ml.
    Type: Application
    Filed: January 22, 2002
    Publication date: September 11, 2003
    Applicant: ZEOCHEM LLC
    Inventors: Dave Jaussaud, Kerry Weston, Armin Pfenninger, Beat Kleeb
  • Patent number: 6530975
    Abstract: A molecular sieve adsorbent for the purification of gas streams containing water vapor and carbon dioxide. The adsorbent is a combination of sodium form of a low-silica faujasite, having a residual content of potassium ions less than about 8.0 percent (equiv.), a low content of crystalline and amorphous admixtures and crystal sizes generally within the range of 1-4 &mgr;m, and a binder. A process for the adsorbent preparation which comprises specific parameters of low silica faujasite synthesis, sodium-potassium ion exchange, blending and granulation.
    Type: Grant
    Filed: January 19, 2001
    Date of Patent: March 11, 2003
    Assignee: Zeochem
    Inventors: Edward J. Rode, Albert M. Tsybulevskiy